JP2012529549A5 - - Google Patents
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- Publication number
- JP2012529549A5 JP2012529549A5 JP2012514476A JP2012514476A JP2012529549A5 JP 2012529549 A5 JP2012529549 A5 JP 2012529549A5 JP 2012514476 A JP2012514476 A JP 2012514476A JP 2012514476 A JP2012514476 A JP 2012514476A JP 2012529549 A5 JP2012529549 A5 JP 2012529549A5
- Authority
- JP
- Japan
- Prior art keywords
- per
- fluoroionomer
- group
- solvent
- liquid composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000000034 method Methods 0.000 claims description 14
- 239000002904 solvent Substances 0.000 claims description 9
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 6
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 6
- 239000002131 composite material Substances 0.000 claims description 3
- 238000005470 impregnation Methods 0.000 claims description 2
- 239000012528 membrane Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims 23
- 239000007788 liquid Substances 0.000 claims 11
- 229910052731 fluorine Inorganic materials 0.000 claims 9
- 229910052794 bromium Inorganic materials 0.000 claims 8
- 229910052801 chlorine Inorganic materials 0.000 claims 8
- 229910052736 halogen Inorganic materials 0.000 claims 8
- 150000002367 halogens Chemical group 0.000 claims 8
- 229910052740 iodine Inorganic materials 0.000 claims 8
- 150000001768 cations Chemical class 0.000 claims 6
- 239000000178 monomer Substances 0.000 claims 5
- 239000003495 polar organic solvent Substances 0.000 claims 5
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 claims 4
- 239000004215 Carbon black (E152) Substances 0.000 claims 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims 3
- 238000003682 fluorination reaction Methods 0.000 claims 3
- 229930195733 hydrocarbon Natural products 0.000 claims 3
- 150000002430 hydrocarbons Chemical group 0.000 claims 3
- 229920001774 Perfluoroether Polymers 0.000 claims 2
- 125000003118 aryl group Chemical group 0.000 claims 2
- 238000005341 cation exchange Methods 0.000 claims 2
- 125000005843 halogen group Chemical group 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims 2
- 239000002243 precursor Substances 0.000 claims 2
- 125000000008 (C1-C10) alkyl group Chemical group 0.000 claims 1
- RRZIJNVZMJUGTK-UHFFFAOYSA-N 1,1,2-trifluoro-2-(1,2,2-trifluoroethenoxy)ethene Chemical class FC(F)=C(F)OC(F)=C(F)F RRZIJNVZMJUGTK-UHFFFAOYSA-N 0.000 claims 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims 1
- 238000000137 annealing Methods 0.000 claims 1
- 239000012736 aqueous medium Substances 0.000 claims 1
- 125000006615 aromatic heterocyclic group Chemical group 0.000 claims 1
- 229920001577 copolymer Polymers 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 1
- 125000001033 ether group Chemical group 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 239000011737 fluorine Substances 0.000 claims 1
- 125000001153 fluoro group Chemical group F* 0.000 claims 1
- 125000003709 fluoroalkyl group Chemical group 0.000 claims 1
- 229920002313 fluoropolymer Polymers 0.000 claims 1
- 239000004811 fluoropolymer Substances 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 125000005010 perfluoroalkyl group Chemical group 0.000 claims 1
- -1 vinyl ether carboxylate Chemical class 0.000 claims 1
- 239000006185 dispersion Substances 0.000 description 5
- 0 *C(F)=C(O*)F Chemical compound *C(F)=C(O*)F 0.000 description 1
- 241000023320 Luma <angiosperm> Species 0.000 description 1
