JP2014237723A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2014237723A5 JP2014237723A5 JP2014190893A JP2014190893A JP2014237723A5 JP 2014237723 A5 JP2014237723 A5 JP 2014237723A5 JP 2014190893 A JP2014190893 A JP 2014190893A JP 2014190893 A JP2014190893 A JP 2014190893A JP 2014237723 A5 JP2014237723 A5 JP 2014237723A5
- Authority
- JP
- Japan
- Prior art keywords
- formula
- meth
- acrylate
- oxygen
- less
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000006243 chemical reaction Methods 0.000 claims description 11
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 claims description 6
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- NWVVVBRKAWDGAB-UHFFFAOYSA-N p-methoxyphenol Chemical compound COC1=CC=C(O)C=C1 NWVVVBRKAWDGAB-UHFFFAOYSA-N 0.000 claims description 4
- WDQMWEYDKDCEHT-UHFFFAOYSA-N 2-ethylhexyl 2-methylprop-2-enoate Chemical group CCCCC(CC)COC(=O)C(C)=C WDQMWEYDKDCEHT-UHFFFAOYSA-N 0.000 claims description 2
- 238000004821 distillation Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims 15
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 15
- 239000001301 oxygen Substances 0.000 claims 15
- 229910052760 oxygen Inorganic materials 0.000 claims 15
- 238000006116 polymerization reaction Methods 0.000 claims 6
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 4
- 125000000217 alkyl group Chemical group 0.000 claims 4
- 239000003112 inhibitor Substances 0.000 claims 4
- -1 2-ethylhexyl group Chemical group 0.000 claims 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 3
- 125000004432 carbon atom Chemical group C* 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 3
- 229920001577 copolymer Polymers 0.000 claims 3
- 238000004519 manufacturing process Methods 0.000 claims 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 239000007789 gas Substances 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 150000002642 lithium compounds Chemical class 0.000 claims 2
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 claims 2
- 239000011541 reaction mixture Substances 0.000 claims 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 229940043430 calcium compound Drugs 0.000 claims 1
- 150000001674 calcium compounds Chemical class 0.000 claims 1
- 229920001519 homopolymer Polymers 0.000 claims 1
- 238000010992 reflux Methods 0.000 description 4
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- ZMVHTLOQSTVDFE-UHFFFAOYSA-N methanol;methyl 2-methylprop-2-enoate Chemical compound OC.COC(=O)C(C)=C ZMVHTLOQSTVDFE-UHFFFAOYSA-N 0.000 description 2
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US1492707P | 2007-12-19 | 2007-12-19 | |
| US61/014,927 | 2007-12-19 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010538506A Division JP2011506517A (ja) | 2007-12-19 | 2008-09-29 | （メタ）アクリレートの製造方法 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017000518A Division JP2017088608A (ja) | 2007-12-19 | 2017-01-05 | （メタ）アクリレートの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2014237723A JP2014237723A (ja) | 2014-12-18 |
