JP4809324B2 - 水性ポリマー分散物およびそれらの分散物による製品 - Google Patents
水性ポリマー分散物およびそれらの分散物による製品 Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/0427—Coating with only one layer of a composition containing a polymer binder
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/043—Improving the adhesiveness of the coatings per se, e.g. forming primers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/052—Forming heat-sealable coatings
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/26—Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
- Y10T428/263—Coating layer not in excess of 5 mils thick or equivalent
- Y10T428/264—Up to 3 mils
- Y10T428/265—1 mil or less
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31855—Of addition polymer from unsaturated monomers
- Y10T428/31938—Polymer of monoethylenically unsaturated hydrocarbon
Description
{N}=KMa
式中、Kpp=1.90×10-4、app=0.725およびKps=1.26×10-4、aps=0.702。
(融点および結晶性)
実施例
約28重量%のビニルアセテート含有率、約0.95g/cm3の密度(ASTM D−792)および約6g/10分のメルトインデックス(190℃および2.16kgにてASTM D1238に従って決定したように)、ならびに約73℃の融点(ASTM D3417に従って決定したように)を有する、DuPontより市販されている熱可塑性エチレン−ビニルアセテート 100重量部と、C32カルボン酸(Baker−Petroliteによって製造されたUnicid 425、酸価97mg KOH/g)4.2重量部とを180℃にて2軸スクリュー押出機内で、8.3kg/時の速度にて溶融混練する。
(製造例2)
(製造例3)
(製造例4)
(製造例5)
(製造例6)
(分散物の生成(ステップ200))
ヒートシール挙動−ヒートシール開始温度、シール強度、およびホットタック;
ベースフィルム基材への接着;
フィルム形成特性−分散物の乾燥中に、粒子は好ましくは凝集して、凝集性の透明層を形成する。
分散粒径;
フィルム形成特徴;
剪断および貯蔵安定性−分散物が分散物特性(たとえば粒径)の著しい変化なしに、高剪断(剪断安定性)および長時間(貯蔵安定性)に耐える能力;
湿潤性−基材上での「引込み」または「ビーズ化」なしに基材上へ流れる能力;
基材への接着。
(コーティング用途条件(ステップ202))
(乾燥条件(ステップ204))
Claims (28)
- ヒートシールが可能なコーティングされた基材を形成する方法であって:
2軸延伸された基材を選択するステップと;
樹脂溶融物を形成するための(A)少なくとも1つの熱可塑性ポリマーおよび(B)少なくとも1つの分散剤の押出機における溶融混練と、(C)水とに由来し、かつ8〜11のpHおよび5ミクロン未満の平均体積粒径を有する水性分散物を選択するステップであって、前記押出機において塩基および初期水を前記樹脂溶融物に供給して1〜3重量%の水を含有する乳化混合物を形成し、前記押出機において前記乳化混合物を最初に希釈して25重量%を超える水を含有させ、前記押出機から前記乳化混合物を押し出した後に追加の水を含むように前記乳化混合物をさらに希釈して前記水性分散物を形成し、前記(A)少なくとも1つの熱可塑性ポリマーが、エチレンと、C 4 −C 20 直鎖、分岐または環状ジエン、ビニルアセテート、および式H 2 C=CHR(式中、RはC 1 −C 20 直鎖、分岐または環状アルキル基またはC 6 −C 20 アリール基である)によって表される化合物から成る群より選択される少なくとも1つのコモノマーとのインターポリマー、または、プロピレンと、C 2 あるいはC 4 −C 20 直鎖、分岐または環状ジエン、ビニルアセテート、および式H 2 C=CHR(式中、RはC 2 −C 20 直鎖、分岐または環状アルキル基またはC 6 −C 20 アリール基である)によって表される化合物から成る群より選択される少なくとも1つのコモノマーとのインターポリマーを含むステップと;
前記水性分散物を前記2軸延伸された基材の少なくとも1つの面に塗布するステップと;
前記水の少なくとも一部を除去するステップであって、コーティング層を形成するために、前記水性分散物の前記熱可塑性ポリマーのピーク融点より20℃高い温度〜前記延伸された基材の軟化点より20℃低い温度にて前記水性分散物を乾燥するステップと;
それによって前記2軸延伸された基材を被覆するコーティング層を形成するステップと;
