JP2018123288A - テルペン系炭化水素香料化合物高含有の水中油型乳化香料組成物 - Google Patents
テルペン系炭化水素香料化合物高含有の水中油型乳化香料組成物 Download PDFInfo
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- JP2018123288A JP2018123288A JP2017019024A JP2017019024A JP2018123288A JP 2018123288 A JP2018123288 A JP 2018123288A JP 2017019024 A JP2017019024 A JP 2017019024A JP 2017019024 A JP2017019024 A JP 2017019024A JP 2018123288 A JP2018123288 A JP 2018123288A
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- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
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- A23L2/38—Other non-alcoholic beverages
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
-
- C—CHEMISTRY; METALLURGY
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Abstract
【解決手段】以下の成分(A)〜(C)を含有する、水中油型乳化香料組成物を提供する:(A)香料であって、その全量に対し(a)テルペン系炭化水素香料化合物(リモネンを除く):10質量%以上および(b)リモネン:0質量%以上50質量%未満の香料化合物を含有する;(B)乳化剤;および(C)糖類、エタノールおよび多価アルコールからなる群より選ばれる1種または2種以上。
【選択図】なし
Description
[1] 下記(A)、(B)、および(C)を含有する水中油型乳化香料組成物。
(A)香料
下記(a)および(b)の香料化合物を、香料全量に対し下記の割合で含有する
(a)テルペン系炭化水素香料化合物(リモネンを除く):10質量%以上
(b)リモネン:0質量%以上50質量%未満
(B)乳化剤
(C)糖類、エタノールおよび多価アルコールからなる群より選ばれる1種または2種以上
[2] (A)香料が、更に(c)含酸素香料化合物を、(A)香料全量に対し90質量%未満含有する、前記[1]に記載の水中油型乳化香料組成物。
[3] 更に(D)動植物油脂、(E)水、および(F)油溶性抗酸化剤から選択される1種または2種以上を含有する、前記[1]または[2]に記載の水中油型乳化香料組成物。
[4] (a)のテルペン系炭化水素香料化合物が、アロオシメン、オシメン、ミルセン、ジヒドロミルセン、α‐ファルネセン、β−ファルネセン、α−ピネン、β−ピネン、カンフェン、α−フェランドレン、α−テルピネン、β−テルピネン、γ−テルピネン、3−カレン、p−サイメン、α−ビサボレン、β−ビサボレン、γ−ビサボレン、α−セドレン、β−セドレン、α−カリオフィレン、β−カリオフィレン、γ−カリオフィレン、バレンセン、α−ツヨプセン、β−ツヨプセン、α−グアイエン、β−グアイエン、γ−グアイエン、δ−グアイエン、ロンギホレン、テルピノーレン、カジネンからなる群より選ばれる1種または2種以上である、前記[1]〜[3]のいずれかに記載の水中油型乳化香料組成物。
[5] 水中油型乳化香料組成物がクリアエマルジョンである前記[1]〜[4]のいずれかに記載の水中油型乳化香料組成物。
[6] 前記[1]〜[5]のいずれかに記載の水中油型乳化香料組成物が配合された飲食品。
[7] 更に、水溶性香料が配合された前記[6]に記載の飲食品。
[8] 水溶性香料が、エッセンス香料である前記[7]に記載の飲食品。
[9] 飲食品が飲料である前記[6]〜[8]のいずれかに記載の飲食品。
[10] 飲料が透明飲料である前記[9]に記載の飲料。
下記(a)および(b)の香料化合物を、香料全量に対し下記の割合で含有する
(a)テルペン系炭化水素香料化合物(リモネンを除く):10質量%以上
(b)リモネン:0質量%以上50質量%未満
(B)乳化剤