- 239000012470 diluted sample Substances 0.000 description 1
- 229920000554 ionomer Polymers 0.000 description 1
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09162625 | 2009-06-12 | ||
| EP09162625.9 | 2009-06-12 | ||
| PCT/EP2010/058182 WO2010142772A1 (en) | 2009-06-12 | 2010-06-10 | Fluoroionomers dispersions having low surface tension, low liquid viscosity and high solid content |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012529549A JP2012529549A (ja) | 2012-11-22 |
| JP2012529549A5 true JP2012529549A5 (https=) | 2014-06-26 |
| JP5575885B2 JP5575885B2 (ja) | 2014-08-20 |
Family
ID=41202555
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012514476A Active JP5575885B2 (ja) | 2009-06-12 | 2010-06-10 | 低い表面張力、低い液体粘度および高い固体含量を有するフルオロイオノマー分散体 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US9450262B2 (https=) |
| EP (1) | EP2440586B1 (https=) |
| JP (1) | JP5575885B2 (https=) |
| KR (1) | KR101740746B1 (https=) |
| CN (2) | CN110272512A (https=) |
| WO (1) | WO2010142772A1 (https=) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102317324B (zh) * | 2008-12-11 | 2014-12-24 | 索尔维索莱克西斯公司 | 氟代离聚物组合物的纯化 |
| US8709199B2 (en) * | 2011-09-13 | 2014-04-29 | GM Global Technology Operations LLC | Method of preparing a water vapor transfer membrane |
| EP2774203B8 (en) * | 2011-11-04 | 2016-06-01 | Greenerity GmbH | Method for the preparation of catalyst-coated membranes |
| US10020526B2 (en) | 2012-09-12 | 2018-07-10 | GM Global Technology Operations LLC | Reverse osmosis membranes made with PFSA ionomer and ePTFE |
| FR3001732B1 (fr) | 2013-02-04 | 2016-02-26 | Rhodia Operations | Utilisation d'agents dispersants pour la preparation d'encres pour piles a combustible |
| KR20140128895A (ko) * | 2013-04-29 | 2014-11-06 | 주식회사 엘지화학 | 고분자 전해질막, 고분자 전해질막을 포함하는 막전극 접합체 및 막 전극 접합체를 포함하는 연료전지 |
| JP6151111B2 (ja) * | 2013-07-02 | 2017-06-21 | 旭化成株式会社 | 電解質溶液の製造方法、電解質溶液、電解質膜、電極触媒層、膜電極接合体、及び固体高分子電解質型燃料電池 |
| EP2842620A1 (en) | 2013-08-26 | 2015-03-04 | Agfa-Gevaert | A method for preparing a composite membrane |
| WO2020183306A1 (en) * | 2019-03-12 | 2020-09-17 | 3M Innovative Properties Company | Dispersible perfluorosulfonic acid ionomer compositions |
| CN115805185B (zh) * | 2019-06-06 | 2024-04-19 | W.L.戈尔及同仁股份有限公司 | 润湿低表面能基材的方法以及用于该方法的系统 |
| KR102507911B1 (ko) * | 2021-03-31 | 2023-03-07 | 도레이첨단소재 주식회사 | 양이온 교환막 및 이의 제조방법 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3282875A (en) * | 1964-07-22 | 1966-11-01 | Du Pont | Fluorocarbon vinyl ether polymers |
| NL160013C (nl) | 1968-11-26 | 1979-09-17 | Du Pont | Werkwijze ter bereiding van oplossingen van een sulfonyl- groepen bevattend fluorkoolstofpolymeer. |
| US4433082A (en) * | 1981-05-01 | 1984-02-21 | E. I. Du Pont De Nemours And Company | Process for making liquid composition of perfluorinated ion exchange polymer, and product thereof |
| JPH01217042A (ja) * | 1986-09-26 | 1989-08-30 | Dow Chem Co:The | パーフルオロスルホネートイオノマー薄膜の製造方法 |
| WO1998016581A1 (en) | 1996-10-15 | 1998-04-23 | E.I. Du Pont De Nemours And Company | Compositions containing particles of highly fluorinated ion exchange polymer |
| US6025092A (en) * | 1998-02-13 | 2000-02-15 | E. I. Du Pont De Nemours And Company | Fluorinated ionomers and their uses |
| US6100324A (en) * | 1998-04-16 | 2000-08-08 | E. I. Du Pont De Nemours And Company | Ionomers and ionically conductive compositions |