| JP2014237723A5 true JP2014237723A5 (enExample) | 2016-06-23 |
Family
ID=40530354
Family Applications (5)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010538506A Pending JP2011506517A (ja) | 2007-12-19 | 2008-09-29 | （メタ）アクリレートの製造方法 |
| JP2014190893A Pending JP2014237723A (ja) | 2007-12-19 | 2014-09-19 | （メタ）アクリレートの製造方法 |
| JP2017000518A Pending JP2017088608A (ja) | 2007-12-19 | 2017-01-05 | （メタ）アクリレートの製造方法 |
| JP2020000396A Pending JP2020073555A (ja) | 2007-12-19 | 2020-01-06 | （メタ）アクリレートの製造方法 |
| JP2022035159A Pending JP2022081593A (ja) | 2007-12-19 | 2022-03-08 | （メタ）アクリレートの製造方法 |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010538506A Pending JP2011506517A (ja) | 2007-12-19 | 2008-09-29 | （メタ）アクリレートの製造方法 |
Family Applications After (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017000518A Pending JP2017088608A (ja) | 2007-12-19 | 2017-01-05 | （メタ）アクリレートの製造方法 |
| JP2020000396A Pending JP2020073555A (ja) | 2007-12-19 | 2020-01-06 | （メタ）アクリレートの製造方法 |
| JP2022035159A Pending JP2022081593A (ja) | 2007-12-19 | 2022-03-08 | （メタ）アクリレートの製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US9206270B2 (enExample) |
| EP (1) | EP2220023B1 (enExample) |
| JP (5) | JP2011506517A (enExample) |
| CN (1) | CN101462958B (enExample) |
| TW (1) | TWI555728B (enExample) |
| WO (1) | WO2009080380A2 (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9206270B2 (en) * | 2007-12-19 | 2015-12-08 | Evonik Roehm Gmbh | Process for preparing (meth)acrylates |
| US20160090348A1 (en) | 2014-09-30 | 2016-03-31 | Basf Se | Preparation of c8-c24 alkyl (meth)acrylates |
| WO2016071052A1 (de) | 2014-11-05 | 2016-05-12 | Basf Se | Verfahren zur herstellung von c8-c22-alkyl(meth)acrylaten |
| MY185479A (en) * | 2014-12-01 | 2021-05-19 | Basf Se | Process for preparing heonone (meth)acrylate |
| CN107531724B (zh) | 2015-02-26 | 2020-06-23 | 巴斯夫欧洲公司 | 制备异山梨醇乙氧基化物二甲基丙烯酸酯的方法 |
| KR102572781B1 (ko) | 2015-02-26 | 2023-08-31 | 바스프 에스이 | 이소소르비드 디(메트)아크릴레이트의 제조 방법 |
| EP3390338A1 (de) | 2015-12-15 | 2018-10-24 | Basf Se | Verfahren zur herstellung von hydroxybenzophenonpolyglykolether-(meth)acrylat |
| JP7044758B2 (ja) | 2016-08-05 | 2022-03-30 | ビーエーエスエフ ソシエタス・ヨーロピア | ポリイソブテン基を有するマクロモノマー、およびそれらのホモポリマーまたはコポリマー |
| US20240067596A1 (en) * | 2021-01-25 | 2024-02-29 | Basf Se | Continuous method for obtaining 2-ethylhexyl acrylate |
| WO2023143939A1 (de) | 2022-01-26 | 2023-08-03 | Basf Se | Lagerung und/oder transport ethylenisch ungesättigter verbindungen |
| WO2023242259A1 (en) * | 2022-06-15 | 2023-12-21 | Evonik Operations Gmbh | Method for increasing reaction performance by intermediate removal of side product holdup |
