JP2018504357A5 - - Google Patents
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- Publication number
- JP2018504357A5 JP2018504357A5 JP2017540166A JP2017540166A JP2018504357A5 JP 2018504357 A5 JP2018504357 A5 JP 2018504357A5 JP 2017540166 A JP2017540166 A JP 2017540166A JP 2017540166 A JP2017540166 A JP 2017540166A JP 2018504357 A5 JP2018504357 A5 JP 2018504357A5
- Authority
- JP
- Japan
- Prior art keywords
- mordenite zeolite
- zeolite according
- sda
- crystallite
- mordenite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910021536 Zeolite Inorganic materials 0.000 claims description 34
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 34
- 229910052680 mordenite Inorganic materials 0.000 claims description 34
- 239000010457 zeolite Substances 0.000 claims description 34
- 239000013078 crystal Substances 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 14
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 4
- 229910052783 alkali metal Inorganic materials 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 238000001354 calcination Methods 0.000 claims description 4
- 150000002894 organic compounds Chemical class 0.000 claims description 4
- 239000011148 porous material Substances 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 229910052710 silicon Inorganic materials 0.000 claims description 4
- 239000010703 silicon Substances 0.000 claims description 4
- 238000003786 synthesis reaction Methods 0.000 claims description 4
- HWCKGOZZJDHMNC-UHFFFAOYSA-M tetraethylammonium bromide Chemical group [Br-].CC[N+](CC)(CC)CC HWCKGOZZJDHMNC-UHFFFAOYSA-M 0.000 claims description 4
- 229940073455 tetraethylammonium hydroxide Drugs 0.000 claims description 4
- LRGJRHZIDJQFCL-UHFFFAOYSA-M tetraethylazanium;hydroxide Chemical compound [OH-].CC[N+](CC)(CC)CC LRGJRHZIDJQFCL-UHFFFAOYSA-M 0.000 claims description 4
- NIUZJTWSUGSWJI-UHFFFAOYSA-M triethyl(methyl)azanium;chloride Chemical compound [Cl-].CC[N+](C)(CC)CC NIUZJTWSUGSWJI-UHFFFAOYSA-M 0.000 claims description 4
- JAJRRCSBKZOLPA-UHFFFAOYSA-M triethyl(methyl)azanium;hydroxide Chemical compound [OH-].CC[N+](C)(CC)CC JAJRRCSBKZOLPA-UHFFFAOYSA-M 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000002441 X-ray diffraction Methods 0.000 claims description 2
- -1 alkali metal cations Chemical class 0.000 claims description 2
- 150000001340 alkali metals Chemical class 0.000 claims description 2
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims description 2
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 claims description 2
- 239000011260 aqueous acid Substances 0.000 claims description 2
- 239000003054 catalyst Substances 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 239000012084 conversion product Substances 0.000 claims description 2
- 238000002425 crystallisation Methods 0.000 claims description 2
- 230000008025 crystallization Effects 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 2
- 238000005342 ion exchange Methods 0.000 claims description 2
- 239000000377 silicon dioxide Substances 0.000 claims description 2
- 229910001388 sodium aluminate Inorganic materials 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 238000005554 pickling Methods 0.000 claims 1
- 238000012805 post-processing Methods 0.000 claims 1
- 238000010025 steaming Methods 0.000 claims 1
- 239000000463 material Substances 0.000 description 2
- 230000003466 anti-cipated effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201562111730P | 2015-02-04 | 2015-02-04 | |
| US62/111,730 | 2015-02-04 | ||
| EP15160258.8 | 2015-03-23 | ||
