JP5227809B2 - チタン金属表面をチタンのナノメートル粒子で機能化する方法及び機能化された製品 - Google Patents

チタン金属表面をチタンのナノメートル粒子で機能化する方法及び機能化された製品 Download PDF

Info

Publication number
JP5227809B2
JP5227809B2 JP2008552819A JP2008552819A JP5227809B2 JP 5227809 B2 JP5227809 B2 JP 5227809B2 JP 2008552819 A JP2008552819 A JP 2008552819A JP 2008552819 A JP2008552819 A JP 2008552819A JP 5227809 B2 JP5227809 B2 JP 5227809B2
Authority
JP
Japan
Prior art keywords
titanium
titanium dioxide
suspension
nanometer particles
nanometer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2008552819A
Other languages
English (en)
Japanese (ja)
Other versions
JP2009525405A (ja
JP2009525405A5 (enExample
Inventor
バルディ・ジョヴァンニ
ビトッシ・マルコ
バルヅァンティ・アンドレア
Original Assignee
コロロッビア イタリア ソシエタ ペル アチオニ
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by コロロッビア イタリア ソシエタ ペル アチオニ filed Critical コロロッビア イタリア ソシエタ ペル アチオニ
Publication of JP2009525405A publication Critical patent/JP2009525405A/ja
Publication of JP2009525405A5 publication Critical patent/JP2009525405A5/ja
Application granted granted Critical
Publication of JP5227809B2 publication Critical patent/JP5227809B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C20/00—Chemical coating by decomposition of either solid compounds or suspensions of the coating forming compounds, without leaving reaction products of surface material in the coating
    • C23C20/02—Coating with metallic material
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
    • A61L27/28—Materials for coating prostheses
    • A61L27/30—Inorganic materials
    • A61L27/306—Other specific inorganic materials not covered by A61L27/303 - A61L27/32
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
    • A61L27/02—Inorganic materials
    • A61L27/04—Metals or alloys
    • A61L27/06—Titanium or titanium alloys
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/04—Pretreatment of the material to be coated
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208—Oxides, e.g. ceramics
    • C23C18/1216—Metal oxides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C23C18/1262—Process of deposition of the inorganic material involving particles, e.g. carbon nanotubes [CNT], flakes
    • C23C18/127—Preformed particles
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C20/00—Chemical coating by decomposition of either solid compounds or suspensions of the coating forming compounds, without leaving reaction products of surface material in the coating
    • C23C20/02—Coating with metallic material
    • C23C20/04—Coating with metallic material with metals
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2400/00—Materials characterised by their function or physical properties
    • A61L2400/12—Nanosized materials, e.g. nanofibres, nanoparticles, nanowires, nanotubes; Nanostructured surfaces
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Transplantation (AREA)
  • Veterinary Medicine (AREA)
  • Medicinal Chemistry (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Dermatology (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Ceramic Engineering (AREA)
  • Nanotechnology (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Materials For Medical Uses (AREA)
  • Dental Preparations (AREA)
  • Dental Tools And Instruments Or Auxiliary Dental Instruments (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Paints Or Removers (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)
  • Powder Metallurgy (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Catalysts (AREA)
JP2008552819A 2006-02-03 2007-02-02 チタン金属表面をチタンのナノメートル粒子で機能化する方法及び機能化された製品 Expired - Fee Related JP5227809B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IT000034A ITFI20060034A1 (it) 2006-02-03 2006-02-03 Processo per la funzionalizzazione di superfici metalliche in titanio con particelle di titanio nanometriche e prodotti cosi' funzionalizzati
ITFI2006A000034 2006-02-03
PCT/EP2007/051030 WO2007088199A2 (en) 2006-02-03 2007-02-02 A process for functionalizing titanium metal surfaces with nanometric particles of titanium and products thus functionalized

Publications (3)

Publication Number Publication Date
JP2009525405A JP2009525405A (ja) 2009-07-09
JP2009525405A5 JP2009525405A5 (enExample) 2012-09-20
JP5227809B2 true JP5227809B2 (ja) 2013-07-03

Family

ID=38222232

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2008552819A Expired - Fee Related JP5227809B2 (ja) 2006-02-03 2007-02-02 チタン金属表面をチタンのナノメートル粒子で機能化する方法及び機能化された製品

