JP2010083902A5 - - Google Patents
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- Publication number
- JP2010083902A5 JP2010083902A5 JP2010011440A JP2010011440A JP2010083902A5 JP 2010083902 A5 JP2010083902 A5 JP 2010083902A5 JP 2010011440 A JP2010011440 A JP 2010011440A JP 2010011440 A JP2010011440 A JP 2010011440A JP 2010083902 A5 JP2010083902 A5 JP 2010083902A5
- Authority
- JP
- Japan
- Prior art keywords
- group
- carbon atoms
- alkyl
- replaced
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 125000004432 carbon atom Chemical group C* 0.000 claims 13
- 238000000034 method Methods 0.000 claims 12
- 125000000217 alkyl group Chemical group 0.000 claims 10
- 238000006069 Suzuki reaction reaction Methods 0.000 claims 7
- 238000006243 chemical reaction Methods 0.000 claims 7
- -1 piperidine-1,4-diyl Chemical group 0.000 claims 6
- 125000003118 aryl group Chemical group 0.000 claims 5
- 229910052801 chlorine Inorganic materials 0.000 claims 5
- 150000001923 cyclic compounds Chemical class 0.000 claims 5
- 229910052731 fluorine Inorganic materials 0.000 claims 5
- 125000003342 alkenyl group Chemical group 0.000 claims 4
- 229910052794 bromium Inorganic materials 0.000 claims 4
- 150000001875 compounds Chemical class 0.000 claims 4
- 229910052736 halogen Inorganic materials 0.000 claims 4
- 150000002367 halogens Chemical class 0.000 claims 4
- 229910052739 hydrogen Inorganic materials 0.000 claims 4
- ZADPBFCGQRWHPN-UHFFFAOYSA-N boronic acid Chemical compound OBO ZADPBFCGQRWHPN-UHFFFAOYSA-N 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 3
- 238000005828 desilylation reaction Methods 0.000 claims 3
- 150000002148 esters Chemical class 0.000 claims 3
- 229910052740 iodine Inorganic materials 0.000 claims 3
- 239000002904 solvent Substances 0.000 claims 3
- 239000000758 substrate Substances 0.000 claims 3
- KWKAKUADMBZCLK-UHFFFAOYSA-N 1-octene Chemical group CCCCCCC=C KWKAKUADMBZCLK-UHFFFAOYSA-N 0.000 claims 2
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 2
- MZRVEZGGRBJDDB-UHFFFAOYSA-N N-Butyllithium Chemical compound [Li]CCCC MZRVEZGGRBJDDB-UHFFFAOYSA-N 0.000 claims 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims 2
- 125000002252 acyl group Chemical group 0.000 claims 2
- 125000003545 alkoxy group Chemical group 0.000 claims 2
- 125000000304 alkynyl group Chemical group 0.000 claims 2
- XJHCXCQVJFPJIK-UHFFFAOYSA-M caesium fluoride Chemical compound [F-].[Cs+] XJHCXCQVJFPJIK-UHFFFAOYSA-M 0.000 claims 2
- 229910052799 carbon Inorganic materials 0.000 claims 2
- 125000006297 carbonyl amino group Chemical group [H]N([*:2])C([*:1])=O 0.000 claims 2
- 125000005842 heteroatom Chemical group 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- 125000000896 monocarboxylic acid group Chemical group 0.000 claims 2
- YJVFFLUZDVXJQI-UHFFFAOYSA-L palladium(ii) acetate Chemical compound [Pd+2].CC([O-])=O.CC([O-])=O YJVFFLUZDVXJQI-UHFFFAOYSA-L 0.000 claims 2
- 125000005407 trans-1,4-cyclohexylene group Chemical group [H]C1([H])C([H])([H])[C@]([H])([*:2])C([H])([H])C([H])([H])[C@@]1([H])[*:1] 0.000 claims 2
- 125000004642 (C1-C12) alkoxy group Chemical group 0.000 claims 1
- 125000006710 (C2-C12) alkenyl group Chemical group 0.000 claims 1
