JP5171266B2 - 防汚性を有する複合部材 - Google Patents
防汚性を有する複合部材 Download PDFInfo
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- JP5171266B2 JP5171266B2 JP2007553882A JP2007553882A JP5171266B2 JP 5171266 B2 JP5171266 B2 JP 5171266B2 JP 2007553882 A JP2007553882 A JP 2007553882A JP 2007553882 A JP2007553882 A JP 2007553882A JP 5171266 B2 JP5171266 B2 JP 5171266B2
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Classifications
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- B32B27/18—Layered products comprising a layer of synthetic resin characterised by the use of special additives
- B32B27/20—Layered products comprising a layer of synthetic resin characterised by the use of special additives using fillers, pigments, thixotroping agents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1606—Antifouling paints; Underwater paints characterised by the anti-fouling agent
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B32B27/14—Layered products comprising a layer of synthetic resin next to a particulate layer
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- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/042—Coating with two or more layers, where at least one layer of a composition contains a polymer binder
- C08J7/0423—Coating with two or more layers, where at least one layer of a composition contains a polymer binder with at least one layer of inorganic material and at least one layer of a composition containing a polymer binder
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
- D06M13/5135—Unsaturated compounds containing silicon atoms
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M14/00—Graft polymerisation of monomers containing carbon-to-carbon unsaturated bonds on to fibres, threads, yarns, fabrics, or fibrous goods made from such materials
- D06M14/18—Graft polymerisation of monomers containing carbon-to-carbon unsaturated bonds on to fibres, threads, yarns, fabrics, or fibrous goods made from such materials using wave energy or particle radiation
- D06M14/26—Graft polymerisation of monomers containing carbon-to-carbon unsaturated bonds on to fibres, threads, yarns, fabrics, or fibrous goods made from such materials using wave energy or particle radiation on to materials of synthetic origin
- D06M14/30—Graft polymerisation of monomers containing carbon-to-carbon unsaturated bonds on to fibres, threads, yarns, fabrics, or fibrous goods made from such materials using wave energy or particle radiation on to materials of synthetic origin of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M14/32—Polyesters
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
- D06M15/277—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof containing fluorine
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- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/08—Processes in which the treating agent is applied in powder or granular form
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B32B2255/00—Coating on the layer surface
- B32B2255/20—Inorganic coating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