| EP4293010A1 (en) * | 2022-06-15 | 2023-12-20 | Evonik Operations GmbH | Process for the discontinuous (trans)esterification of (meth)acrylate compounds |
| EP4299155A1 (en) * | 2022-06-27 | 2024-01-03 | Evonik Operations GmbH | Process to precisely calculate the raw material demand of intermediate batches within a production campaign |
| CN119562975A (zh) * | 2022-10-31 | 2025-03-04 | 三菱化学株式会社 | 含有酯化合物的组合物及其制造方法、聚合性组合物、（甲基）丙烯酸系聚合物及其制造方法 |
Family Cites Families (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3423443A1 (de) * | 1984-06-26 | 1986-01-02 | Röhm GmbH, 6100 Darmstadt | Verfahren zur herstellung von estern der acryl- und methacrylsaeure durch umesterung |
| WO1991016037A1 (en) * | 1990-04-16 | 1991-10-31 | Minnesota Mining And Manufacturing Company | Mildness additives for skin cleansing compositions |
| JP3081707B2 (ja) * | 1992-06-16 | 2000-08-28 | ダイセル化学工業株式会社 | メタクリル酸グリシジルの製造方法 |
| JP3513209B2 (ja) * | 1994-03-30 | 2004-03-31 | 積水化学工業株式会社 | 熱可塑性ポリウレタン |
| JPH0931018A (ja) * | 1995-07-24 | 1997-02-04 | Dainippon Ink & Chem Inc | ペンタエリスリトール（メタ）アクリルエステル類の製造法 |
| JPH10175919A (ja) * | 1996-12-18 | 1998-06-30 | Daicel Chem Ind Ltd | （メタ）アクリル酸テトラヒドロベンジルの製造法 |
| JPH10175918A (ja) * | 1996-12-18 | 1998-06-30 | Daicel Chem Ind Ltd | （メタ）アクリル酸テトラヒドロベンジルの製造方法 |
| EP0882739A3 (en) | 1997-06-06 | 1999-04-07 | Nippon Shokubai Co., Ltd. | High molecular weight polymer and producing method the same and drag reducer |
| JPH1149810A (ja) | 1997-06-06 | 1999-02-23 | Nippon Shokubai Co Ltd | 高分子量ポリマーおよびその製造方法並びにドラッグレデューサ |
| JPH1180082A (ja) * | 1997-09-10 | 1999-03-23 | Kao Corp | （メタ）アクリル酸高級アルキルエステルの製造法 |
| JP2949150B1 (ja) | 1998-02-27 | 1999-09-13 | 日精化学工業株式会社 | メタクリル酸シクロヘキシルの製造方法 |
| JP2000198835A (ja) * | 1999-01-05 | 2000-07-18 | Daicel Chem Ind Ltd | ヒドロキシアルキル（メタ）アクリラ―ト・メチル置換ε―カプロラクトン変性物含有組成物の製造方法 |
| JP2000319225A (ja) * | 1999-04-28 | 2000-11-21 | Mitsubishi Rayon Co Ltd | メタクリル酸アルキルエステルの製造方法 |
| DE19940622C1 (de) * | 1999-08-27 | 2001-05-17 | Roehm Gmbh | Verfahren zur Herstellung von Di(meth)acrylsäureestern |
| CA2384389A1 (en) * | 2000-08-08 | 2002-02-14 | Kaneka Corporation | Expandable vinyl chloride resin composition |
| EP1201641B1 (en) | 2000-10-23 | 2013-08-14 | Nippon Shokubai Co., Ltd. | Composition of vinyl ether group containing (meth)acrylic acid ester and production method thereof |
| JP2002169220A (ja) * | 2000-11-30 | 2002-06-14 | Mamiya Op Co Ltd | カメラのストラップ用吊金具 |
| DE10301902A1 (de) * | 2003-01-17 | 2003-12-04 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| JP2004269417A (ja) | 2003-03-07 | 2004-09-30 | Mitsubishi Rayon Co Ltd | （メタ）アクリル酸エステルの製造方法 |
| WO2005040088A1 (ja) | 2003-10-24 | 2005-05-06 | Mitsubishi Rayon Co., Ltd. | (メタ)アクリル酸エステルの製造方法 |
| JP2006104168A (ja) | 2004-10-08 | 2006-04-20 | Osaka Organic Chem Ind Ltd | （メタ）アクリル酸エステルの製造法 |
