JP2017512132A5 - - Google Patents
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- Publication number
- JP2017512132A5 JP2017512132A5 JP2016568118A JP2016568118A JP2017512132A5 JP 2017512132 A5 JP2017512132 A5 JP 2017512132A5 JP 2016568118 A JP2016568118 A JP 2016568118A JP 2016568118 A JP2016568118 A JP 2016568118A JP 2017512132 A5 JP2017512132 A5 JP 2017512132A5
- Authority
- JP
- Japan
- Prior art keywords
- particulate
- material according
- silsesquioxane
- silica particles
- preparing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 18
- 239000002245 particle Substances 0.000 claims description 9
- 230000007062 hydrolysis Effects 0.000 claims description 7
- 238000006460 hydrolysis reaction Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 5
- 239000004094 surface-active agent Substances 0.000 claims description 5
- 239000002244 precipitate Substances 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000011148 porous material Substances 0.000 claims description 2
- 239000000463 material Substances 0.000 claims 18
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 8
- 238000004587 chromatography analysis Methods 0.000 claims 7
- 239000011236 particulate material Substances 0.000 claims 7
- 125000000962 organic group Chemical group 0.000 claims 5
- 229910004298 SiO 2 Inorganic materials 0.000 claims 4
- 229910052710 silicon Inorganic materials 0.000 claims 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims 2
- 125000001183 hydrocarbyl group Chemical group 0.000 claims 2
- 238000004811 liquid chromatography Methods 0.000 claims 2
- 238000002414 normal-phase solid-phase extraction Methods 0.000 claims 2
- 229910000077 silane Inorganic materials 0.000 claims 2
- 230000005526 G1 to G0 transition Effects 0.000 claims 1
- DHXVGJBLRPWPCS-UHFFFAOYSA-N Tetrahydropyran Chemical group C1CCOCC1 DHXVGJBLRPWPCS-UHFFFAOYSA-N 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 238000006482 condensation reaction Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 239000003361 porogen Substances 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 10
- 239000000243 solution Substances 0.000 description 10
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 description 6
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 238000010923 batch production Methods 0.000 description 3
- 238000005119 centrifugation Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000003760 magnetic stirring Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- -1 isooctyl Chemical group 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010907 stover Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14/175,689 | 2014-02-07 | ||
| US14/175,689 US20150224473A1 (en) | 2014-02-07 | 2014-02-07 | Chromatographic material and methods for the synthesis thereof |
| PCT/EP2015/052511 WO2015118105A1 (en) | 2014-02-07 | 2015-02-06 | Chromatographic material and methods for the synthesis thereof |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017512132A JP2017512132A (ja) | 2017-05-18 |
| JP2017512132A5 true JP2017512132A5 (enExample) | 2018-12-13 |
| JP6480471B2 JP6480471B2 (ja) | 2019-03-13 |
Family
ID=52596942
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016568118A Active JP6480471B2 (ja) | 2014-02-07 | 2015-02-06 | クロマトグラフィー材料及びその合成方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US20150224473A1 (enExample) |
| JP (1) | JP6480471B2 (enExample) |
| CN (1) | CN105960281B (enExample) |
| DE (1) | DE112015000675T5 (enExample) |