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- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/73—Hydrophobic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
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- C—CHEMISTRY; METALLURGY
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
- C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- D—TEXTILES; PAPER
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2400/00—Specific information on the treatment or the process itself not provided in D06M23/00-D06M23/18
- D06M2400/01—Creating covalent bondings between the treating agent and the fibre
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
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- Y10T428/25—Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
- Y10T428/254—Polymeric or resinous material
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31652—Of asbestos
- Y10T428/31663—As siloxane, silicone or silane
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
- Y10T442/20—Coated or impregnated woven, knit, or nonwoven fabric which is not [a] associated with another preformed layer or fiber layer or, [b] with respect to woven and knit, characterized, respectively, by a particular or differential weave or knit, wherein the coating or impregnation is neither a foamed material nor a free metal or alloy layer
- Y10T442/2164—Coating or impregnation specified as water repellent
- Y10T442/218—Organosilicon containing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
- Y10T442/20—Coated or impregnated woven, knit, or nonwoven fabric which is not [a] associated with another preformed layer or fiber layer or, [b] with respect to woven and knit, characterized, respectively, by a particular or differential weave or knit, wherein the coating or impregnation is neither a foamed material nor a free metal or alloy layer
- Y10T442/2279—Coating or impregnation improves soil repellency, soil release, or anti- soil redeposition qualities of fabric
- Y10T442/2287—Fluorocarbon containing
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- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Toxicology (AREA)
- Laminated Bodies (AREA)
- Paints Or Removers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Graft Or Block Polymers (AREA)
Description
1 :基体
2 :無機微粒子
3 :シランモノマー
4 :バインダー成分
5 :化学結合
10 :無機微粒子層
ば、ビニルトリメトキシシランや、ビニルトリエトキシシランや、ビニルトリアセトキシシランや、N−β−(N−ビニルベンジルアミノエチル)−γ−アミノプロピルトリメトキシシランなどが用いられる。
物、例えば、メチルトリルメトキシシランや、メチルトリエトキシシランや、ジメチルジエトキシシランや、フェニルトリエトキシシランや、ヘキサメチルジシラザンや、ヘキシルトリメトキシシランなどが用いられる。
無機微粒子として市販の二酸化チタン粒子(石原産業株式会社製、TTO−S−1)をメタノールに10.0質量%分散してpHを4.0に塩酸で調製する。その後、二酸化チタン粒子をビーズミルにより平均粒子径15nmに粉砕分散した。得られた分散溶液にシランモノマーとして不飽和結合を有する3−メタクリロキシプロピルトリメトキシシラン(信越化学工業株式会社製、KBM−503)を無機微粒子に対して3.0質量%加える。
インダー成分を含む上記粉砕分散溶液をバーコーターで塗布し、110℃、1分間乾燥した。次に、二酸化チタン微粒子分散液を塗布したポリエステルフィルムに電子線を200kVの加速電圧で5Mrad照射することで、二酸化チタン微粒子をシランモノマーのグラフト重合によりポリエステルフィルム表面に結合させた防塵特性を有する複合部材を得た。
実施例1において、粉砕分散溶液中にバインダー成分として、撥水性を有する物質として、(1)アクリル単量体としてステアリルアクリレート(共栄社化学工業株式会社製)を、(2)シリコーン系オリゴマー(松下電気産業株式会社製、フレッセラD)を、シランモノマーで被覆された無機微粒子の含有量に対して15質量%の含有量となるように添加すること以外は実施例1と同様である。