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 claims 1
- UCCUXODGPMAHRL-UHFFFAOYSA-N 1-bromo-4-iodobenzene Chemical compound BrC1=CC=C(I)C=C1 UCCUXODGPMAHRL-UHFFFAOYSA-N 0.000 claims 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 1
- QZRGKCOWNLSUDK-UHFFFAOYSA-N Iodochlorine Chemical compound ICl QZRGKCOWNLSUDK-UHFFFAOYSA-N 0.000 claims 1
- RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 claims 1
- 229910001863 barium hydroxide Inorganic materials 0.000 claims 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims 1
- 239000013078 crystal Substances 0.000 claims 1
- 125000004122 cyclic group Chemical group 0.000 claims 1
- 238000007324 demetalation reaction Methods 0.000 claims 1
- 239000012467 final product Substances 0.000 claims 1
- 150000004673 fluoride salts Chemical class 0.000 claims 1
- 239000011737 fluorine Substances 0.000 claims 1
- 150000004679 hydroxides Chemical class 0.000 claims 1
- 239000013067 intermediate product Substances 0.000 claims 1
- 239000012336 iodinating agent Substances 0.000 claims 1
- 230000002083 iodinating effect Effects 0.000 claims 1
- 238000002414 normal-phase solid-phase extraction Methods 0.000 claims 1
- UUEVFMOUBSLVJW-UHFFFAOYSA-N oxo-[[1-[2-[2-[2-[4-(oxoazaniumylmethylidene)pyridin-1-yl]ethoxy]ethoxy]ethyl]pyridin-4-ylidene]methyl]azanium;dibromide Chemical compound [Br-].[Br-].C1=CC(=C[NH+]=O)C=CN1CCOCCOCCN1C=CC(=C[NH+]=O)C=C1 UUEVFMOUBSLVJW-UHFFFAOYSA-N 0.000 claims 1
- 229910052763 palladium Inorganic materials 0.000 claims 1
- 239000002798 polar solvent Substances 0.000 claims 1
- 238000000746 purification Methods 0.000 claims 1
- 238000001953 recrystallisation Methods 0.000 claims 1
- 238000001308 synthesis method Methods 0.000 claims 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10211597.4 | 2002-03-15 | ||
| DE10211597A DE10211597A1 (de) | 2002-03-15 | 2002-03-15 | Verfahren zur Herstellung von Ringverbindungen |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003069260A Division JP5461751B2 (ja) | 2002-03-15 | 2003-03-14 | 環状化合物の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010083902A JP2010083902A (ja) | 2010-04-15 |
| JP2010083902A5 true JP2010083902A5 (enExample) | 2011-09-01 |
| JP5642396B2 JP5642396B2 (ja) | 2014-12-17 |
Family
ID=27771362
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003069260A Expired - Fee Related JP5461751B2 (ja) | 2002-03-15 | 2003-03-14 | 環状化合物の製造方法 |
| JP2010011440A Expired - Fee Related JP5642396B2 (ja) | 2002-03-15 | 2010-01-21 | 環状化合物の製造方法 |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003069260A Expired - Fee Related JP5461751B2 (ja) | 2002-03-15 | 2003-03-14 | 環状化合物の製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (6) | US7183447B2 (enExample) |
| EP (3) | EP2103589A1 (enExample) |
| JP (2) | JP5461751B2 (enExample) |
| KR (3) | KR101017375B1 (enExample) |
| DE (1) | DE10211597A1 (enExample) |
| TW (3) | TWI350831B (enExample) |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7067179B1 (en) * | 1999-08-03 | 2006-06-27 | Dainippon Ink And Chemicals, Inc. | Fused ring compound |
| ES2299561T3 (es) * | 2001-01-26 | 2008-06-01 | Btg International Limited | Analogo de bencilamina. |