それによって前記コーティングされた基材を形成するステップと;
を含む方法。 - 前記2軸延伸された基材が、ポリエステル、ポリカーボネート、ポリアリーレート、ポリアミド、ポリイミド、ポリアミド−イミド、ポリエーテル−アミド、ポリエーテルイミド、ポリアリールエーテル、ポリアリールエーテルケトン、脂肪族ポリケトン、ポリフェニレンスルフィド、ポリスルホン、ポリスチレンおよびその誘導体、ポリアクリレート、ポリメタクリレート、セルロース誘導体、ポリエチレン、ポリオレフィン、主にオレフィンモノマーを有するコポリマー、フッ素化ポリマーおよびコポリマー、塩素化ポリマー、ポリアクリロニトリル、ポリビニルアセテート、ポリビニルアルコール、ポリエーテル、アイオノマー樹脂、エラストマー、シリコーン樹脂、エポキシ樹脂、ポリウレタン、混和性または非混和性ポリマー混合物、又は上述のポリマーのいずれかの構成モノマーのいずれかのコポリマーを含む、請求項1に記載の方法。
- 前記2軸延伸された基材が2軸配向ポリプロピレン、2軸配向ポリアミド、2軸配向ポリエステル、2軸配向ポリエチレン、および2軸配向ポリスチレンから成る群より選択される少なくとも1つを含む、請求項2に記載の方法。
- 前記少なくとも1つの熱可塑性ポリマーが、少なくとも60重量パーセントのプロピレン由来単位および少なくとも0.1重量パーセントのエチレン由来単位を含むプロピレン/エチレンコポリマーを含み、該コポリマーは、14.6ppmおよび15.7ppmにおけるレジオエラーに相当する13C NMRピークであって、等しい強度のピークを有し、前記ピークは、成長コポリマー鎖へのプロピレン単位の立体選択性2,1−挿入エラーの結果であることを特徴とする、請求項1から3のいずれかに記載の方法。
- 前記熱可塑性ポリマーが0.85〜0.90g/ccの密度を有する、請求項1に記載の方法。
- 前記コーティングされた基材が、他の層をさらに含む、請求項1から5のいずれかに記載の方法。
- 前記分散物が2ミクロン未満の平均体積粒径を有する、請求項1に記載の方法。
- 前記分散物が1ミクロン未満の平均体積粒径を有する、請求項7に記載の方法。
- 前記コーティング層が乾燥後に0.5〜75ミクロンの範囲の厚さを有する、請求項1から8のいずれかに記載の方法。
- 前記コーティング層が乾燥後に0.5〜25ミクロンの範囲の厚さを有する、請求項9に記載の方法。
- 前記コーティング層が乾燥後に0.75〜2ミクロンの範囲の厚さを有する、請求項10に記載の方法。
- 前記コーティング層をヒートシール開始温度まで加熱するステップをさらに含む、請求項1から11のいずれかに記載の方法。
- 前記ヒートシール開始温度が80℃未満である、請求項12に記載の方法。
- 前記ヒートシール開始温度が70℃未満である、請求項13に記載の方法。
- ヒートシールが可能なコーティングされた基材を形成する方法であって:
熱可塑性の基材を選択するステップと;
樹脂溶融物を形成するための(A)少なくとも1つの熱可塑性ポリマーおよび(B)少なくとも1つの分散剤の押出機における溶融混練と、(C)水とに由来し、かつ8〜11のpHおよび5ミクロン未満の平均体積粒径を有する水性分散物を選択するステップであって、前記押出機において塩基および初期水を前記樹脂溶融物に供給して1〜3重量%の水を含有する乳化混合物を形成し、前記押出機において前記乳化混合物を最初に希釈して25重量%を超える水を含有させ、前記押出機から前記乳化混合物を押し出した後に追加の水を含むように前記乳化混合物をさらに希釈して前記水性分散物を形成し、前記(A)少なくとも1つの熱可塑性ポリマーが、エチレンと、C 4 −C 20 直鎖、分岐または環状ジエン、ビニルアセテート、および式H 2 C=CHR(式中、RはC 1 −C 20 直鎖、分岐または環状アルキル基またはC 6 −C 20 アリール基である)によって表される化合物から成る群より選択される少なくとも1つのコモノマーとのインターポリマー、または、プロピレンと、C 2 あるいはC 4 −C 20 直鎖、分岐または環状ジエン、ビニルアセテート、および式H 2 C=CHR(式中、RはC 2 −C 20 直鎖、分岐または環状アルキル基またはC 6 −C 20 アリール基である)によって表される化合物から成る群より選択される少なくとも1つのコモノマーとのインターポリマーを含むステップと;
前記水性分散物を前記熱可塑性の基材の少なくとも1つの面に塗布するステップと;
前記水の少なくとも一部を除去するステップであって、コーティング層を形成するために、前記水性分散物の前記熱可塑性ポリマーのピーク融点より20℃高い温度〜前記熱可塑性の基材の軟化点より20℃低い温度にて前記水性分散物を乾燥するステップと;
それによって前記熱可塑性の基材を被覆するコーティング層を形成するステップと;
コーティングされた前記熱可塑性の基材を2軸延伸するステップと;
それによって前記コーティングされた基材を形成するステップと;
を含む方法。 - 前記2軸延伸された基材が、ポリエステル、ポリカーボネート、ポリアリーレート、ポリアミド、ポリイミド、ポリアミド−イミド、ポリエーテル−アミド、ポリエーテルイミド、ポリアリールエーテル、ポリアリールエーテルケトン、脂肪族ポリケトン、
、ポリスルホン、ポリスチレンおよびその誘導体、ポリアクリレート、ポリメタクリレート、セルロース誘導体、ポリエチレン、ポリオレフィン、主にオレフィンモノマーを有するコポリマー、フッ素化ポリマーおよびコポリマー、塩素化ポリマー、ポリアクリロニトリル、ポリビニルアセテート、ポリビニルアルコール、ポリエーテル、アイオノマー樹脂、エラストマー、シリコーン樹脂、エポキシ樹脂、ポリウレタン、混和性または非混和性ポ