| IT1303779B1 (it) | 1998-11-23 | 2001-02-23 | Ausimont Spa | Preparazione di soluzioni di polimeri fluorurati solfonici. |
| DE60119307T2 (de) | 2000-02-16 | 2007-04-12 | Daikin Industries, Ltd. | Verfahren zur herstellung eines fluorionomers, verfahren zur reinigung und konzentrierung von ionomeren und verfahren zur filmbildung |
| ITMI20010921A1 (it) | 2001-05-07 | 2002-11-07 | Ausimont Spa | Polimeri (per)fluorurati amorfi |
| US6713567B2 (en) * | 2001-07-13 | 2004-03-30 | E. I. Du Pont De Nemours And Company | Method for forming fluorinated ionomers |
| EP1602687B1 (en) * | 2003-03-03 | 2012-01-04 | Daikin Industries, Ltd. | Liquid fluoropolymer composition, process for producing organosol, film, and fuel cell |
| WO2004102714A1 (ja) | 2003-05-13 | 2004-11-25 | Asahi Glass Company, Limited | 固体高分子型燃料電池用電解質ポリマー、その製造方法及び膜・電極接合体 |
| US20070129500A1 (en) | 2003-09-10 | 2007-06-07 | Eiji Honda | Stabilized fluoropolymer and method for producing same |
| US6986947B2 (en) * | 2003-10-09 | 2006-01-17 | 3M Innovative Properties Company | Method of modifying a fluoropolymer and articles thereby |
| US7173067B2 (en) * | 2003-12-17 | 2007-02-06 | 3M Innovative Properties Company | Polymer electrolyte membranes crosslinked by direct fluorination |
| JP4437407B2 (ja) | 2004-01-22 | 2010-03-24 | 旭化成株式会社 | フッ素化スルホン酸ポリマーの製造方法 |
| ITMI20040789A1 (it) | 2004-04-22 | 2004-07-22 | Solvay Solexis Spa | Membrane fluorurate |
| US20060014887A1 (en) | 2004-07-19 | 2006-01-19 | 3M Innovative Properties Company | Method of hydrolyzing a dispersion of ionic fluoropolymer |
| US7304101B2 (en) | 2004-07-19 | 2007-12-04 | 3M Innovative Properties Company | Method of purifying a dispersion of ionic fluoropolymer |
| WO2006019097A1 (ja) * | 2004-08-18 | 2006-02-23 | Asahi Glass Company, Limited | 燃料電池用電解質ポリマー、その製造方法、電解質膜、及び膜・電極接合体 |
| ITMI20042554A1 (it) * | 2004-12-30 | 2005-03-30 | Solvay Solexis Spa | Procedimento per la preparazione di dispersioni di fluoropolimeri |
| US7214740B2 (en) | 2005-05-03 | 2007-05-08 | 3M Innovative Properties Company | Fluorinated ionomers with reduced amounts of carbonyl end groups |
| US8617765B2 (en) | 2005-12-22 | 2013-12-31 | E I Du Pont De Nemours And Company | Chemically stabilized ionomers containing inorganic fillers |
| WO2007073500A2 (en) | 2005-12-22 | 2007-06-28 | E. I. Du Pont De Nemours And Company | Methods to prepare chemically stabilized ionomers containing inorganic fillers |
| WO2007089017A1 (ja) * | 2006-02-03 | 2007-08-09 | Daikin Industries, Ltd. | －ｓｏ３ｈ基含有フルオロポリマー製造方法及び－ｓｏ３ｈ基含有フルオロポリマー |
| EP1914251A1 (en) | 2006-10-17 | 2008-04-23 | Solvay Solexis S.p.A. | Process for stabilizing fluoropolymer having ion exchange groups |
| CN101606262B (zh) * | 2006-12-22 | 2013-10-02 | 索维索莱克西斯公开有限公司 | 干燥条件下操作燃料电池的方法 |
| CN101020758B (zh) * | 2007-02-25 | 2010-05-19 | 山东东岳神舟新材料有限公司 | 一种聚合物离子交换膜及其制备方法 |
-
2010
- 2010-06-10 CN CN201910500316.XA patent/CN110272512A/zh active Pending
- 2010-06-10 JP JP2012514476A patent/JP5575885B2/ja active Active
- 2010-06-10 WO PCT/EP2010/058182 patent/WO2010142772A1/en not_active Ceased
- 2010-06-10 US US13/376,641 patent/US9450262B2/en active Active
- 2010-06-10 CN CN201080025899.2A patent/CN102459361B/zh active Active
- 2010-06-10 EP EP10725124.1A patent/EP2440586B1/en active Active
- 2010-06-10 KR KR1020117030673A patent/KR101740746B1/ko active Active
-
2016
- 2016-08-16 US US15/238,385 patent/US9947952B2/en active Active
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