JP2015515499A5 - - Google Patents
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- Publication number
- JP2015515499A5 JP2015515499A5 JP2015510423A JP2015510423A JP2015515499A5 JP 2015515499 A5 JP2015515499 A5 JP 2015515499A5 JP 2015510423 A JP2015510423 A JP 2015510423A JP 2015510423 A JP2015510423 A JP 2015510423A JP 2015515499 A5 JP2015515499 A5 JP 2015515499A5
- Authority
- JP
- Japan
- Prior art keywords
- zeolite
- acetone
- stream
- isopropanol
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 72
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 21
- AMIMRNSIRUDHCM-UHFFFAOYSA-N Isopropylaldehyde Chemical compound CC(C)C=O AMIMRNSIRUDHCM-UHFFFAOYSA-N 0.000 claims description 10
- NBBJYMSMWIIQGU-UHFFFAOYSA-N Propionic aldehyde Chemical compound CCC=O NBBJYMSMWIIQGU-UHFFFAOYSA-N 0.000 claims description 10
- GELKGHVAFRCJNA-UHFFFAOYSA-N 2,2-Dimethyloxirane Chemical compound CC1(C)CO1 GELKGHVAFRCJNA-UHFFFAOYSA-N 0.000 claims description 5
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 claims description 5
- ZTQSAGDEMFDKMZ-UHFFFAOYSA-N butyric aldehyde Natural products CCCC=O ZTQSAGDEMFDKMZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 claims description 4
- 229920005989 resin Polymers 0.000 claims description 2
- 239000011347 resin Substances 0.000 claims description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 38
- 229910021536 Zeolite Inorganic materials 0.000 claims 33
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 33
- 239000010457 zeolite Substances 0.000 claims 33
- 238000000034 method Methods 0.000 claims 19
- 239000012535 impurity Substances 0.000 claims 15
- 238000009835 boiling Methods 0.000 claims 13
- BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 claims 12
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims 9
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 claims 9
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 claims 6
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims 6
- TZIHFWKZFHZASV-UHFFFAOYSA-N methyl formate Chemical compound COC=O TZIHFWKZFHZASV-UHFFFAOYSA-N 0.000 claims 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 4
- 238000004519 manufacturing process Methods 0.000 claims 4
- FXNDIJDIPNCZQJ-UHFFFAOYSA-N 2,4,4-trimethylpent-1-ene Chemical group CC(=C)CC(C)(C)C FXNDIJDIPNCZQJ-UHFFFAOYSA-N 0.000 claims 3
- IKHGUXGNUITLKF-XPULMUKRSA-N acetaldehyde Chemical compound [14CH]([14CH3])=O IKHGUXGNUITLKF-XPULMUKRSA-N 0.000 claims 3
- 150000001299 aldehydes Chemical class 0.000 claims 3
- 239000011973 solid acid Substances 0.000 claims 3
- RUPAXCPQAAOIPB-UHFFFAOYSA-N tert-butyl formate Chemical compound CC(C)(C)OC=O RUPAXCPQAAOIPB-UHFFFAOYSA-N 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 claims 2
- JYIBXUUINYLWLR-UHFFFAOYSA-N aluminum;calcium;potassium;silicon;sodium;trihydrate Chemical compound O.O.O.[Na].[Al].[Si].[K].[Ca] JYIBXUUINYLWLR-UHFFFAOYSA-N 0.000 claims 2
- UNYSKUBLZGJSLV-UHFFFAOYSA-L calcium;1,3,5,2,4,6$l^{2}-trioxadisilaluminane 2,4-dioxide;dihydroxide;hexahydrate Chemical compound O.O.O.O.O.O.[OH-].[OH-].[Ca+2].O=[Si]1O[Al]O[Si](=O)O1.O=[Si]1O[Al]O[Si](=O)O1 UNYSKUBLZGJSLV-UHFFFAOYSA-L 0.000 claims 2
- 229910052676 chabazite Inorganic materials 0.000 claims 2
- 229910001603 clinoptilolite Inorganic materials 0.000 claims 2
- -1 cyhairite Inorganic materials 0.000 claims 2
- 229910052675 erionite Inorganic materials 0.000 claims 2
- 239000012013 faujasite Substances 0.000 claims 2
- 238000005984 hydrogenation reaction Methods 0.000 claims 2
- 229910052680 mordenite Inorganic materials 0.000 claims 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 230000002378 acidificating effect Effects 0.000 claims 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- 150000002924 oxiranes Chemical class 0.000 claims 1