| EP15160258 | 2015-03-23 | ||
| PCT/US2016/014264 WO2016126431A1 (en) | 2015-02-04 | 2016-01-21 | Process for preparing a molecular sieve |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2018504357A JP2018504357A (ja) | 2018-02-15 |
| JP2018504357A5 true JP2018504357A5 (OSRAM) | 2018-12-27 |
| JP6724020B2 JP6724020B2 (ja) | 2020-07-15 |
Family
ID=55524427
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017540166A Active JP6724020B2 (ja) | 2015-02-04 | 2016-01-21 | 分子ふるいを調製するための方法 |
Country Status (11)
| Country | Link |
|---|---|
| US (2) | US10017394B2 (OSRAM) |
| EP (1) | EP3253713B1 (OSRAM) |
| JP (1) | JP6724020B2 (OSRAM) |
| KR (1) | KR102527695B1 (OSRAM) |
| CN (1) | CN107207269B (OSRAM) |
| CA (1) | CA2983038C (OSRAM) |
| ES (1) | ES2750826T3 (OSRAM) |
| RU (1) | RU2700052C2 (OSRAM) |
| SG (2) | SG11201705830RA (OSRAM) |
| WO (1) | WO2016126431A1 (OSRAM) |
| ZA (1) | ZA201704548B (OSRAM) |
Families Citing this family (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104276586B (zh) * | 2013-07-03 | 2016-10-05 | 中国石油大学(北京) | 一种丝光沸石的制备方法 |
| CA2983038C (en) * | 2015-02-04 | 2023-01-31 | Exxonmobil Chemical Patents Inc. | Process for preparing a molecular sieve |
| US10118165B2 (en) | 2015-02-04 | 2018-11-06 | Exxonmobil Chemical Patents Inc. | Catalyst compositions and use in heavy aromatics conversion processes |
| US10053403B2 (en) | 2015-02-04 | 2018-08-21 | Exxonmobil Chemical Patents Inc. | Catalyst compositions and their use in transalkylation of heavy aromatics to xylenes |
| WO2018071185A1 (en) | 2016-10-10 | 2018-04-19 | Exxonmobil Chemical Patents Inc. | Heavy aromatics to btx conversion process and dual bed catalyst systems used |
| WO2018071184A1 (en) | 2016-10-10 | 2018-04-19 | Exxonmobil Chemical Patents Inc. | Heavy aromatics to btx conversion process and catalyst compositions used |
| EA038140B1 (ru) * | 2016-12-09 | 2021-07-12 | Далянь Инститьют Оф Кемикал Физикс, Чайниз Академи Оф Сайенсез | Способ синтеза морденитовых молекулярных сит, продукт и его применение |
| ES2732235B2 (es) * | 2017-01-23 | 2020-10-05 | Compania Espanola De Petroleos S A U Cepsa | Catalizador de núcleo-corteza para reacciones de hidroisomerización de hidrocarburos lineales |
| WO2018140149A1 (en) | 2017-01-25 | 2018-08-02 | Exxonmobil Chemical Patents Inc. | Transalkylation process and catalyst composition used therein |
| WO2018160327A1 (en) | 2017-02-28 | 2018-09-07 | Exxonmobil Chemical Patents Inc. | Catalyst compositions and their use in aromatic alkylation processes |
| RU2769447C2 (ru) * | 2017-02-28 | 2022-03-31 | Эксонмобил Кемикэл Пейтентс Инк. | Каталитические композиции и их применение в способах алкилирования ароматических соединений |
| WO2018183012A1 (en) | 2017-03-29 | 2018-10-04 | Exxonmobil Chemical Patents Inc. | Methods for removing impurities from a hydrocarbon stream and their use in aromatic alkylation processes |
| WO2018183009A1 (en) | 2017-03-29 | 2018-10-04 | Exxonmobil Chemical Patents Inc. | Catalyst compositions and their use in aromatic alkylation processes |
| SG11201911593SA (en) * | 2017-07-27 | 2020-02-27 | Exxonmobil Res & Eng Co | Small crystal emm-17, its method of making and use |
| WO2019222371A1 (en) | 2018-05-16 | 2019-11-21 | University Of Houston System | Synthesis of mordenite using multiple organics |
| KR102685518B1 (ko) * | 2018-07-27 | 2024-07-17 | 에스케이이노베이션 주식회사 | 입자 균일도가 우수한 모데나이트 제올라이트 및 그 제조방법 |
| WO2020022868A1 (ko) * | 2018-07-27 | 2020-01-30 | 에스케이이노베이션 주식회사 | 입자 균일도가 우수한 모데나이트 제올라이트 및 그 제조방법 |