| GB0126844D0 (en) * | 2001-11-08 | 2002-01-02 | Qinetiq Ltd | Novel compounds |
| DE10211597A1 (de) | 2002-03-15 | 2003-10-02 | Merck Patent Gmbh | Verfahren zur Herstellung von Ringverbindungen |
| WO2005123879A1 (de) | 2004-06-18 | 2005-12-29 | Merck Patent Gmbh | Flüssigkristallines medium |
| ATE517967T1 (de) * | 2004-06-18 | 2011-08-15 | Merck Patent Gmbh | Flüssigkristallines medium |
| WO2006053628A1 (en) * | 2004-11-20 | 2006-05-26 | Merck Patent Gmbh | Liquid crystal compounds, liquid crystal medium and liquid crystal display |
| CN101090955B (zh) * | 2005-01-13 | 2010-10-13 | Lg化学株式会社 | 包含新的含硅化合物的液晶组合物及使用该液晶组合物的液晶显示器 |
| CN101090954B (zh) | 2005-01-13 | 2010-10-13 | Lg化学株式会社 | 包含新的含硅化合物的液晶组合物及使用该液晶组合物的液晶显示器 |
| JP4740615B2 (ja) * | 2005-03-10 | 2011-08-03 | マナック株式会社 | ｐ−クォーターフェニルの製造方法 |
| DE502006004279D1 (de) * | 2005-05-21 | 2009-09-03 | Merck Patent Gmbh | Flüssigkristallines Medium |
| ATE417910T1 (de) * | 2005-05-25 | 2009-01-15 | Merck Patent Gmbh | Flüssigkristallines medium und flüssigkristallanzeige |
| TW200740823A (en) * | 2005-08-01 | 2007-11-01 | Ihara Chemical Ind Co | Oxadiazole-substituted Sym-triindole derivative and organic el element employing the same |
| JO3598B1 (ar) | 2006-10-10 | 2020-07-05 | Infinity Discovery Inc | الاحماض والاسترات البورونية كمثبطات اميد هيدروليز الحامض الدهني |
| ATE525448T1 (de) | 2006-10-12 | 2011-10-15 | Merck Patent Gmbh | Flüssigkristallines medium |
| CN101868439B (zh) * | 2007-09-06 | 2014-02-05 | Jnc株式会社 | 具有侧向氟的4、5环液晶性化合物、液晶组成物以及液晶显示元件 |
| EP2075601A1 (de) * | 2007-12-24 | 2009-07-01 | Lofo High Tech Film GmbH | Optische Kompensationsfolien für Flüssigkristallanzeigen und damit zusammenhängende Erfindungen |
| WO2009126691A1 (en) * | 2008-04-09 | 2009-10-15 | Infinity Pharmaceuticals, Inc | Inhibitors of fatty acid amide hydrolase |
| KR20110067129A (ko) | 2008-09-17 | 2011-06-21 | 테트라곤 엘체 케미 아게 | 키랄 화합물, 이들 키랄 화합물을 포함하는 콜레스테릭 및 강유전성 액정 조성물, 및 이들 액정 조성물을 포함하는 액정 디스플레이 |
| US8501285B2 (en) * | 2008-11-19 | 2013-08-06 | Jnc Corporation | Optically isotropic liquid crystal medium and optical device |
| TWI458811B (zh) | 2009-01-16 | 2014-11-01 | Jnc Corp | 液晶性化合物、液晶組成物以及液晶顯示元件 |
| EP2417115A4 (en) | 2009-04-07 | 2012-10-31 | Infinity Pharmaceuticals Inc | FATTY ACID AMIDE HYDROLASE INHIBITORS |
| WO2010118155A1 (en) | 2009-04-07 | 2010-10-14 | Infinity Pharmaceuticals, Inc. | Inhibitors of fatty acid amide hydrolase |
| DE102009034301A1 (de) | 2009-07-21 | 2011-01-27 | Merck Patent Gmbh | Flüssigkristallines Medium und dieses enthaltende Hochfrequenzbauteile |
| TWI458813B (zh) | 2009-09-18 | 2014-11-01 | Jnc Corp | 液晶性化合物、液晶組成物以及液晶顯示元件 |
| MX336742B (es) * | 2010-02-03 | 2016-01-29 | Infinity Pharmaceuticals Inc | Inhibidores de amida hidrolasa de acido graso. |
| JP5672043B2 (ja) | 2010-04-05 | 2015-02-18 | Jnc株式会社 | ５環化合物、液晶組成物および液晶表示素子 |
| DE102010025572A1 (de) | 2010-06-30 | 2012-01-05 | Merck Patent Gmbh | Flüssigkristallines Medium und dieses enthaltende Hochfrequenzbauteile |
| JP5887713B2 (ja) | 2011-05-10 | 2016-03-16 | Jnc株式会社 | フルオロビニル誘導体、液晶組成物及び液晶表示素子 |
| PT2725903T (pt) * | 2011-06-30 | 2020-06-30 | Dow Agrosciences Llc | 3-alcoxi-, tioalquil- e amino-4-aminopicolinatos 6-substituídos e sua utilização como herbicidas |