- 229920001467 poly(styrenesulfonates) Polymers 0.000 claims 1
- 239000002952 polymeric resin Substances 0.000 claims 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- 229920003002 synthetic resin Polymers 0.000 claims 1
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 4
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 238000004817 gas chromatography Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/464,726 | 2012-05-04 | ||
| US13/464,726 US8710274B2 (en) | 2012-05-04 | 2012-05-04 | Method of purifying crude acetone stream |
| PCT/US2013/039039 WO2013166130A1 (en) | 2012-05-04 | 2013-05-01 | Method of purifying crude acetone stream |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015515499A JP2015515499A (ja) | 2015-05-28 |
| JP2015515499A5 true JP2015515499A5 (enExample) | 2016-04-28 |
| JP5934433B2 JP5934433B2 (ja) | 2016-06-15 |
Family
ID=49513054
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015510423A Expired - Fee Related JP5934433B2 (ja) | 2012-05-04 | 2013-05-01 | 粗アセトン流の精製方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8710274B2 (enExample) |
| EP (1) | EP2844631B1 (enExample) |
| JP (1) | JP5934433B2 (enExample) |
| KR (1) | KR101662927B1 (enExample) |
| CN (1) | CN104245655B (enExample) |
| WO (1) | WO2013166130A1 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10208008B2 (en) * | 2014-11-26 | 2019-02-19 | Visolis, Inc. | Processes for conversion of biologically derived mevalonic acid |
| CN107513011B (zh) * | 2017-09-25 | 2020-06-26 | 惠州赛力珑新材料有限公司 | 一种丙酮纯化方法 |
| EP3784644B1 (en) | 2018-04-25 | 2022-03-02 | Lyondell Chemical Technology, L.P. | Methods and apparatuses for purifying crude propane |
| CN110003136B (zh) * | 2019-04-26 | 2023-08-01 | 江苏扬农化工集团有限公司 | 一种使用高效助剂脱除hppo工艺中醛酮杂质的方法和装置 |
| CN115335966B (zh) * | 2020-04-02 | 2023-07-18 | 株式会社德山 | 半导体处理液及其制造方法 |
Family Cites Families (41)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2238016A (en) | 1940-06-25 | 1941-04-08 | Shell Dev | Purification of ketones |
| GB623063A (en) * | 1946-11-19 | 1949-05-11 | Commercial Solvents Great Brit | Improvements in or relating to the process for refining acetone |
| US2906676A (en) | 1956-12-21 | 1959-09-29 | Hercules Powder Co Ltd | Process for purifying crude acetone |
| DE1191798B (de) | 1963-03-12 | 1965-04-29 | Hoechst Ag | Verfahren und Vorrichtung zur Reinigung von Aceton |
| GB1092629A (en) | 1964-11-27 | 1967-11-29 | Distillers Co Yeast Ltd | Separation of acetone from organic mixtures |
| US3531376A (en) | 1968-12-23 | 1970-09-29 | Mitsubishi Chem Ind | Purification of acetone by extractive distillation and rectification with simultaneous alkali-containing acetone solution contact and halogen impurity side stream removal |
| US3668256A (en) | 1969-08-13 | 1972-06-06 | Allied Chem | Purification of acetone |
| JPS5432412A (en) | 1977-08-16 | 1979-03-09 | Mitsui Petrochem Ind Ltd | Purification of ketone |
| JPS55157531A (en) | 1979-05-25 | 1980-12-08 | Sumitomo Chem Co Ltd | Recovery of acetone |
| DE3160695D1 (en) | 1980-05-27 | 1983-09-01 | Bp Chem Int Ltd | Process for the recovery of pure acetone from cumene hydroperoxide cleavage reaction product |
| DE3149094A1 (de) | 1981-12-11 | 1983-06-16 | Hoechst Ag, 6230 Frankfurt | Verfahren zur entfernung von aceton aus reaktionsgemischen von carbonylierungsreaktionen |
| US4584063A (en) | 1982-06-28 | 1986-04-22 | Lloyd Berg | Separation of acetone from methanol by extractive distillation |
| JPH0629198B2 (ja) | 1984-10-19 | 1994-04-20 | 武田薬品工業株式会社 | 化学的脱水反応方法 |
| US4722769A (en) | 1986-04-24 | 1988-02-02 | Allied Corporation | Process for recovery of acetone |
| US4766249A (en) | 1986-04-25 | 1988-08-23 | Mallinckrodt, Inc. | Method of catalytically hydrolyzing alpha, beta-unsaturated carbonyl compounds |