| JP2006169220A (ja) | 2004-12-20 | 2006-06-29 | Osaka Organic Chem Ind Ltd | （メタ）アクリル酸エステルの製造法 |
| US7285582B2 (en) * | 2004-12-30 | 2007-10-23 | Conocophillips Company | Modified latex drag reducer and processes therefor and therewith |
| US7361628B2 (en) * | 2004-12-30 | 2008-04-22 | Conocophillips Company | Remote delivery of latex drag-reducing agent without introduction of immiscible low-viscosity flow facilitator |
| TW200728270A (en) * | 2005-11-21 | 2007-08-01 | Toagosei Co Ltd | The manufacture method of (meta) acrylic esters |
| US9206270B2 (en) * | 2007-12-19 | 2015-12-08 | Evonik Roehm Gmbh | Process for preparing (meth)acrylates |
-
2008
- 2008-09-29 US US12/745,703 patent/US9206270B2/en active Active
- 2008-09-29 EP EP08804845.9A patent/EP2220023B1/en active Active
- 2008-09-29 JP JP2010538506A patent/JP2011506517A/ja active Pending
- 2008-09-29 WO PCT/EP2008/062982 patent/WO2009080380A2/en not_active Ceased
- 2008-12-16 TW TW097148967A patent/TWI555728B/zh active
- 2008-12-17 CN CN200810185589.1A patent/CN101462958B/zh active Active
-
2014
- 2014-09-19 JP JP2014190893A patent/JP2014237723A/ja active Pending
-
2015
- 2015-10-27 US US14/924,018 patent/US9688601B2/en active Active
-
2017
- 2017-01-05 JP JP2017000518A patent/JP2017088608A/ja active Pending
-
2020
- 2020-01-06 JP JP2020000396A patent/JP2020073555A/ja active Pending
-
2022
- 2022-03-08 JP JP2022035159A patent/JP2022081593A/ja active Pending
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2014237723A5 (enExample) | ||
| JP5840617B2 (ja) | Ｃ１７−アルコール混合物の（メタ）アクリラートの製造方法 | |
| JP6747560B2 (ja) | カルボン酸エステルの製造方法 | |
| JP2014237723A (ja) | （メタ）アクリレートの製造方法 | |
| BR112020006451B1 (pt) | Processo para preparar dimetilaminoalquil (met)acrilatos | |
| JP6030564B2 (ja) | ブチルアクリレートの製造方法 | |
| EP2848605A1 (en) | Methods for preparing acrylic acid from biobased starting materials | |
| JP5373643B2 (ja) | （メタ）アクリルアミドモノマーを製造する方法 | |
| JP2006206590A (ja) | （メタ）アクリレートエステルモノマーを製造するためのエステル交換方法 | |
| TW201641480A (zh) | （甲基）丙烯酸酯化合物之製造方法 | |
| US2526310A (en) | Process for producing esters of acrylic acid | |
| JPWO2014046261A1 (ja) | ヒドロキシアルキルアクリレート、およびその製造方法 | |
| CN104053642A (zh) | 通过酯交换制备丙烯酸2-辛基酯的方法 | |
| TW201412699A (zh) | 羥烷基（甲基）丙烯酸酯及其製造方法 | |
| CN105481691B (zh) | 双环戊烯基氧乙基甲基丙烯酸酯的合成方法 | |
| JP6030150B2 (ja) | エステル交換による２−オクチルアクリレートの生成のための方法 | |
| JP6828500B2 (ja) | ２−メチル−２−ヒドロキシ−１−プロピル（メタ）アクリレートおよび／または３−メチル−３−ヒドロキシ−１−ブチル（メタ）アクリレートの製造方法ならびに組成物 | |
| CN103582655A (zh) | 协同聚合抑制剂组合物和方法 | |
| JP6957875B2 (ja) | ２−メチル−２−ヒドロキシ−１−プロピル（メタ）アクリレートおよび／または３−メチル−３−ヒドロキシ−１−ブチル（メタ）アクリレートの製造方法ならびに組成物 | |
| KR101178238B1 (ko) | 공비적 에스테르화에 의한 알킬 아크릴레이트의 제조방법 | |
| CN100579951C (zh) | 含氟丙烯酸酯的制造方法 | |
| CN100579950C (zh) | 含氟(甲基)丙烯酸酯的制造方法 | |
| JP2004210745A (ja) | （メタ）アクリル酸エステルの製造方法 | |
| JP2006257138A5 (enExample) | ||
| JP2016210690A (ja) | （メタ）アクリル酸エステル化合物の製造方法 |