JP3899418B2 - 担持ゼオライト膜の生成方法および得られた膜 - Google Patents

担持ゼオライト膜の生成方法および得られた膜 Download PDF

Info

Publication number
JP3899418B2
JP3899418B2 JP32720996A JP32720996A JP3899418B2 JP 3899418 B2 JP3899418 B2 JP 3899418B2 JP 32720996 A JP32720996 A JP 32720996A JP 32720996 A JP32720996 A JP 32720996A JP 3899418 B2 JP3899418 B2 JP 3899418B2
Authority
JP
Japan
Prior art keywords
oxide
gel
zeolite
liquid
carrier
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP32720996A
Other languages
English (en)
Japanese (ja)
Other versions
JPH09173799A (ja
JPH09173799A5 (enExample
Inventor
アーンステット マルチン
ル ドレド ロナン
ルイ グット ジャン
メチヴィエ アラン
ストレシェール クリスチャン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies nouvelles
Original Assignee
IFP Energies nouvelles
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IFP Energies nouvelles filed Critical IFP Energies nouvelles
Publication of JPH09173799A publication Critical patent/JPH09173799A/ja
Publication of JPH09173799A5 publication Critical patent/JPH09173799A5/ja
Application granted granted Critical
Publication of JP3899418B2 publication Critical patent/JP3899418B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0048—Inorganic membrane manufacture by sol-gel transition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0051—Inorganic membrane manufacture by controlled crystallisation, e,.g. hydrothermal growth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0081—After-treatment of organic or inorganic membranes
    • B01D67/0083—Thermal after-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/10—Supported membranes; Membrane supports
    • B01D69/105—Support pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/12—Composite membranes; Ultra-thin membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B01D71/028—Molecular sieves
    • B01D71/0281—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B01J20/183—Physical conditioning without chemical treatment, e.g. drying, granulating, coating, irradiation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0246—Coatings comprising a zeolite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/08—Specific temperatures applied
    • B01D2323/081—Heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/46—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/60—Synthesis on support
    • B01J2229/64—Synthesis on support in or on refractory materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S95/00—Gas separation: processes
    • Y10S95/90—Solid sorbent
    • Y10S95/902—Molecular sieve

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Thermal Sciences (AREA)
  • Materials Engineering (AREA)
  • Geology (AREA)
  • Analytical Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
JP32720996A 1995-12-08 1996-12-06 担持ゼオライト膜の生成方法および得られた膜 Expired - Fee Related JP3899418B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9514563A FR2742070B1 (fr) 1995-12-08 1995-12-08 Procede d'elaboration controlee de membranes de zeolithe supportee
FR9514563 1995-12-08

Publications (3)

Publication Number Publication Date
JPH09173799A JPH09173799A (ja) 1997-07-08
JPH09173799A5 JPH09173799A5 (enExample) 2004-11-25
JP3899418B2 true JP3899418B2 (ja) 2007-03-28

Family

ID=9485300

Family Applications (1)

Application Number Title Priority Date Filing Date
JP32720996A Expired - Fee Related JP3899418B2 (ja) 1995-12-08 1996-12-06 担持ゼオライト膜の生成方法および得られた膜

Country Status (5)