Country Status (13)

Country Link
US (1) US8118923B2 (enExample)
EP (1) EP1989342B1 (enExample)
JP (1) JP5227809B2 (enExample)
KR (1) KR101409714B1 (enExample)
CN (1) CN101379216B (enExample)
AU (1) AU2007211493B2 (enExample)
BR (1) BRPI0707257B8 (enExample)
CA (1) CA2641180C (enExample)
IT (1) ITFI20060034A1 (enExample)
NZ (1) NZ570394A (enExample)
RU (1) RU2432182C2 (enExample)
WO (1) WO2007088199A2 (enExample)
ZA (1) ZA200806990B (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007029672A1 (de) * 2007-06-27 2009-01-02 Lzh Laserzentrum Hannover E.V. Implantat und Verfahren zu dessen Herstellung
WO2011113568A1 (en) 2010-03-15 2011-09-22 Nobel Biocare Services Ag Surface treatment method
CZ303566B6 (cs) * 2010-11-30 2012-12-12 Zpusob depozice nanocástic kovu na povrch substrátu
KR101771089B1 (ko) 2012-01-19 2017-08-24 삼성에스디아이 주식회사 복합음극활물질, 그 제조방법, 이를 포함하는 음극 및 리튬전지
CN103041976B (zh) * 2012-12-25 2014-04-30 苏州大学附属第二医院 口腔用CoCr合金材料表面制备含银抗菌涂层的方法
PT107263B (pt) 2013-10-30 2019-04-10 Innovnano - Materiais Avançados, Sa. Suspensão de óxido metálico, seu fabrico e utilizações
RU2554819C1 (ru) * 2014-04-16 2015-06-27 Общество с ограниченной ответственностью "КОНМЕТ" Способ получения биоактивного покрытия на имплантируемом в костную ткань человека титановом имплантате
US10481116B2 (en) 2014-10-30 2019-11-19 BAE Systems Information and Electronic Systems Integratlon Inc. High resolution inspection device for casting defects using IR imaging
US11052460B2 (en) * 2017-02-01 2021-07-06 Hrl Laboratories, Llc Methods for nanofunctionalization of powders, and nanofunctionalized materials produced therefrom

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI91713C (fi) 1992-04-23 1994-08-10 Axidental Oy Uusia bioaktiivisia pinnotteita ja niiden valmistus ja käyttö
JPH072522A (ja) * 1992-12-21 1995-01-06 Ishihara Sangyo Kaisha Ltd 酸化チタン膜の製造方法
JP2517874B2 (ja) * 1993-09-30 1996-07-24 工業技術院長 酸化チタン薄膜光触媒の製造方法
JP3655349B2 (ja) * 1995-04-28 2005-06-02 株式会社日立製作所 炭酸ガス変換装置
JP3567693B2 (ja) * 1996-10-22 2004-09-22 住友金属工業株式会社 固定化光触媒の製造方法および有害物質の分解・除去方法
JP3122082B2 (ja) * 1999-02-04 2001-01-09 川崎重工業株式会社 酸化チタンコート材の製造方法
JP2001089142A (ja) * 1999-09-27 2001-04-03 Nok Corp 酸化チタン膜の製造方法
RU2159094C1 (ru) * 1999-11-01 2000-11-20 Закрытое акционерное общество Клиническое научно-производственное объединение "Биотехника" Способ нанесения покрытия на имплантат из титана и его сплавов
JP5019084B2 (ja) * 1999-12-03 2012-09-05 クラレノリタケデンタル株式会社 歯科・口腔用組成物
JP2002088485A (ja) * 2000-09-12 2002-03-27 Kawasaki Heavy Ind Ltd 金属部材への防眩方法
DE10243132B4 (de) * 2002-09-17 2006-09-14 Biocer Entwicklungs Gmbh Antiinfektiöse, biokompatible Titanoxid-Beschichtungen für Implantate sowie Verfahren zu deren Herstellung
AU2003250566A1 (en) * 2003-05-21 2004-12-13 Dentium Co., Ltd Titanium substrate for biocompatible implant coated with hydroxyapatite/titania double layer and a coating method of the same
EP1527790B1 (de) * 2003-10-27 2008-08-13 Straumann Holding AG Implantat mit einer keramischen Beschichtung
ITFI20040252A1 (it) * 2004-12-06 2005-03-06 Colorobbia Italiana Spa Processo per la preparazione di dispersioni di ti02 in forma di nanoparticelle, e dispersioni ottenibili con questo processo
ITFI20060030A1 (it) 2006-02-01 2007-08-02 Colorobbia Italiana Spa Processo per la preparazione di dispersioni acquose di ti02 in forma nanoparticelle e dispersioni ottenibili con questo processo