無機微粒子として市販の二酸化チタン微粒子(テイカ株式会社製、MT−100HD)をメタノールに対して10.0質量%、シランモノマーとして3−メタクリロキシプロピ
ルトリメトキシシラン(信越化学工業株式会社製、KBM−503)を微粒子に対して3.0質量%加えてpHを3.0に塩酸で調製した。その後、二酸化チタン微粒子をビーズミルにより平均粒子径18nmに粉砕分散した。その後、凍結乾燥機により固液分離して120℃で加熱してシランモノマーを二酸化チタン微粒子の表面に脱水縮合反応により化学結合させて被覆を形成した。得られた表面処理された二酸化チタン微粒子をメタノールに10.0質量%添加し、バインダー成分としてパーフルオロアルキル基とシラノール基を有するオリゴマー(信越化学工業株式会社製KP−801M)を、シランモノマーで被覆された無機微粒子の含有量に対して(1)1質量%、(2)5質量%、(3)10質量%の含有量となるように添加すること以外は実施例1と同様である。
実施例1で使用基体であるポリエステルフィルムの代わりに、ポリエステル製80メッシュに無機微粒子層を形成したこと以外は実施例1と同様である。
実施例3で使用基体であるポリエステルフィルムの代わりに、ポリエステル製80メッシュに無機微粒子層を形成したこと以外は実施例3と同様である。
実施例3で使用基体であるポリエステルフィルムの代わりに、目付けが70g/m2のポリエステル製不織布(旭化成株式会社製、エルタスE01070)に無機微粒子層を形成したこと以外は実施例3と同様である。
実施例3において、分散溶液中にバインダー成分を(1)0.1質量%、(2)40質量%、の含有量となるように添加すること以外は、実施例3と同様である。
実施例7において、電子線を照射せず、すなわち二酸化チタン微粒子をシランモノマーのグラフト重合によりポリエステルフィルム表面に結合させる工程を省く以外は、実施例7と同様である。
実施例3において、分散溶液中にバインダー成分を(1)添加しない、(2)0.05質量%の含有量になるように添加すること以外は実施例3と同様である。
実施例3で用いた分散溶液中にバインダー成分としてペンタエリスリトールトリアクリレート(共栄社化学工業株式会社製)を50質量%添加し、ポリエステルフィルム基体に替えてポリエステル製80メッシュを用いた以外は実施例3と同様である。
ポリエステル製80メッシュに処理を施さないそのままの状態で特性を評価した。
実施例5で用いたポリエステル製80メッシュに、市販の撥水・撥油性を付与する処理剤(住友スリーエム株式会社製、SCOTCHGARD)をスプレー塗布して室温で2時間以上放置後、特性を評価した。
市販のフッ素系樹脂からなる目付けが70g/m2の不織布(日東電工株式会社製、NTF9307)を、処理を施さないそのままの状態で特性を評価した。
防塵性は、それぞれのサンプルを10×10cmの大きさに切り取り、JIS Z 8901に準拠した、関東ローム、ケイ砂、混合ダストの3種類を満遍なく振りかけた後、質量を測定してダスト付着前後の試験サンプルの質量を測定して評価した。
Claims (13)
- 基体と、
不飽和結合部を有するシランモノマーが不飽和結合を外側に向けて配向することで被覆された無機微粒子と、バインダー成分と、を含み、前記基体の表面部に備わる無機微粒子層と、
を有し、
前記無機微粒子層に含まれる前記バインダー成分の含有量が、前記無機微粒子の含有量に対して、0.1質量%以上40質量%以下であり、
前記無機微粒子層内の無機微粒子同士は、互いのシランモノマーの不飽和結合部が化学結合することにより、前記無機微粒子層を形成するとともに、
前記無機微粒層内の無機微粒子のシランモノマーの不飽和結合部と前記基体の表面部とが化学結合することにより、前記基体と前記無機微粒子層とが固定されてなることを特徴とする防汚性を有する複合部材。 - 前記バインダー成分は、少なくとも撥水性や撥油性を有する化合物を含む請求項1に記載の防汚性を有する複合部材。
- 前記バインダー成分は、少なくともフッ素系化合物を含む請求項1記載に記載の防汚性を有する複合部材。
- 前記化学結合は、グラフト重合であることを特徴とする請求項1に記載の防汚性を有する複合部材。
- 前記グラフト重合は、放射線グラフト重合であることを特徴とする請求項4に記載の防汚性を有する複合部材。
- 前記基体の少なくとも表面が樹脂であることを特徴とする請求項1に記載の防汚性を有する複合部材。
- 前記基体は、樹脂であることを特徴とする請求項1に記載の防汚性を有する複合部材。
- 前記基体は、繊維構造体であることを特徴とする請求項1に記載の防汚性を有する複合部材。
- 請求項7に記載の防汚性を有する複合部材を用いてなることを特徴とする衣類。
- 請求項7に記載の防汚性を有する複合部材を用いてなることを特徴とするフィルター。
- 請求項7に記載の防汚性を有する複合部材を用いてなることを特徴とする防虫網。
- 請求項6に記載の防汚性を有する複合部材を用いてなることを特徴とする建装材。
- 請求項7に記載の防汚性を有する複合部材を用いてなることを特徴とする内装材。
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KR (1) | KR101314287B1 (ja) |
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CA2631131C (en) | 2013-10-29 |
RU2008132469A (ru) | 2010-02-20 |
CN101341025B (zh) | 2012-05-30 |
CN101341025A (zh) | 2009-01-07 |
WO2007080804A1 (ja) | 2007-07-19 |
HK1126449A1 (en) | 2009-09-04 |
KR101314287B1 (ko) | 2013-10-02 |
EP1972437A1 (en) | 2008-09-24 |
BRPI0621186B1 (pt) | 2019-04-09 |
BRPI0621186A2 (pt) | 2012-05-22 |
CA2631131A1 (en) | 2007-07-19 |
AU2006335491A1 (en) | 2007-07-19 |
AU2006335491B2 (en) | 2011-01-27 |
KR20080083624A (ko) | 2008-09-18 |
RU2453441C2 (ru) | 2012-06-20 |
US20090094954A1 (en) | 2009-04-16 |
EP1972437B1 (en) | 2016-05-11 |
EP1972437A4 (en) | 2012-03-21 |
US8349447B2 (en) | 2013-01-08 |
JPWO2007080804A1 (ja) | 2009-06-11 |
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