Country Link
US (1) US6140263A (enExample)
EP (1) EP0778076B1 (enExample)
JP (1) JP3899418B2 (enExample)
DE (1) DE69630570T2 (enExample)
FR (1) FR2742070B1 (enExample)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19624862A1 (de) * 1996-06-21 1998-01-02 Basf Ag Mesoporöse Oxidformkörper
DE19741498B4 (de) * 1997-09-20 2008-07-03 Evonik Degussa Gmbh Herstellung eines Keramik-Edelstahlgewebe-Verbundes
GR1003047B (el) * 1997-12-24 1999-01-14 Μεθοδος για αυξηση των πορων ανοργανων σωματιδιων με χρηση ανοργανων προδρομων ουσιων, επιφανειοδραστικων και λιποφιλων οργανικων ενωσεων χαμηλης πτητικοτητας
AU754663B2 (en) * 1998-10-20 2002-11-21 Ngk Insulators, Ltd. Zeolite composite film and process for producing the same
FR2786710B1 (fr) * 1998-12-04 2001-11-16 Ceramiques Tech Soc D Membrane comprenant un support poreux et une couche d'un tamis modeculaire et son procede de preparation
US6767384B1 (en) * 2000-01-21 2004-07-27 The Regents Of The University Of Colorado Isomorphously substituted molecular sieve membranes
EP1232999B1 (en) 2000-03-02 2018-07-25 NGK Insulators, Ltd. Zeolite formed product, zeolite laminate intermediate, zeolite laminate composite and method for their preparation
AU2003248380B2 (en) * 2000-03-02 2006-06-29 Ngk Insulators, Ltd Porous zeolite shaped body
JP4531997B2 (ja) * 2001-02-16 2010-08-25 日本碍子株式会社 ゼオライト成形体、ゼオライト積層中間体、ゼオライト積層複合体及びそれらの製造方法
US6500490B1 (en) * 2000-03-23 2002-12-31 Honeywell International Inc. Hydrophilic zeolite coating
JP3871501B2 (ja) * 2000-08-07 2007-01-24 株式会社ノリタケカンパニーリミテド ゼオライト膜とその製造方法と膜リアクター
US6340433B1 (en) * 2000-09-15 2002-01-22 Engelhard Corporation Water purification using titanium silicate membranes
US6942784B2 (en) * 2000-09-22 2005-09-13 Engelhard Corporation Structurally enhanced cracking catalysts
JP4855582B2 (ja) * 2001-02-09 2012-01-18 日本碍子株式会社 メソポーラスシリカ、メソポーラスシリカ複合体及びそれらの製造方法
DE10107539A1 (de) * 2001-02-17 2002-09-05 Aaflowsystems Gmbh & Co Kg Filterkörper
KR20030026515A (ko) * 2001-09-26 2003-04-03 주식회사 신성이엔지 제올라이트를 이용한 기체 분리 장치
DE10208276A1 (de) * 2002-02-26 2003-09-04 Creavis Tech & Innovation Gmbh Compositmembran, Verfahren zu deren Herstellung und die Verwendung der Membran
US6818333B2 (en) * 2002-06-03 2004-11-16 Institut Francais Du Petrole Thin zeolite membrane, its preparation and its use in separation
FR2840236B1 (fr) * 2002-06-03 2005-02-04 Inst Francais Du Petrole Membrane zeolithique de faible epaisseur, sa preparation et son utilisation en separation
US7476635B2 (en) * 2002-06-03 2009-01-13 Institut Francais Du Petrole Process for making supported thin zeolite membrane
FR2850588B1 (fr) * 2003-01-31 2007-08-03 Inst Francais Du Petrole Membrane inorganique poreuse contenant du carbone, son procede de preparation et son utilisation
JP4795626B2 (ja) * 2003-03-04 2011-10-19 紀夫 寺前 多孔体膜並びに薄膜の作製方法
JP3922389B2 (ja) 2003-08-06 2007-05-30 株式会社物産ナノテク研究所 ゼオライト膜の製造方法及び製造装置、並びにこの方法により得られたゼオライト管状分離膜
US7316727B2 (en) * 2004-03-19 2008-01-08 The Regents Of The University Of Colorado High-selectivity supported SAPO membranes
CA2573685A1 (en) 2004-08-03 2006-02-16 The Regents Of The University Of Colorado, A Body Corporate Membranes for highly selective separations
WO2007081212A1 (en) * 2006-01-16 2007-07-19 Stichting Energieonderzoek Centrum Nederland Microporous molecular separation membrane with high hydrothermal stability
CN101443298A (zh) * 2006-05-15 2009-05-27 科罗拉多州立大学董事会 用于co2/ch4分离的高通量和高选择性的sapo-34膜
EP2032239B1 (de) * 2006-06-13 2014-03-19 Basf Se Verfahren zur herstellung einer komposit-membran sowie verwendungen
US7811359B2 (en) * 2007-01-18 2010-10-12 General Electric Company Composite membrane for separation of carbon dioxide
US8302782B2 (en) * 2007-03-09 2012-11-06 The Regents of the University of Colorado, a body corporated Synthesis of zeolites and zeolite membranes using multiple structure directing agents
JP5481075B2 (ja) * 2009-02-04 2014-04-23 日本碍子株式会社 ゼオライト膜の製造方法
DE102010009542A1 (de) 2010-02-26 2011-09-01 Dbi - Gastechnologisches Institut Ggmbh Freiberg Verfahren zur Abtrennung von Erdgas- oder Erdölbegleitgaskomponenten an anorganisch porösen Membranen
US8679227B2 (en) 2010-04-29 2014-03-25 The Regents Of The University Of Colorado High flux SAPO-34 membranes for CO2/CH4 separation and template removal method
WO2014130998A1 (en) * 2013-02-25 2014-08-28 Spinnaker Biosciences, Inc. Surface functionalized porous silicon
JP5901817B2 (ja) * 2015-04-06 2016-04-13 日揮触媒化成株式会社 重質炭化水素油の接触分解、水素化分解触媒用ヘテロ接合多孔性結晶体
CN112999890B (zh) * 2021-03-03 2022-04-19 大连理工大学 一种平板有机无机杂化SiO2复合膜及其制备方法和应用