| KR101994765B1 (ko) * | 2018-09-21 | 2019-07-01 | 에스케이이노베이션 주식회사 | 계층화된 제올라이트 및 이의 제조방법 |
| KR102020445B1 (ko) * | 2018-09-21 | 2019-09-10 | 에스케이이노베이션 주식회사 | 입자 크기의 제어가 가능한 모데나이트 제올라이트의 제조방법 |
| CN112996597B (zh) * | 2018-10-30 | 2024-03-15 | 埃克森美孚化学专利公司 | 微孔分子筛催化剂的煅烧 |
| TWI749489B (zh) | 2019-03-29 | 2021-12-11 | 美商艾克頌美孚化學專利股份有限公司 | 用於轉化芳族化合物之觸媒及方法 |
| US12239964B2 (en) | 2019-03-29 | 2025-03-04 | ExxonMobil Engineering & Technology Company | Catalysts and processes for converting aromatics |
| US11820723B2 (en) | 2019-10-17 | 2023-11-21 | Exxonmobil Chemicals Patents Inc. | Production of alkylaromatic compounds |
| CN112850743B (zh) * | 2019-11-26 | 2023-01-13 | 中国科学院大连化学物理研究所 | 一种调控丝光沸石分子筛形貌的绿色合成方法 |
| EP4103513A1 (en) * | 2020-02-12 | 2022-12-21 | University of Houston System | Synthesis of finned zeolite crystals |
| US12410111B2 (en) * | 2020-04-17 | 2025-09-09 | Exxonmobil Chemical Patents Inc. | Processes for converting C8 aromatic hydrocarbons |
| WO2021218982A1 (zh) | 2020-04-28 | 2021-11-04 | 中国石油化工股份有限公司 | 加氢催化剂及其制备方法和应用 |
| US11590481B2 (en) | 2021-06-17 | 2023-02-28 | Exxonmobil Technology & Engineering Company | Heteroatom-doped zeolites for bifunctional catalytic applications |
| CN113751056B (zh) * | 2021-10-15 | 2022-07-26 | 河南大学 | 用于催化烃类裂解制取丙烯的分子筛催化剂及其制备方法和用途 |
| CN116588949B (zh) * | 2023-04-20 | 2025-08-22 | 延长中科（大连）能源科技股份有限公司 | 一种高硅丝光沸石分子筛的制备方法及其应用 |
| CN116621191A (zh) * | 2023-06-02 | 2023-08-22 | 深圳鼎诚环境科学有限公司 | 用于去除VOCs中苯系物的分子筛吸附剂及其制备方法 |
Family Cites Families (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3354078A (en) | 1965-02-04 | 1967-11-21 | Mobil Oil Corp | Catalytic conversion with a crystalline aluminosilicate activated with a metallic halide |
| US3551353A (en) * | 1968-10-04 | 1970-12-29 | Mobil Oil Corp | Dealuminzation of mordenite |
| US4536486A (en) | 1983-03-31 | 1985-08-20 | Texaco Inc. | Process for dewaxing with mordenite |
| FR2637200B1 (fr) | 1988-10-05 | 1991-01-04 | Inst Francais Du Petrole | Catalyseur a base de mordenite renfermant au moins un metal du groupe viii et son utilisation en isomerisation d'une coupe c8 aromatique |
| US5234872A (en) * | 1992-05-11 | 1993-08-10 | Mobil Oil Corp. | Method for producing zeolites with reduced surface acidity |
| US5238677A (en) * | 1992-06-15 | 1993-08-24 | Mobil Oil Corp. | Process for the dealumination of mordenite |
| EA003270B1 (ru) * | 1996-05-29 | 2003-02-27 | Эксон Кемикэл Пейтентс Инк. | Способ конверсии ароматических соединений и применяемый для этого цеолитный катализатор |
| US6060417A (en) | 1996-06-28 | 2000-05-09 | Toray Industries, Inc. | Catalyst composition for transalkylation of alkylaromatic hydrocarbons and process for production of xylene |
| FR2761904B1 (fr) | 1997-04-09 | 1999-05-14 | Inst Francais Du Petrole | Catalyseur a base de mordenite desaluminee et son utilisation en dismutation et/ou transalkylation d'hydrocarbures aromatiques |
| FR2772751B1 (fr) | 1997-12-22 | 2000-04-14 | Inst Francais Du Petrole | Catalyseur a base de mordenite contenant au moins un metal du groupe viii et au moins un metal des groupes iii et iv et son utilisation en isomerisation d'une coupe c8 aromatique |
| GB9816508D0 (en) * | 1998-07-29 | 1998-09-23 | Exxon Chemical Patents Inc | Molecular sieves and processes for their manufacture |
| US6867340B2 (en) | 1998-12-24 | 2005-03-15 | Sk Corporation | Disproportionation/transalkylation of aromatic hydrocarbons |
| RU2160228C1 (ru) * | 1999-04-30 | 2000-12-10 | Институт нефтехимии и катализа АН РБ и УНЦ РАН | Способ получения цеолита типа морденит |