| CN102965123A (zh) * | 2012-11-15 | 2013-03-13 | 深圳市华星光电技术有限公司 | 液晶添加剂及其液晶组合物与液晶面板 |
| JP6146072B2 (ja) * | 2013-03-19 | 2017-06-14 | Jnc株式会社 | 液晶組成物および液晶表示素子 |
| US20160194561A1 (en) * | 2013-05-31 | 2016-07-07 | Dic Corporation | Difluorophenyl liquid crystal composition |
| DE102014015267A1 (de) | 2014-10-16 | 2016-04-21 | Merck Patent Gmbh | Substituierte Polyphenyle |
| RU2633578C2 (ru) | 2015-08-19 | 2017-10-13 | Самсунг Электроникс Ко., Лтд. | Мезогенные соединения, жидкокристаллические композиции, содержащие эти соединения, и устройства для высокочастотной техники |
| US11078528B2 (en) | 2015-10-12 | 2021-08-03 | Advanced Cell Diagnostics, Inc. | In situ detection of nucleotide variants in high noise samples, and compositions and methods related thereto |
| CN105348308B (zh) * | 2015-10-13 | 2017-04-19 | 东莞理工学院 | 一种中位含芴桥联的双氟化硼络合二吡咯甲川衍生物及其制备方法 |
| CN109082280B (zh) * | 2018-11-05 | 2020-07-28 | 宁夏中星显示材料有限公司 | 一种液晶材料的制备方法 |
Family Cites Families (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4841009A (en) * | 1982-12-28 | 1989-06-20 | Amoco Corporation | Substantially linear monomeric composition and liquid crystal polymeric compositions derived therefrom |
| EP0329752B1 (en) * | 1987-09-09 | 1993-03-17 | MERCK PATENT GmbH | Fluorinated oligophenyls and their use in liquid crystal materials |
| JP2782444B2 (ja) * | 1987-09-09 | 1998-07-30 | メルク・パテント・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング | フツ素化オリゴフエニル化合物および液晶材料におけるそれらの使用 |
| DE3807862A1 (de) * | 1988-03-10 | 1989-09-21 | Merck Patent Gmbh | Smektische fluessigkristallphase |
| US5273680A (en) * | 1988-03-10 | 1993-12-28 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Fluorinated oligophenyls and their use in liquid crystal materials |
| GB8819387D0 (en) * | 1988-08-15 | 1988-09-14 | Merck Patent Gmbh | Liquid crystal display devices & liquid crystal medium to be used therein |
| YU245190A (sh) * | 1989-10-02 | 1992-07-20 | Merck Patent Gesellschaft Mit Beschraenkter Haftung | Elektrooptički tečni kristali |
| GB2240778B (en) * | 1990-02-07 | 1993-09-01 | Merck Patent Gmbh | Fluorinated terphenyls |
| GB9017482D0 (en) * | 1990-08-09 | 1990-09-26 | Ici Plc | Manufacturing process |
| DE59206518D1 (de) * | 1991-02-25 | 1996-07-18 | Hoffmann La Roche | Flüssigkristalline Verbindungen mit endständigem 1-Alkinylrest |
| DE4220082C2 (de) * | 1992-06-19 | 1994-09-15 | Merck Patent Gmbh | Verfahren zur Kreuzkopplung von Boronsäuren mit Halogenverbindungen |
| JP3268658B2 (ja) * | 1992-08-26 | 2002-03-25 | 旭硝子株式会社 | 含フッ素ｐ−ターフェニル誘導体およびその製造方法 |
| DE4338348B4 (de) * | 1992-11-19 | 2006-05-11 | Merck Patent Gmbh | 2,6-Disubstituierte Benzotrifluoride |
| JPH0881416A (ja) * | 1994-07-11 | 1996-03-26 | Seiko Epson Corp | クォターフェニル誘導体及びそれを用いた高分子分散型液晶表示素子 |
| EP0730019A4 (en) * | 1994-07-15 | 1996-12-18 | Seiko Epson Corp | LIQUID CRYSTAL COMPOSITION AND LIQUID CRYSTAL DISPLAY ELEMENT PRODUCED THEREFROM |
| DE4426671A1 (de) * | 1994-07-28 | 1996-02-01 | Hoechst Ag | Verfahren zur Kreuzkupplung von aromatischen Borverbindungen mit aromatischen Halogenverbindungen oder Perfluoralkylsulfonaten |