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4310440A (en) * 1980-07-07 1982-01-12 Union Carbide Corporation Crystalline metallophosphate compositions
JPS6028826A (ja) * 1983-07-26 1985-02-14 Hiroshi Suzuki かご型ゼオライト薄膜表層を有する複合膜及びその製造法
GB8609249D0 (en) * 1986-04-16 1986-05-21 Alcan Int Ltd Anodic oxide membrane catalyst support
US5374411A (en) * 1987-08-28 1994-12-20 The Dow Chemical Company Crystalline aluminumphosphate compositions
US4861743A (en) * 1987-11-25 1989-08-29 Uop Process for the production of molecular sieves
US5109263A (en) * 1989-07-28 1992-04-28 Hitachi, Ltd. Semiconductor device with optimal distance between emitter and trench isolation
US5100596A (en) 1990-06-05 1992-03-31 Mobil Oil Corp. Synthesis of membrane composed of a pure molecular sieve
GB9022836D0 (en) * 1990-10-19 1990-12-05 British Petroleum Co Plc Membranes
NL9100217A (nl) * 1991-02-07 1992-09-01 Univ Delft Tech Moleculaire-zeefkristallen bevattend anorganisch composietmembraan.
JPH05105420A (ja) * 1991-03-29 1993-04-27 Ngk Insulators Ltd ゼオライト結晶体の合成膜およびその製造方法
US5183482A (en) * 1991-06-19 1993-02-02 Texaco Inc. Separation by membrane techniques
DE4131447A1 (de) * 1991-09-21 1993-03-25 Basf Ag Farbige, kristalline alumophosphate und/oder silicoalumophosphate vom ael-typ
US5258339A (en) * 1992-03-12 1993-11-02 Worcester Polytechnic Institute Formation of zeolite membranes from sols
GB9206783D0 (en) * 1992-03-27 1992-05-13 British Petroleum Co Plc Deposition process
DE69207596T2 (de) * 1992-09-07 1996-07-04 Shell Int Research Herstellung einer keramischen Membran
EP0695216B1 (en) * 1993-04-23 1998-07-22 Exxon Chemical Patents Inc. Layers containing crystalline molecular sieves and processes for their manufacture
US5464798A (en) * 1994-02-24 1995-11-07 Jia; Meng-Dong Ceramic-zeolite composite membranes and use for separation of vapor/gas mixtures

Also Published As

Publication number Publication date
DE69630570T2 (de) 2004-05-13
JPH09173799A (ja) 1997-07-08
FR2742070B1 (fr) 1998-01-09
EP0778076A1 (fr) 1997-06-11
DE69630570D1 (de) 2003-12-11
FR2742070A1 (fr) 1997-06-13
US6140263A (en) 2000-10-31
EP0778076B1 (fr) 2003-11-05

Similar Documents

Publication Publication Date Title
US6140263A (en) Process for the production of supported zeolite membranes, and zeolite membranes so produced
Bein Synthesis and applications of molecular sieve layers and membranes
US5567664A (en) Supported zeo-type membrane
EP0460512B2 (en) Membrane formed of crystalline molecular sieve material
EP0808655B1 (en) Molecular sieve layers and processes for their manufacture
US10682626B2 (en) Method for producing a crystalline film of zeolite and/or zeolite like crystals on a porous substrate
US6387269B1 (en) Membrane for separating fluids
JP3723888B2 (ja) ガラス質細孔による担持ゼオライト膜の生成方法及 び得られたゼオライト膜
WO1993017781A1 (en) Formation of zeolite membranes from sols
CA2346983C (en) Zeolite composite film and process for producing the same
JP4759724B2 (ja) ゼオライト膜及びその製造方法
CN104583220A (zh) 用于晶体生长、仅诱导从硅沸石-1或沸石β晶种表面的二次生长的合成凝胶
GB2287459A (en) Porous amorphous silica-alumina
JP2001031416A (ja) ゼオライト膜の製造方法、mfi型ゼオライト膜および分子を分離する方法
US20030228969A1 (en) Method for synthesizing zeolite membranes
CN1307096C (zh) 沸石成型体的制备方法和沸石层压复合体的制备方法
JP2003088734A (ja) ゼオライト積層複合体及びそれを用いたゼオライトメンブレンリアクタ
JP4348431B2 (ja) 高シリカ型cds−1ゼオライト膜及びその製造方法
JP2002058973A (ja) マイクロ波を用いたzsm−5膜の製造方法
AU9416798A (en) Molecular sieve layers and processes for their manufacture

Legal Events

Date Code Title Description
A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20051110

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20051122

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20060216

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20060718

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20061013

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20061114

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20061211

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110112

Year of fee payment: 4

LAPS Cancellation because of no payment of annual fees