リマー混合物、又は上述のポリマーのいずれかの構成モノマーのいずれかのコポリマーを含む、請求項15に記載の方法。 - 前記2軸延伸された基材が2軸配向ポリプロピレン、2軸配向ポリアミド、2軸配向ポリエステル、2軸配向ポリエチレン、および2軸配向ポリスチレンから成る群より選択される少なくとも1つを含む、請求項15に記載の方法。
- 前記少なくとも1つの熱可塑性ポリマーが、少なくとも60重量パーセントのプロピレン由来単位および少なくとも0.1重量パーセントのエチレン由来単位を含むプロピレン/エチレンコポリマーを含み、該コポリマーは、14.6ppmおよび15.7ppmにおけるレジオエラーに相当する13C NMRピークであって、等しい強度のピークを有し、前記ピークは、成長コポリマー鎖へのプロピレン単位の立体選択性2,1−挿入エラーの結果であることを特徴とする、請求項15から17のいずれかに記載の方法。
- 前記熱可塑性ポリマーが0.85〜0.90g/ccの密度を有する、請求項15に記載の方法。
- 前記コーティングされた基材が、他の層をさらに含む、請求項15から19のいずれかに記載の方法。
- 前記分散物が2ミクロン未満の平均体積粒径を有する、請求項15に記載の方法。
- 前記分散物が1ミクロン未満の平均体積粒径を有する、請求項21に記載の方法。
- 前記コーティング層が乾燥後に0.5〜75ミクロンの範囲の厚さを有する、請求項15から22のいずれかに記載の方法。
- 前記コーティング層が乾燥後に0.5〜25ミクロンの範囲の厚さを有する、請求項23に記載の方法。
- 前記コーティング層が乾燥後に0.75〜2ミクロンの範囲の厚さを有する、請求項24に記載の方法。
- 前記コーティング層をヒートシール開始温度まで加熱するステップをさらに含む、請求項15から25のいずれかに記載の方法。
- 前記ヒートシール開始温度が80℃未満である、請求項26に記載の方法。
- 前記ヒートシール開始温度が70℃未満である、請求項27に記載の方法。
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US10/925,693 US7803865B2 (en) | 2003-08-25 | 2004-08-25 | Aqueous dispersion, its production method, and its use |
US10/925,693 | 2004-08-25 | ||
PCT/US2005/006493 WO2005085331A1 (en) | 2004-02-27 | 2005-02-28 | Aqueous polymer dispersions and products from those dispersions |
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US8357749B2 (en) * | 2003-08-25 | 2013-01-22 | Dow Global Technologies Llc | Coating composition and articles made therefrom |
US8349929B2 (en) * | 2003-08-25 | 2013-01-08 | Dow Global Technologies Llc | Coating composition and articles made therefrom |
US7763676B2 (en) * | 2003-08-25 | 2010-07-27 | Dow Global Technologies Inc. | Aqueous polymer dispersions and products from those dispersions |
US8779053B2 (en) | 2003-08-25 | 2014-07-15 | Dow Global Technologies Llc | Coating compositions |
US8158711B2 (en) * | 2003-08-25 | 2012-04-17 | Dow Global Technologies Llc | Aqueous dispersion, its production method, and its use |
US9169406B2 (en) | 2003-08-25 | 2015-10-27 | Dow Global Technologies Llc | Coating compositions |
US8722787B2 (en) | 2003-08-25 | 2014-05-13 | Dow Global Technologies Llc | Coating composition and articles made therefrom |
EP1834981B1 (en) * | 2004-11-12 | 2011-09-21 | Toray Industries, Inc. | Biaxially oriented polyarylene sulfide film and laminated polyarylene sulfide sheets comprising the same |
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