(C)糖類、エタノールおよび多価アルコールからなる群より選ばれる1種または2種以上
以下、成分(A)〜(C)、および本発明の乳化香料組成物が含んでいてよいその他の化合物について説明する。
本発明の乳化香料組成物は、香料を成分(A)として含む。成分(A)は、リモネンを除くテルペン系炭化水素香料化合物である成分(a)を必須成分として含有する。成分(A)は、更に成分(b)としてリモネンを含有してよく、また更に、その他の香料化合物および/または組成物を含有してもよい。
また、上記記載のアルコール類以外に、例えば3−メチル−1−ペンタノール、1−ヘプタノール、2−ヘプタノール、3−オクタノール、1−ノナノール、2−ノナノール、2,6−ジメチルヘプタノール、1−デカノール、トランス−2−ヘキセノール、シス−4−ヘキセノール、シトロネロール、ロジノール、ゲラニオール、ネロール、リナロール、テトラヒドロリナロール、ジメチルオクタノール、ヒドロキシシトロネロール、イソプレゴール、メントール、テルピネオール、ジヒドロテルピネオール、カルベオール、ジヒドロカルベオール、ペリラアルコール、4−ツヤノール、ミルテノール、α−フェンキルアルコール、ファルネソール、ネロリドール、セドレノール、アニスアルコール、ヒドロトロパアルコール、3−フェニルプロピルアルコール、シンナミックアルコール、アミルシンナミックアルコールなどが挙げられる。
本発明の乳化香料組成物は成分(B)として乳化剤を含む。本発明の乳化香料組成物に使用可能な乳化剤の種類は、特に限定されない。例として、グリセリン脂肪酸エステル、アラビアガム、キラヤ抽出物、加工澱粉、ショ糖脂肪酸エステル、ポリソルベート、およびレシチンから選択される1種または2種以上を挙げることができる。グリセリン脂肪酸エステルとしては、例えば、モノグリセリン脂肪酸エステル、ジグリセリン脂肪酸エステル、ポリグリセリン脂肪酸エステルなどが挙げられ、脂肪酸部分はパルミチン酸、ラウリン酸、ステアリン酸、オレイン酸、ミリスチン酸、アラキジン酸、ベヘン酸であるものが例示される。ポリグリセリン脂肪酸エステルの具体例としては、デカグリセリンラウレート、デカグリセリンステアレート、デカグリセリンオレエート、およびデカグリセリンミリステートなどが挙げられる。ショ糖脂肪酸エステルとしては、脂肪酸部分がパルミチン酸、ステアリン酸、アラキジン酸、ベヘン酸であるものが例示される。
本発明の乳化香料組成物は、成分(C)として、糖類、エタノール、および多価アルコールから選択される1種または2種以上を含有する。これらは乳化粒子を安定化させる乳化助剤としての効果を奏し得る。
本発明の乳化香料組成物は、上記成分(A)〜(C)以外にも、本発明の効果を失わない範囲で任意の成分を更に含んでいてよい。以下、そのような成分を例示する。
本発明の乳化香料組成物の粒径は特に限定されないが、以下に記載の粒径とすることができる。
本発明の乳化香料組成物は、テルペン系炭化水素を含有する油相部(成分(A)を含む油溶性成分)と任意の水相部(成分(B)および(C)を含む水溶性成分)とを、公知の任意の方法で撹拌混合などして製造することができる。
本発明の乳化香料組成物は、飲食品、香粧品、保健衛生品、医薬品などに用いる香料組成物の調合素材として有用である。
テルペン系炭化水素香料化合物を含有する水溶性香料および乳化香料組成物の、水性溶媒中での安定性を確認した。
(1)テルペン系炭化水素の高配合による香味への効果
下記表3に示す2種類の処方によりアップルフレーバー(処方Aおよび処方B)を調製した。
(2)乳化香料組成物の調製
次いで、これらのアップルフレーバーを含有する乳化香料組成物の調製を試みた。
(3)テルペン系炭化水素を高含有する乳化香料組成物およびエッセンス香料の飲食品への添加効果
水溶性香料として、エッセンス香料を、アップルフレーバーAまたはBを下記表5に示す処方により約60%の含水エタノールに混合溶解して調製した。アップルフレーバーAを含有するものをエッセンス香料1、アップルフレーバー2を含有するものをエッセンス香料2とした。
下記表8に示す処方により水相部および油相部を調製し、これらをT.K.ロボミックス(登録商標)(プライミクス社製)により8000rpmで10分間撹拌しながら混合し、水中油型乳化香料組成物を2種類(本発明品3および比較品3)調製した。得られた各乳化香料組成物の平均粒径を実施例2と同様に測定したところ、どちらも0.06μmであった。
非常によい:10点
良い:8点
やや良い:6点
やや悪い:4点
悪い:2点
非常に悪い:0点
