JP2009541334A5 - - Google Patents
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- Publication number
- JP2009541334A5 JP2009541334A5 JP2009516618A JP2009516618A JP2009541334A5 JP 2009541334 A5 JP2009541334 A5 JP 2009541334A5 JP 2009516618 A JP2009516618 A JP 2009516618A JP 2009516618 A JP2009516618 A JP 2009516618A JP 2009541334 A5 JP2009541334 A5 JP 2009541334A5
- Authority
- JP
- Japan
- Prior art keywords
- rebaudioside
- solution
- composition
- substantially pure
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000001512 FEMA 4601 Substances 0.000 claims 73
- HELXLJCILKEWJH-SEAGSNCFSA-N Rebaudioside A Natural products O=C(O[C@H]1[C@@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)[C@@]1(C)[C@@H]2[C@](C)([C@H]3[C@@]4(CC(=C)[C@@](O[C@H]5[C@H](O[C@H]6[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O6)[C@@H](O[C@H]6[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O6)[C@H](O)[C@@H](CO)O5)(C4)CC3)CC2)CCC1 HELXLJCILKEWJH-SEAGSNCFSA-N 0.000 claims 73
- HELXLJCILKEWJH-UHFFFAOYSA-N entered according to Sigma 01432 Natural products C1CC2C3(C)CCCC(C)(C(=O)OC4C(C(O)C(O)C(CO)O4)O)C3CCC2(C2)CC(=C)C21OC(C1OC2C(C(O)C(O)C(CO)O2)O)OC(CO)C(O)C1OC1OC(CO)C(O)C(O)C1O HELXLJCILKEWJH-UHFFFAOYSA-N 0.000 claims 73
- HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 claims 73
- 235000019203 rebaudioside A Nutrition 0.000 claims 73
- 238000000034 method Methods 0.000 claims 36
- 239000000203 mixture Substances 0.000 claims 30
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 24
- 239000000243 solution Substances 0.000 claims 24
- 239000002152 aqueous-organic solution Substances 0.000 claims 12
- 238000010438 heat treatment Methods 0.000 claims 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 9
- 238000001816 cooling Methods 0.000 claims 6
- 238000002441 X-ray diffraction Methods 0.000 claims 5
- 238000001035 drying Methods 0.000 claims 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims 3
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 claims 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims 3
- 238000010992 reflux Methods 0.000 claims 3
- 238000005406 washing Methods 0.000 claims 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 2
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 claims 2
- 238000002425 crystallisation Methods 0.000 claims 2
- 230000008025 crystallization Effects 0.000 claims 2
- 238000002156 mixing Methods 0.000 claims 2
- RPYRMTHVSUWHSV-CUZJHZIBSA-N rebaudioside D Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O RPYRMTHVSUWHSV-CUZJHZIBSA-N 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- GIPHUOWOTCAJSR-UHFFFAOYSA-N Rebaudioside A. Natural products C1CC2C3(C)CCCC(C)(C(=O)OC4C(C(O)C(O)C(CO)O4)O)C3CCC2(C2)CC(=C)C21OC1OC(CO)C(O)C(O)C1OC(C1O)OC(CO)C(O)C1OC1OC(CO)C(O)C(O)C1O GIPHUOWOTCAJSR-UHFFFAOYSA-N 0.000 claims 1
- 239000003125 aqueous solvent Substances 0.000 claims 1
- 238000000498 ball milling Methods 0.000 claims 1
- 238000004108 freeze drying Methods 0.000 claims 1
- 238000000227 grinding Methods 0.000 claims 1
- 239000012535 impurity Substances 0.000 claims 1
- 238000010899 nucleation Methods 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 238000001556 precipitation Methods 0.000 claims 1
- 239000012453 solvate Substances 0.000 claims 1
- 238000001694 spray drying Methods 0.000 claims 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US80521606P | 2006-06-19 | 2006-06-19 | |
| US60/805,216 | 2006-06-19 | ||
| US88931807P | 2007-02-12 | 2007-02-12 | |
| US60/889,318 | 2007-02-12 | ||