| US6984764B1 (en) * | 1999-05-04 | 2006-01-10 | Exxonmobil Oil Corporation | Alkylaromatics production |
| JP4506908B2 (ja) * | 1999-08-03 | 2010-07-21 | 三菱瓦斯化学株式会社 | メチルアミン製造触媒 |
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| JP4120172B2 (ja) * | 2001-02-28 | 2008-07-16 | 東レ株式会社 | モルデナイト構造を有するゼオライト、モルデナイト構造を有するゼオライトの製造方法、芳香族化合物転化用触媒組成物および転化方法 |
| US6504076B1 (en) | 2001-05-18 | 2003-01-07 | Fina Technology, Inc. | Method of conversion of heavy aromatics |
| US6815570B1 (en) | 2002-05-07 | 2004-11-09 | Uop Llc | Shaped catalysts for transalkylation of aromatics for enhanced xylenes production |
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| JP4882202B2 (ja) * | 2004-02-09 | 2012-02-22 | 東ソー株式会社 | 高シリカモルデナイトの合成方法 |
| US6972348B2 (en) | 2004-03-24 | 2005-12-06 | Uop Llc | Catalytic conversion of polycyclic aromatics into xylenes |
| DK1586376T3 (da) | 2004-04-14 | 2009-10-12 | Inst Francais Du Petrole | Katalysator, der omfatter en 10 MR zeolit og en 12 MR zeolit samt anvendelse deraf til transalkylering af alkylaromatiske carbonhydrider |
| US7273828B1 (en) | 2004-05-27 | 2007-09-25 | Uop Llc | Catalyst treatment useful for aromatics conversion process |
| US7154014B1 (en) | 2004-09-22 | 2006-12-26 | Uop Llc | Alumina guard bed for aromatics transalkylation process |
| CN1666956A (zh) * | 2005-02-04 | 2005-09-14 | 华东理工大学 | 一种纳米尺寸丝光沸石合成方法 |
| CN101519217B (zh) * | 2008-02-28 | 2011-01-19 | 中国石油化工股份有限公司石油化工科学研究院 | 一种小晶粒丝光沸石的制备方法 |
| US7687423B2 (en) | 2008-06-26 | 2010-03-30 | Uop Llc | Selective catalyst for aromatics conversion |
| US7626064B1 (en) * | 2008-06-26 | 2009-12-01 | Uop Llc | Transalkylation process |
| EP2174713A1 (en) * | 2008-10-13 | 2010-04-14 | BP Chemicals Limited | Dealumination process |
| KR20110121474A (ko) * | 2010-04-30 | 2011-11-07 | 인하대학교 산학협력단 | 계층적 메조세공 무기 재료 및 그의 제조 방법 |
| JP5351216B2 (ja) | 2010-07-01 | 2013-11-27 | 日本化学工業株式会社 | ゼオライトの製造方法 |
| CN102530984A (zh) * | 2010-12-30 | 2012-07-04 | 中国石油化工股份有限公司 | 改性丝光沸石、其制备方法及其应用 |
| JP5657458B2 (ja) * | 2011-04-04 | 2015-01-21 | 日本化学工業株式会社 | 薄片状の結晶形状を有するモルデナイト型ゼオライトおよびその製造方法 |
| JP6084829B2 (ja) * | 2012-11-29 | 2017-02-22 | 株式会社Ihi | 放射性物質収着剤の製造方法 |
| WO2014135662A1 (en) * | 2013-03-08 | 2014-09-12 | Bp Chemicals Limited | Carbonylation process |
| CN103482645B (zh) * | 2013-09-22 | 2015-07-08 | 华东师范大学 | 一种多级孔纳米丝光沸石分子筛的制备方法 |
| CA2983038C (en) * | 2015-02-04 | 2023-01-31 | Exxonmobil Chemical Patents Inc. | Process for preparing a molecular sieve |
| US10118165B2 (en) * | 2015-02-04 | 2018-11-06 | Exxonmobil Chemical Patents Inc. | Catalyst compositions and use in heavy aromatics conversion processes |
-
2016
- 2016-01-21 CA CA2983038A patent/CA2983038C/en active Active
- 2016-01-21 JP JP2017540166A patent/JP6724020B2/ja active Active
- 2016-01-21 CN CN201680008751.5A patent/CN107207269B/zh active Active
- 2016-01-21 US US15/002,809 patent/US10017394B2/en active Active
- 2016-01-21 RU RU2017125266A patent/RU2700052C2/ru not_active IP Right Cessation
- 2016-01-21 ES ES16709611T patent/ES2750826T3/es active Active
- 2016-01-21 SG SG11201705830RA patent/SG11201705830RA/en unknown
- 2016-01-21 SG SG10202010226SA patent/SG10202010226SA/en unknown
- 2016-01-21 WO PCT/US2016/014264 patent/WO2016126431A1/en not_active Ceased
- 2016-01-21 KR KR1020177022220A patent/KR102527695B1/ko active Active
- 2016-01-21 EP EP16709611.4A patent/EP3253713B1/en active Active
-
2017
- 2017-07-05 ZA ZA2017/04548A patent/ZA201704548B/en unknown
-
2018
- 2018-05-21 US US15/984,595 patent/US10745285B2/en active Active
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