DE69630570T2 - Verfahren zur Herstellung von gestützten Membranen - Google Patents

Verfahren zur Herstellung von gestützten Membranen Download PDF

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Publication number
DE69630570T2
DE69630570T2 DE69630570T DE69630570T DE69630570T2 DE 69630570 T2 DE69630570 T2 DE 69630570T2 DE 69630570 T DE69630570 T DE 69630570T DE 69630570 T DE69630570 T DE 69630570T DE 69630570 T2 DE69630570 T2 DE 69630570T2
Authority
DE
Germany
Prior art keywords
oxide
gel
zeolite
membrane
carrier
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69630570T
Other languages
German (de)
English (en)
Other versions
DE69630570D1 (de
Inventor
Martine Anstett
Ronan Le Dred
Jean-Louis Guth
Alain Methivier
Christian Streicher
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies nouvelles
Original Assignee
IFP Energies nouvelles
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IFP Energies nouvelles filed Critical IFP Energies nouvelles
Application granted granted Critical
Publication of DE69630570D1 publication Critical patent/DE69630570D1/de
Publication of DE69630570T2 publication Critical patent/DE69630570T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0048—Inorganic membrane manufacture by sol-gel transition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0051—Inorganic membrane manufacture by controlled crystallisation, e,.g. hydrothermal growth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0081—After-treatment of organic or inorganic membranes
    • B01D67/0083—Thermal after-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/10—Supported membranes; Membrane supports
    • B01D69/105—Support pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/12—Composite membranes; Ultra-thin membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B01D71/028—Molecular sieves
    • B01D71/0281—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B01J20/183—Physical conditioning without chemical treatment, e.g. drying, granulating, coating, irradiation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0246—Coatings comprising a zeolite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/08—Specific temperatures applied
    • B01D2323/081—Heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/46—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/60—Synthesis on support
    • B01J2229/64—Synthesis on support in or on refractory materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S95/00—Gas separation: processes
    • Y10S95/90—Solid sorbent
    • Y10S95/902—Molecular sieve

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Thermal Sciences (AREA)
  • Materials Engineering (AREA)
  • Geology (AREA)
  • Analytical Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
DE69630570T 1995-12-08 1996-11-29 Verfahren zur Herstellung von gestützten Membranen Expired - Lifetime DE69630570T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9514563A FR2742070B1 (fr) 1995-12-08 1995-12-08 Procede d'elaboration controlee de membranes de zeolithe supportee
FR9514563 1995-12-08

Publications (2)

Publication Number Publication Date
DE69630570D1 DE69630570D1 (de) 2003-12-11
DE69630570T2 true DE69630570T2 (de) 2004-05-13

Family

ID=9485300

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69630570T Expired - Lifetime DE69630570T2 (de) 1995-12-08 1996-11-29 Verfahren zur Herstellung von gestützten Membranen

Country Status (5)

Country Link
US (1) US6140263A (enExample)
EP (1) EP0778076B1 (enExample)
JP (1) JP3899418B2 (enExample)
DE (1) DE69630570T2 (enExample)
FR (1) FR2742070B1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010009542A1 (de) 2010-02-26 2011-09-01 Dbi - Gastechnologisches Institut Ggmbh Freiberg Verfahren zur Abtrennung von Erdgas- oder Erdölbegleitgaskomponenten an anorganisch porösen Membranen