| PCT/US2007/069548 WO2007149672A2 (en) | 2006-06-19 | 2007-05-23 | Rebaudioside a composition and method for purifying rebaudioside a |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009541334A JP2009541334A (ja) | 2009-11-26 |
| JP2009541334A5 true JP2009541334A5 (OSRAM) | 2010-07-08 |
| JP5536449B2 JP5536449B2 (ja) | 2014-07-02 |
Family
ID=38834209
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009516618A Active JP5536449B2 (ja) | 2006-06-19 | 2007-05-23 | レバウディオシドａ組成物及びレバウディオシドａを精製するための方法 |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US8791253B2 (OSRAM) |
| EP (1) | EP2037761B1 (OSRAM) |
| JP (1) | JP5536449B2 (OSRAM) |
| KR (1) | KR101494374B1 (OSRAM) |
| AP (1) | AP2008004716A0 (OSRAM) |
| AR (1) | AR061516A1 (OSRAM) |
| AU (1) | AU2007261243B2 (OSRAM) |
| BR (1) | BRPI0713127A2 (OSRAM) |
| CA (1) | CA2655440C (OSRAM) |
| CL (1) | CL2007001753A1 (OSRAM) |
| MX (1) | MX2008016334A (OSRAM) |
| NZ (1) | NZ597210A (OSRAM) |
| RU (1) | RU2438353C2 (OSRAM) |
| TW (1) | TWI419651B (OSRAM) |
| UY (1) | UY30388A1 (OSRAM) |
| WO (1) | WO2007149672A2 (OSRAM) |
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|---|---|---|---|---|
| US7943185B1 (en) | 2007-03-16 | 2011-05-17 | Pom Wonderful, Llc | Method and composition for producing a stable and deodorized form of pomegranate seed oil |
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| US9386797B2 (en) | 2011-02-17 | 2016-07-12 | Purecircle Sdn Bhd | Glucosyl stevia composition |
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| US8790730B2 (en) | 2005-10-11 | 2014-07-29 | Purecircle Usa | Process for manufacturing a sweetener and use thereof |
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| US8017168B2 (en) | 2006-11-02 | 2011-09-13 | The Coca-Cola Company | High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith |
| CN101200480B (zh) * | 2006-12-15 | 2011-03-30 | 成都华高药业有限公司 | 莱鲍迪甙a的提取方法 |
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| US8889199B1 (en) | 2007-02-07 | 2014-11-18 | Pom Wonderful Llc | Method and composition for producing a stable and deodorized form of pomegranate seed oil |
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| US8277861B2 (en) | 2007-03-14 | 2012-10-02 | Concentrate Manufacturing Company Of Ireland | Beverage products having steviol glycosides and at least one acid |
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-
2007
- 2007-05-21 US US11/751,627 patent/US8791253B2/en active Active
- 2007-05-23 KR KR1020097000860A patent/KR101494374B1/ko not_active Expired - Fee Related
- 2007-05-23 AP AP2008004716A patent/AP2008004716A0/xx unknown
- 2007-05-23 NZ NZ597210A patent/NZ597210A/xx not_active IP Right Cessation
- 2007-05-23 MX MX2008016334A patent/MX2008016334A/es active IP Right Grant
- 2007-05-23 WO PCT/US2007/069548 patent/WO2007149672A2/en not_active Ceased
- 2007-05-23 JP JP2009516618A patent/JP5536449B2/ja active Active
- 2007-05-23 EP EP07797688.4A patent/EP2037761B1/en active Active
- 2007-05-23 AU AU2007261243A patent/AU2007261243B2/en not_active Ceased
- 2007-05-23 CA CA2655440A patent/CA2655440C/en active Active
- 2007-05-23 BR BRPI0713127-5A patent/BRPI0713127A2/pt not_active IP Right Cessation
- 2007-05-23 RU RU2008149916/13A patent/RU2438353C2/ru active
- 2007-06-04 TW TW096119975A patent/TWI419651B/zh not_active IP Right Cessation
- 2007-06-05 UY UY30388A patent/UY30388A1/es not_active Application Discontinuation
- 2007-06-15 CL CL200701753A patent/CL2007001753A1/es unknown
- 2007-06-19 AR ARP070102681A patent/AR061516A1/es unknown
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