| JP3702426B2 (ja) * | 1994-08-03 | 2005-10-05 | 関東化学株式会社 | トリフルオロメチルベンゼン誘導体および液晶組成物 |
| WO1997005151A1 (de) * | 1995-07-25 | 1997-02-13 | Clariant Gmbh | Katalysatoren zur durchführung von kreuzkupplungsreaktionen |
| EP0959060A1 (en) * | 1996-11-28 | 1999-11-24 | Chisso Corporation | Chlorobenzene derivatives, liquid-crystal composition, and liquid-crystal display elements |
| CA2285455A1 (en) * | 1997-04-09 | 1998-10-15 | Sebastian Mario Marcuccio | Process for covalently coupling organic compounds utilizing diboron derivatives |
| GB2329391A (en) * | 1997-09-17 | 1999-03-24 | Sharp Kk | Liquid crystal composition containing fluorinated phenylpyrimidines with SmC phase and fluorinated terphenyl(s), and use thereof in a liquid crystal shutter |
| US6307087B1 (en) * | 1998-07-10 | 2001-10-23 | Massachusetts Institute Of Technology | Ligands for metals and improved metal-catalyzed processes based thereon |
| DE19933175B4 (de) * | 1998-07-17 | 2008-04-30 | Merck Patent Gmbh | Schwefelpentalfurorid-Derivate und Verwendung für ein flüssigkristallines Medium |
| DE19858594A1 (de) * | 1998-12-18 | 2000-06-21 | Merck Patent Gmbh | Verfahren zur Herstellung von Cyanbenzolboronsäuren |
| GB2367058B (en) * | 2000-07-12 | 2004-07-14 | Merck Patent Gmbh | Acetylene derivatives and liquid-crystalline medium |
| JP4972826B2 (ja) * | 2001-04-10 | 2012-07-11 | Ｊｎｃ株式会社 | ジフルオロアルコキシを末端に有する化合物、液晶組成物および液晶表示素子 |
| DE10211597A1 (de) | 2002-03-15 | 2003-10-02 | Merck Patent Gmbh | Verfahren zur Herstellung von Ringverbindungen |
| JP4206687B2 (ja) * | 2002-04-09 | 2009-01-14 | チッソ株式会社 | 液晶組成物および液晶表示素子 |
-
2002
- 2002-03-15 DE DE10211597A patent/DE10211597A1/de not_active Withdrawn
-
2003
- 2003-02-20 EP EP08010867A patent/EP2103589A1/de not_active Withdrawn
- 2003-02-20 EP EP03003811A patent/EP1346995A1/de not_active Withdrawn
- 2003-02-20 EP EP10010446A patent/EP2332944A3/de not_active Ceased
- 2003-03-11 TW TW099139032A patent/TWI350831B/zh not_active IP Right Cessation
- 2003-03-11 TW TW100127541A patent/TWI370811B/zh not_active IP Right Cessation
- 2003-03-11 TW TW092105237A patent/TWI337989B/zh not_active IP Right Cessation
- 2003-03-14 JP JP2003069260A patent/JP5461751B2/ja not_active Expired - Fee Related
- 2003-03-14 KR KR1020030016038A patent/KR101017375B1/ko not_active Expired - Fee Related
- 2003-03-17 US US10/388,607 patent/US7183447B2/en not_active Expired - Fee Related
-
2006
- 2006-05-22 US US11/437,608 patent/US7411100B2/en not_active Expired - Fee Related
-
2008
- 2008-08-08 US US12/188,288 patent/US7786332B2/en not_active Expired - Fee Related
-
2009
- 2009-05-22 US US12/470,605 patent/US7842845B2/en not_active Expired - Fee Related
-
2010
- 2010-01-21 JP JP2010011440A patent/JP5642396B2/ja not_active Expired - Fee Related
- 2010-10-19 US US12/907,612 patent/US8124817B2/en not_active Expired - Fee Related
- 2010-10-25 KR KR1020100103828A patent/KR101085502B1/ko not_active Expired - Fee Related
-
2011
- 2011-07-19 KR KR1020110071391A patent/KR101186241B1/ko not_active Expired - Fee Related
-
2012
- 2012-02-16 US US13/398,367 patent/US8350100B2/en not_active Expired - Fee Related
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