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DE19624862A1 (de) * 1996-06-21 1998-01-02 Basf Ag Mesoporöse Oxidformkörper
DE19741498B4 (de) * 1997-09-20 2008-07-03 Evonik Degussa Gmbh Herstellung eines Keramik-Edelstahlgewebe-Verbundes
GR1003047B (el) * 1997-12-24 1999-01-14 Μεθοδος για αυξηση των πορων ανοργανων σωματιδιων με χρηση ανοργανων προδρομων ουσιων, επιφανειοδραστικων και λιποφιλων οργανικων ενωσεων χαμηλης πτητικοτητας
AU754663B2 (en) * 1998-10-20 2002-11-21 Ngk Insulators, Ltd. Zeolite composite film and process for producing the same
FR2786710B1 (fr) * 1998-12-04 2001-11-16 Ceramiques Tech Soc D Membrane comprenant un support poreux et une couche d'un tamis modeculaire et son procede de preparation
US6767384B1 (en) * 2000-01-21 2004-07-27 The Regents Of The University Of Colorado Isomorphously substituted molecular sieve membranes
EP1232999B1 (en) 2000-03-02 2018-07-25 NGK Insulators, Ltd. Zeolite formed product, zeolite laminate intermediate, zeolite laminate composite and method for their preparation
AU2003248380B2 (en) * 2000-03-02 2006-06-29 Ngk Insulators, Ltd Porous zeolite shaped body
JP4531997B2 (ja) * 2001-02-16 2010-08-25 日本碍子株式会社 ゼオライト成形体、ゼオライト積層中間体、ゼオライト積層複合体及びそれらの製造方法
US6500490B1 (en) * 2000-03-23 2002-12-31 Honeywell International Inc. Hydrophilic zeolite coating
JP3871501B2 (ja) * 2000-08-07 2007-01-24 株式会社ノリタケカンパニーリミテド ゼオライト膜とその製造方法と膜リアクター
US6340433B1 (en) * 2000-09-15 2002-01-22 Engelhard Corporation Water purification using titanium silicate membranes
US6942784B2 (en) * 2000-09-22 2005-09-13 Engelhard Corporation Structurally enhanced cracking catalysts
JP4855582B2 (ja) * 2001-02-09 2012-01-18 日本碍子株式会社 メソポーラスシリカ、メソポーラスシリカ複合体及びそれらの製造方法
DE10107539A1 (de) * 2001-02-17 2002-09-05 Aaflowsystems Gmbh & Co Kg Filterkörper
KR20030026515A (ko) * 2001-09-26 2003-04-03 주식회사 신성이엔지 제올라이트를 이용한 기체 분리 장치
DE10208276A1 (de) * 2002-02-26 2003-09-04 Creavis Tech & Innovation Gmbh Compositmembran, Verfahren zu deren Herstellung und die Verwendung der Membran
US6818333B2 (en) * 2002-06-03 2004-11-16 Institut Francais Du Petrole Thin zeolite membrane, its preparation and its use in separation
FR2840236B1 (fr) * 2002-06-03 2005-02-04 Inst Francais Du Petrole Membrane zeolithique de faible epaisseur, sa preparation et son utilisation en separation
US7476635B2 (en) * 2002-06-03 2009-01-13 Institut Francais Du Petrole Process for making supported thin zeolite membrane
FR2850588B1 (fr) * 2003-01-31 2007-08-03 Inst Francais Du Petrole Membrane inorganique poreuse contenant du carbone, son procede de preparation et son utilisation
JP4795626B2 (ja) * 2003-03-04 2011-10-19 紀夫 寺前 多孔体膜並びに薄膜の作製方法
JP3922389B2 (ja) 2003-08-06 2007-05-30 株式会社物産ナノテク研究所 ゼオライト膜の製造方法及び製造装置、並びにこの方法により得られたゼオライト管状分離膜
US7316727B2 (en) * 2004-03-19 2008-01-08 The Regents Of The University Of Colorado High-selectivity supported SAPO membranes
CA2573685A1 (en) 2004-08-03 2006-02-16 The Regents Of The University Of Colorado, A Body Corporate Membranes for highly selective separations
WO2007081212A1 (en) * 2006-01-16 2007-07-19 Stichting Energieonderzoek Centrum Nederland Microporous molecular separation membrane with high hydrothermal stability
CN101443298A (zh) * 2006-05-15 2009-05-27 科罗拉多州立大学董事会 用于co2/ch4分离的高通量和高选择性的sapo-34膜
EP2032239B1 (de) * 2006-06-13 2014-03-19 Basf Se Verfahren zur herstellung einer komposit-membran sowie verwendungen
US7811359B2 (en) * 2007-01-18 2010-10-12 General Electric Company Composite membrane for separation of carbon dioxide
US8302782B2 (en) * 2007-03-09 2012-11-06 The Regents of the University of Colorado, a body corporated Synthesis of zeolites and zeolite membranes using multiple structure directing agents
JP5481075B2 (ja) * 2009-02-04 2014-04-23 日本碍子株式会社 ゼオライト膜の製造方法
US8679227B2 (en) 2010-04-29 2014-03-25 The Regents Of The University Of Colorado High flux SAPO-34 membranes for CO2/CH4 separation and template removal method
WO2014130998A1 (en) * 2013-02-25 2014-08-28 Spinnaker Biosciences, Inc. Surface functionalized porous silicon
JP5901817B2 (ja) * 2015-04-06 2016-04-13 日揮触媒化成株式会社 重質炭化水素油の接触分解、水素化分解触媒用ヘテロ接合多孔性結晶体
CN112999890B (zh) * 2021-03-03 2022-04-19 大连理工大学 一种平板有机无机杂化SiO2复合膜及其制备方法和应用

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010009542A1 (de) 2010-02-26 2011-09-01 Dbi - Gastechnologisches Institut Ggmbh Freiberg Verfahren zur Abtrennung von Erdgas- oder Erdölbegleitgaskomponenten an anorganisch porösen Membranen

Also Published As

Publication number Publication date
JPH09173799A (ja) 1997-07-08
FR2742070B1 (fr) 1998-01-09
EP0778076A1 (fr) 1997-06-11
DE69630570D1 (de) 2003-12-11
FR2742070A1 (fr) 1997-06-13
US6140263A (en) 2000-10-31
EP0778076B1 (fr) 2003-11-05
JP3899418B2 (ja) 2007-03-28

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: IFP ENERGIES NOUVELLES, RUEIL-MALMAISON, FR

8328 Change in the person/name/address of the agent

Representative=s name: VONNEMANN, KLOIBER & KOLLEGEN, 81667 MUENCHEN