Also Published As

Publication number Publication date
KR20080100811A (ko) 2008-11-19
ITFI20060034A1 (it) 2007-08-04
CA2641180C (en) 2014-07-22
AU2007211493B2 (en) 2012-03-22
NZ570394A (en) 2010-06-25
WO2007088199A3 (en) 2007-09-13
BRPI0707257B8 (pt) 2021-06-22
EP1989342A2 (en) 2008-11-12
CN101379216B (zh) 2013-04-17
US20090114124A1 (en) 2009-05-07
JP2009525405A (ja) 2009-07-09
RU2008135707A (ru) 2010-03-10
US8118923B2 (en) 2012-02-21
RU2432182C2 (ru) 2011-10-27
BRPI0707257B1 (pt) 2018-10-16
AU2007211493A1 (en) 2007-08-09
KR101409714B1 (ko) 2014-07-02
CA2641180A1 (en) 2007-08-09
ZA200806990B (en) 2009-06-24
CN101379216A (zh) 2009-03-04
EP1989342B1 (en) 2019-01-09
WO2007088199A2 (en) 2007-08-09
BRPI0707257A2 (pt) 2011-04-26

Similar Documents

Publication Publication Date Title
JP2009525405A (ja) チタン金属表面をチタンのナノメートル粒子で機能化する方法及び機能化された製品
JP2009525405A5 (enExample)
JP2008522931A (ja) ナノ微粒子形状のTiO2分散の調製方法、並びにこの方法により得られる分散及びTiO2分散利用による表面特性変化
JP2010539101A5 (enExample)
JP2008150708A5 (enExample)
US8764916B2 (en) Agent for the production of anti-corrosion layers on metal surfaces
Kiele et al. Methyl–modified hybrid organic-inorganic coatings for the conservation of copper
JP2008522931A5 (enExample)
JP2010094583A (ja) 有機薄膜の製造方法
WO2010140501A1 (ja) 新規チタン酸モノマーおよびその高分子ならびにその製造方法および用途
CN1846007A (zh) 三元银合金
CN108774592A (zh) 一种夏天用汽车玻璃水及其制备方法
JP2012502871A (ja) リン酸チタン(iv)の生成方法
FR3040641A1 (fr) Procede d'application d'un revetement anticorrosion sur une piece metallique, composition de revetement aqueux, revetement anticorrosion de pieces metalliques et piece metallique revetue
JP2007125548A (ja) 基材をオゾン水又は過酸化水素水で洗浄する工程を含む、有機薄膜の製造方法
CN108103474B (zh) 类金刚石膜的制备方法
JP2008104996A (ja) 光触媒、光触媒形成用塗布液、及び光触媒の製造方法
JP4034885B2 (ja) 光触媒性塗料組成物
JP3670755B2 (ja) リン酸カルシウム系皮膜の形成方法
JP2010037173A (ja) 防汚性製品及びその製造方法
JP2025151445A (ja) 槽の洗浄方法及びシリカ粒子の製造方法
JPS605524B2 (ja) アルミナまたはシリカ−アルミナ被膜形成方法
JP2010215424A (ja) メタチタン酸粒子分散液
JPH07145487A (ja) 珪酸系コーティング剤
JPS6026673A (ja) 銅の防錆方法

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20100201

RD02 Notification of acceptance of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7422

Effective date: 20100201

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A821

Effective date: 20100202

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20120425

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20120507

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20120802

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20121010

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20130108

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20130117

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130131

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20130228

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20130318

R150 Certificate of patent or registration of utility model

Ref document number: 5227809

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20160322

Year of fee payment: 3

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees