JP4642328B2 - モノマー含有量の少ないｔｄｉ三量体の製造方法 - Google Patents

モノマー含有量の少ないｔｄｉ三量体の製造方法 Download PDF

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Publication number
JP4642328B2
JP4642328B2 JP2003190279A JP2003190279A JP4642328B2 JP 4642328 B2 JP4642328 B2 JP 4642328B2 JP 2003190279 A JP2003190279 A JP 2003190279A JP 2003190279 A JP2003190279 A JP 2003190279A JP 4642328 B2 JP4642328 B2 JP 4642328B2
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JP
Japan
Prior art keywords
catalyst
tdi
mixture
diisocyanate
diisocyanatotoluene
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Expired - Lifetime
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JP2003190279A
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Japanese (ja)
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JP2004250429A (ja
JP2004250429A5 (enExample
Inventor
マルティン・ブラーム
ヨアヒム・ジモン
オスヴァルト・ヴィルメス
ユルゲン・ヴァロシェク
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Bayer AG
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Bayer AG
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Publication of JP2004250429A5 publication Critical patent/JP2004250429A5/ja
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
    • C08G18/78—Nitrogen
    • C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
    • C08G18/791—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups
    • C08G18/794—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups formed by oligomerisation of aromatic isocyanates or isothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/02—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only
    • C08G18/022—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only the polymeric products containing isocyanurate groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/1841—Catalysts containing secondary or tertiary amines or salts thereof having carbonyl groups which may be linked to one or more nitrogen or oxygen atoms

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2003190279A 2002-07-03 2003-07-02 モノマー含有量の少ないｔｄｉ三量体の製造方法 Expired - Lifetime JP4642328B2 (ja)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10229780A DE10229780A1 (de) 2002-07-03 2002-07-03 Verfahren zur Herstellung monomerenarmer TDI-Trimerisate

Publications (3)

Publication Number Publication Date
JP2004250429A JP2004250429A (ja) 2004-09-09
JP2004250429A5 JP2004250429A5 (enExample) 2006-08-03
JP4642328B2 true JP4642328B2 (ja) 2011-03-02

Family

ID=29719443

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JP2003190279A Expired - Lifetime JP4642328B2 (ja) 2002-07-03 2003-07-02 モノマー含有量の少ないｔｄｉ三量体の製造方法

Country Status (9)

Country Link
US (1) US6936678B2 (enExample)
EP (1) EP1378529B1 (enExample)
JP (1) JP4642328B2 (enExample)
KR (1) KR101010847B1 (enExample)
CN (1) CN1307164C (enExample)
AT (1) ATE321798T1 (enExample)
BR (1) BR0302380B1 (enExample)
DE (2) DE10229780A1 (enExample)
ES (1) ES2261822T3 (enExample)

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CN100439414C (zh) * 2006-09-30 2008-12-03 北京展辰化工有限公司 低游离tdi聚氨酯固化剂的制造方法、制得的固化剂及其制品
DE102007034977A1 (de) * 2007-07-26 2009-01-29 Lanxess Deutschland Gmbh Phthalatfreie Isocyanuratzubereitungen
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EP2354172B1 (de) 2010-02-08 2012-11-21 LANXESS Deutschland GmbH Phthalatfreie Isocyanuratzubereitungen
CN101880516B (zh) * 2010-07-05 2013-01-30 广东多正化工科技有限公司 低游离mdi单体双组份无溶剂聚氨酯胶粘剂
DE102010033061A1 (de) 2010-08-02 2012-02-02 Bayer Materialscience Ag Phthalatfreie Isocyanuratzubereitung
CN102911343B (zh) * 2012-10-24 2014-12-31 华南理工大学 一种甲苯二异氰酸酯三聚体固化剂的制备方法
WO2014139879A1 (de) * 2013-03-12 2014-09-18 Bayer Materialscience Ag Verfahren zur herstellung von tdi-trimerisaten mit besonderer reinheit
CN105131249A (zh) * 2015-09-17 2015-12-09 广东聚盈化工有限公司 一种高容忍度低游离tdi三聚体及制备方法
CN105906784A (zh) * 2016-05-10 2016-08-31 华南理工大学 一种无毒级亚光tdi三聚体固化剂及其制备方法
WO2018076198A1 (en) * 2016-10-26 2018-05-03 Covestro Deutschland Ag Tdi based polyisocyanate mixture with a high solids content
WO2018076199A1 (en) * 2016-10-26 2018-05-03 Covestro Deutschland Ag Tdi based low-viscosity polyisocyanates with isocyanurate groups
CN108499606B (zh) * 2017-02-24 2020-11-20 万华化学集团股份有限公司 一种邻巯基芳基氮杂环卡宾金属配合物催化剂及其制备方法和用途
WO2019007895A1 (de) 2017-07-05 2019-01-10 Covestro Deutschland Ag Kontinuierliche verdünnung von polyisocyanaten
EP3424910A1 (de) 2017-07-05 2019-01-09 Covestro Deutschland AG Kontinuierliche verdünnung von polyisocyanaten
EP3450476A1 (de) 2017-08-31 2019-03-06 Evonik Degussa GmbH Reaktivklebstoffe mit niedrigem gehalt an monomerem diisocyanat
EP3599255A1 (en) 2018-07-23 2020-01-29 Covestro Deutschland AG Ionically hydrophilized polyisocyanates with improved drying
ES2913002T3 (es) 2018-07-20 2022-05-30 Covestro Intellectual Property Gmbh & Co Kg Poliisocianatos iónicamente hidrofilizados con secado mejorado
EP3750934A1 (en) 2019-06-12 2020-12-16 Covestro Deutschland AG Method for the production of isocyanate-group terminated polyoxazolidinones
EP3750933A1 (en) 2019-06-12 2020-12-16 Covestro Deutschland AG Method for the production of epoxy-group terminated polyoxazolidinones
EP3760658A1 (de) 2019-07-03 2021-01-06 Covestro Deutschland AG Beständige 2k-pur-beschichtungen
CN110790880B (zh) * 2019-11-15 2021-07-23 万华化学集团股份有限公司 一种tdi三聚体的制备方法及含溶剂的tdi三聚体和其用途
WO2021165125A1 (de) 2020-02-17 2021-08-26 Covestro Deutschland Ag Polyisocyanatzubereitungen
EP3885387A1 (de) 2020-03-25 2021-09-29 Covestro Deutschland AG Polyisocyanat-basierte polyadditionsverbindungen mit fünfgliedrigen cyclischen iminoether-strukturelementen
EP3916031A1 (de) 2020-05-28 2021-12-01 LANXESS Deutschland GmbH Neue phthalatfreie isocyanurat-zusammensetzung und deren verwendung
EP4259676A1 (en) 2020-12-10 2023-10-18 Covestro Deutschland AG Composition comprising epoxy-functional oxazolidinone
EP4011927A1 (en) 2020-12-10 2022-06-15 Covestro Deutschland AG Composition comprising epoxy-functional oxazolidinone
EP3909994A1 (de) 2021-02-18 2021-11-17 LANXESS Deutschland GmbH Neue phthalatfreie isocyanurat-zusammensetzung
EP4083100A1 (en) 2021-04-26 2022-11-02 Covestro Deutschland AG Method for the production of an isocyanate-group terminated polyoxazolidinone composition
US20240199787A1 (en) 2021-04-26 2024-06-20 Covestro Deutschland Ag Method for the production of an isocyanate-group terminated polyoxazolidinone composition
EP4105251A1 (de) 2021-06-18 2022-12-21 Covestro Deutschland AG Vernetzbare zusammensetzungen, enthaltend imin- und/oder aminal-bildende komponenten
WO2022263306A1 (de) 2021-06-18 2022-12-22 Covestro Deutschland Ag Organische polyisocyanate mit aldehydblockierung
EP4108694A1 (de) 2021-06-21 2022-12-28 Covestro Deutschland AG Beschichtungsmittel und daraus erhältliche beschichtungen mit verbesserten anschmutzungsresistenzen und (selbst-)reinigungseigenschaften
EP4108695A1 (de) 2021-06-21 2022-12-28 Covestro Deutschland AG Beschichtungsmittel und daraus erhältliche beschichtungen mit verbesserten anschmutzungsresistenzen und (selbst-)reinigungseigenschaften
CN113667080B (zh) * 2021-07-01 2022-06-14 华南理工大学 一种hdi-tdi混合多聚体固化剂及其制备方法
EP4198094A1 (de) 2021-12-20 2023-06-21 Covestro Deutschland AG Mehrschichtaufbau auf metallischen untergründen basierend auf polyaspartatbeschichtungen
EP4234600A1 (en) 2022-02-25 2023-08-30 Covestro Deutschland AG Polyisocyanate and process for preparing the same
CN114805740B (zh) * 2022-03-11 2024-04-30 江西五行材料科技有限公司 一种无溶剂tdi三聚体聚氨酯丙烯酸酯及其制备方法
EP4265663A1 (de) 2022-04-21 2023-10-25 Covestro Deutschland AG Polyaspartat-basierte zweikomponenten-beschichtungszusammensetzungen zur herstellung von beschichtungen mit guten selbstheilungseigenschaften bei gleichzeitig geringer klebrigkeit
EP4279522A1 (de) 2022-05-17 2023-11-22 Covestro Deutschland AG In wasser dispergierbare polyisocyanate mit aldehydblockierung und daraus erhältliche wässrige zusammensetzungen
WO2024260926A1 (en) 2023-06-22 2024-12-26 Covestro Deutschland Ag Method for the production of a hydroxyl-group terminated oxazolidinone composition
EP4574860A1 (en) 2023-12-19 2025-06-25 Covestro Deutschland AG Use of a solvent-free composition comprising epoxy-functional oxazolidinones for producing adhesives, sealing compounds, potting compounds, composites, such as fiber composite materials, or moldings, or for producing coatings on mineral, metallic or plastic substrates, and the products thus obtained
WO2025131813A1 (de) 2023-12-20 2025-06-26 Lanxess Deutschland Gmbh Neue phthalatfreie isocyanurat-zusammensetzung und deren verwendung

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Also Published As

Publication number Publication date
CN1307164C (zh) 2007-03-28
ES2261822T3 (es) 2006-11-16
DE10229780A1 (de) 2004-01-15
HK1062560A1 (en) 2004-11-12
BR0302380A (pt) 2004-08-24
KR20040004130A (ko) 2004-01-13
JP2004250429A (ja) 2004-09-09
CN1470509A (zh) 2004-01-28
KR101010847B1 (ko) 2011-01-26
US20040024213A1 (en) 2004-02-05
EP1378529A1 (de) 2004-01-07
DE50302784D1 (de) 2006-05-18
EP1378529B1 (de) 2006-03-29
BR0302380B1 (pt) 2012-09-18
US6936678B2 (en) 2005-08-30
ATE321798T1 (de) 2006-04-15

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