| JP2762591B2 (ja) * | 1989-07-25 | 1998-06-04 | 三菱化学株式会社 | イソプロピルアルコールの製造方法 |
| US4931145A (en) | 1989-10-16 | 1990-06-05 | Lloyd Berg | Separation of benzene from acetone by azeotropic distillation |
| JP2786272B2 (ja) * | 1989-10-24 | 1998-08-13 | 三井化学株式会社 | イソプロパノールの製造方法 |
| US5057192A (en) | 1990-11-02 | 1991-10-15 | Eastman Kodak Company | Acetone removal from acetic anhydride production process |
| US5240566A (en) | 1992-12-07 | 1993-08-31 | The Goodyear Tire & Rubber Company | Separation process |
| US5399776A (en) | 1993-11-24 | 1995-03-21 | The Dow Chemical Company | Purification of acetone |
| US5567853A (en) | 1995-02-17 | 1996-10-22 | Arco Chemical Technology, L.P. | Purification of acetone |
| WO1997012654A1 (en) | 1995-10-05 | 1997-04-10 | Exxon Chemical Patents Inc. | Method for recovering acetone |
| IT1276823B1 (it) | 1995-10-06 | 1997-11-03 | Enichem Spa | Procedimento per la purificazione dell'acetone |
| JP4054846B2 (ja) * | 1995-12-19 | 2008-03-05 | バッジャー・ライセンシング・エルエルシー | ビスフェノールの改良された製造方法 |
| US5762764A (en) | 1996-08-29 | 1998-06-09 | Arco Chemical Technology, L.P. | Purification of acetone |
| JP2000290217A (ja) * | 1999-03-31 | 2000-10-17 | Mitsui Chemicals Inc | アセトンの精製方法 |
| US6340777B1 (en) | 1999-10-22 | 2002-01-22 | General Electric Company | Method for purifying acetone |
| US6303826B1 (en) | 2000-01-19 | 2001-10-16 | Sunoco, Inc. (R&M) | Method for purification of acetone |
| US6331654B1 (en) | 2000-02-10 | 2001-12-18 | Illa International Llc | Method of production of product acetone of high stability to oxidation |
| ZA200107297B (en) | 2000-09-15 | 2002-03-11 | Catalytic Distillation Tech | Production of methyl isobutyl ketone. |
| DE10060503A1 (de) | 2000-12-06 | 2002-06-20 | Phenolchemie Gmbh & Co Kg | Verfahren und Vorrichtung zur destillativen Aufarbeitung von Spaltproduktgemischen, welche bei der Spaltung von Alkylarylhydroperoxiden anfallen |
| ES2301592T3 (es) | 2002-07-11 | 2008-07-01 | INEOS PHENOL GMBH & CO. KG | Proceso continuo para recuperar acetona de una corriente residual resultante de la purificacion de acetona. |
| US7416645B2 (en) | 2002-07-11 | 2008-08-26 | Ineos Phenol Gmbh & Co. Kg | Continuous process for recovering acetone from a waste stream resulting from acetone purification |
| US7282613B2 (en) | 2003-02-14 | 2007-10-16 | Shell Oil Company | Process for producing phenol and methyl ethyl ketone |
| US7041857B1 (en) * | 2005-09-07 | 2006-05-09 | Air Products And Chemicals, Inc. | Hydrogenation of acetone |
| US7605291B2 (en) | 2006-04-27 | 2009-10-20 | Adalberto Maldonado | Method for the preparation of volatile Anesthetics |
| RU2404954C2 (ru) | 2008-10-16 | 2010-11-27 | Общество с ограниченной ответственностью "Еврохим-СПб-Трейдинг" | Способ получения фенола и ацетона |
| RU2403236C2 (ru) | 2008-12-09 | 2010-11-10 | Общество с ограниченной ответственностью "Новые технологии" | Способ очистки ацетона |
| RU2400469C2 (ru) | 2008-12-09 | 2010-09-27 | Общество с ограниченной ответственностью "Новые технологии" | Способ очистки ацетона-сырца |
| EP2204357A1 (en) | 2009-01-06 | 2010-07-07 | BP Chemicals Limited | Process for removing acetone from a stream comprising acetone, methyl acetate and methyl iodide |
-
2012
- 2012-05-04 US US13/464,726 patent/US8710274B2/en active Active
-
2013
- 2013-05-01 EP EP13784982.4A patent/EP2844631B1/en not_active Not-in-force
- 2013-05-01 KR KR1020147032663A patent/KR101662927B1/ko not_active Expired - Fee Related
- 2013-05-01 CN CN201380021149.1A patent/CN104245655B/zh active Active
- 2013-05-01 WO PCT/US2013/039039 patent/WO2013166130A1/en not_active Ceased
- 2013-05-01 JP JP2015510423A patent/JP5934433B2/ja not_active Expired - Fee Related
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