| GB (1) | GB2540269B (enExample) |
| WO (1) | WO2015118105A1 (enExample) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105233811B (zh) * | 2015-10-16 | 2018-03-09 | 苏州大学 | 一种键合型色谱柱固定相及其制备方法 |
| US20210061824A1 (en) * | 2017-04-20 | 2021-03-04 | National Institute Of Advanced Industrial Science And Technology | Silanol compound and method for producing silanol compound |
| US10661250B2 (en) * | 2018-04-13 | 2020-05-26 | Agilent Technologies, Inc. | Synthetic silica as packing material in supported liquid extraction |
| CN108774413A (zh) * | 2018-04-13 | 2018-11-09 | 太仓运通新材料科技有限公司 | 纳米二氧化硅分散液及其制备方法 |
| CN111468087B (zh) * | 2019-01-23 | 2023-05-02 | 中国科学院大连化学物理研究所 | 一种修饰杂化整体材料及其制备和应用 |
| CN112619705B (zh) * | 2019-09-24 | 2023-08-04 | 中国石油化工股份有限公司 | 环氧烷烃加成反应催化剂及其应用 |
| US11964874B2 (en) | 2020-06-09 | 2024-04-23 | Agilent Technologies, Inc. | Etched non-porous particles and method of producing thereof |
| CN113797903A (zh) * | 2020-06-12 | 2021-12-17 | 江苏汉邦科技有限公司 | 一种杂化硅胶色谱填料的制备方法 |
| US20220354757A1 (en) * | 2021-05-04 | 2022-11-10 | Momentive Performance Materials Japan Llc | Method for producing silica particles and their use in cosmetic compositions |
| CN114133571B (zh) * | 2021-10-18 | 2022-10-04 | 镇江海关综合技术中心 | Pmo(slltp-poss)亲水微球及其制备方法与应用 |
| CN114878734B (zh) * | 2022-03-28 | 2023-12-01 | 中国科学院上海微系统与信息技术研究所 | 基于逐层沉积介孔二氧化硅为固定相的微色谱柱制备方法 |
| EP4279454A4 (en) | 2022-03-29 | 2024-04-03 | Nissan Chemical Corporation | Cage silicate and method for producing same |
| WO2023188930A1 (ja) * | 2022-03-29 | 2023-10-05 | 日産化学株式会社 | 層状ケイ酸塩の製造方法、及びシリカナノシートの製造等におけるその応用 |
| TWI802377B (zh) | 2022-04-20 | 2023-05-11 | 台灣創新材料股份有限公司 | 用於吸附層析術的靜相媒質及其製造方法 |
| CN115178245A (zh) * | 2022-06-21 | 2022-10-14 | 南通裕弘分析仪器有限公司 | 一种有机无机杂化硅胶颗粒的制备方法及其应用 |
| US20240229242A9 (en) * | 2022-10-20 | 2024-07-11 | The Regents Of The University Of Michigan | Additive Solution-Processed Structural Colors |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2357184A1 (de) | 1973-11-16 | 1975-05-22 | Merck Patent Gmbh | Verfahren zur herstellung von organisch modifizierten siliciumdioxiden |
| JPH04269656A (ja) * | 1991-02-26 | 1992-09-25 | Toray Dow Corning Silicone Co Ltd | 液体クロマトグラフィー用充填剤 |
| US6686035B2 (en) | 1999-02-05 | 2004-02-03 | Waters Investments Limited | Porous inorganic/organic hybrid particles for chromatographic separations and process for their preparation |
| EP1848762A4 (en) * | 2005-02-14 | 2010-07-21 | Hybrid Plastics Inc | MODULATION OF POROSITY USING SILSESQUIOXANES OLIGOMERES POLYEDRES |
| JP5358570B2 (ja) * | 2007-07-13 | 2013-12-04 | ユニバーシティ・カレッジ・コークーナショナル・ユニバーシティ・オブ・アイルランド，コーク | 微粒子合成方法 |
| US8063113B2 (en) * | 2008-04-23 | 2011-11-22 | Momentive Performance Materials Inc. | Polyurethane foam-forming compositions containing polysilsesquioxane cell opening agents |
| WO2012112553A1 (en) | 2011-02-14 | 2012-08-23 | Dionex Corporation | Nanometer size chemical modified materials and uses |
-
2014
- 2014-02-07 US US14/175,689 patent/US20150224473A1/en not_active Abandoned
-
2015
- 2015-02-06 JP JP2016568118A patent/JP6480471B2/ja active Active
- 2015-02-06 GB GB1610858.1A patent/GB2540269B/en active Active
- 2015-02-06 DE DE112015000675.3T patent/DE112015000675T5/de active Pending
- 2015-02-06 CN CN201580006617.7A patent/CN105960281B/zh active Active
- 2015-02-06 WO PCT/EP2015/052511 patent/WO2015118105A1/en not_active Ceased
-
2019
- 2019-04-08 US US16/378,296 patent/US20190232252A1/en not_active Abandoned
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