その評価の平均点および平均的なコメントを下記表に示す。
下記表10に示す処方により水相部および油相部を調製し、これらをT.K.ロボミックス(登録商標)(プライミクス社製)により8000rpmで10分間撹拌しながら混合し、水中油型乳化香料組成物を3種類(本発明品4、比較品4、および比較品5)調製した。本発明品4において、テルペン系炭化水素は、実施例1と同じβ−カリオフィレンを用い、更に、本発明品4および比較品4には柑橘類などの呈味に良質な苦味を付与する化合物として知られる4−メンチルオキシ−2−ブタノンも配合した(特開2016−084418号公報および特許6001031号公報を参照)。比較品5は、市販の75%テルペンレスグレープフルーツオイルを油相部として用いた。
本発明のテルペン系炭化水素高含有乳化香料組成物が果汁の香味に与える効果を確認した。
本発明の乳化香料組成物が飲食品の果汁使用量に与える影響を確認した。
実施例1〜6で使用した以外の種々のテルペン系炭化水素香料化合物の安定性および風味について、実施例1および2と類似の試験を行った。
Claims (10)
- 下記(A)、(B)、および(C)を含有する水中油型乳化香料組成物。
(A)香料
下記(a)および(b)の香料化合物を、香料全量に対し下記の割合で含有する
(a)テルペン系炭化水素香料化合物(リモネンを除く):10質量%以上
(b)リモネン:0質量%以上50質量%未満
(B)乳化剤
(C)糖類、エタノール、および多価アルコールからなる群より選ばれる1種または2種以上 - (A)香料が、更に(c)含酸素香料化合物を、(A)香料全量に対し90質量%未満含有する、請求項1に記載の水中油型乳化香料組成物。
- 更に(D)動植物油脂、(E)水、および(F)油溶性抗酸化剤から選択される1種または2種以上を含有する、請求項1または2に記載の水中油型乳化香料組成物。
- (a)テルペン系炭化水素香料化合物が、アロオシメン、オシメン、ミルセン、ジヒドロミルセン、α−ファルネセン、β−ファルネセン、α−ピネン、β−ピネン、カンフェン、α−フェランドレン、α−テルピネン、β−テルピネン、γ−テルピネン、3−カレン、p−サイメン、α−ビサボレン、β−ビサボレン、γ−ビサボレン、α−セドレン、β−セドレン、α−カリオフィレン、β−カリオフィレン、γ−カリオフィレン、バレンセン、α−ツヨプセン、β−ツヨプセン、α−グアイエン、β−グアイエン、γ−グアイエン、δ−グアイエン、ロンギホレン、テルピノーレン、カジネンからなる群より選ばれる1種または2種以上である、請求項1〜3のいずれか1項に記載の水中油型乳化香料組成物。
- 水中油型乳化香料組成物がクリアエマルジョンである請求項1〜4のいずれか1項に記載の水中油型乳化香料組成物。
- 請求項1〜5のいずれか1項に記載の水中油型乳化香料組成物が配合された飲食品。
- 更に水溶性香料が配合された請求項6に記載の飲食品。
- 水溶性香料がエッセンス香料である請求項7に記載の飲食品。
- 飲食品が飲料である請求項6〜8のいずれか1項に記載の飲食品。
- 飲料が透明飲料である請求項9に記載の飲料。
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- 2018-01-26 CN CN201880005075.5A patent/CN110049684A/zh active Pending
- 2018-01-26 WO PCT/JP2018/002573 patent/WO2018143103A1/ja active Application Filing
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WO2025005261A1 (ja) * | 2023-06-30 | 2025-01-02 | サントリーホールディングス株式会社 | 組成物、原料酒及び飲料 |
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TW201828823A (zh) | 2018-08-16 |
TWI700045B (zh) | 2020-08-01 |
CN110049684A (zh) | 2019-07-23 |
JP6847520B2 (ja) | 2021-03-24 |
WO2018143103A1 (ja) | 2018-08-09 |
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