JPS56121455A - Separation of stevioside and rebaudioside a by crystallization - Google Patents

Separation of stevioside and rebaudioside a by crystallization

Info

Publication number
JPS56121455A
JPS56121455A JP2375780A JP2375780A JPS56121455A JP S56121455 A JPS56121455 A JP S56121455A JP 2375780 A JP2375780 A JP 2375780A JP 2375780 A JP2375780 A JP 2375780A JP S56121455 A JPS56121455 A JP S56121455A
Authority
JP
Japan
Prior art keywords
stevioside
rebaudioside
crystallization
separation
methanol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2375780A
Other languages
Japanese (ja)
Inventor
Katsunobu Matsushita
Toshio Kitahara
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ajinomoto Co Inc
Original Assignee
Ajinomoto Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ajinomoto Co Inc filed Critical Ajinomoto Co Inc
Priority to JP2375780A priority Critical patent/JPS56121455A/en
Publication of JPS56121455A publication Critical patent/JPS56121455A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE: To separate stevioside and rebaudioside A, in high purity and yield, by crystallization taking advantage of the solubility difference of both compounds in an aqueous solution of methanol.
CONSTITUTION: A mixture of stevioside and rebaudioside A extracted from the leaves and stalks of Stevia rebaudiana Bertoni by conventional process, is dissolved in a 40W70% or ≥85% aqueous solution of methanol, and stevioside is selectively crystallized from the solution.
COPYRIGHT: (C)1981,JPO&Japio
JP2375780A 1980-02-27 1980-02-27 Separation of stevioside and rebaudioside a by crystallization Pending JPS56121455A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2375780A JPS56121455A (en) 1980-02-27 1980-02-27 Separation of stevioside and rebaudioside a by crystallization

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2375780A JPS56121455A (en) 1980-02-27 1980-02-27 Separation of stevioside and rebaudioside a by crystallization

Publications (1)

Publication Number Publication Date
JPS56121455A true JPS56121455A (en) 1981-09-24

Family

ID=12119192

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2375780A Pending JPS56121455A (en) 1980-02-27 1980-02-27 Separation of stevioside and rebaudioside a by crystallization

Country Status (1)

Country Link
JP (1) JPS56121455A (en)

Cited By (58)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6075252A (en) * 1983-09-30 1985-04-27 Sekisui Chem Co Ltd Low-calorie sweetener composition
US5962678A (en) * 1996-09-13 1999-10-05 Alberta Research Council Method of extracting selected sweet glycosides from the Stevia rebaudiana plant
WO2007149672A3 (en) * 2006-06-19 2008-04-10 Coca Cola Co Rebaudioside a composition and method for purifying rebaudioside a
WO2008091547A2 (en) 2007-01-22 2008-07-31 Cargill, Incorporated Method of producing purified rebaudioside a compositions using solvent/antisolvent crystallization
WO2011016558A1 (en) * 2009-08-06 2011-02-10 丸大食品株式会社 Method for producing glucosylceramide-containing material
US8017168B2 (en) 2006-11-02 2011-09-13 The Coca-Cola Company High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith
US8030481B2 (en) 2007-05-21 2011-10-04 The Coca-Cola Company Stevioside polymorphic and amorphous forms, methods for their formulation, and uses
US8257948B1 (en) 2011-02-17 2012-09-04 Purecircle Usa Method of preparing alpha-glucosyl Stevia composition
US8299224B2 (en) 2009-10-15 2012-10-30 Purecircle Sdn Bhd High-purity Rebaudioside D
US8318459B2 (en) 2011-02-17 2012-11-27 Purecircle Usa Glucosyl stevia composition
US8334006B2 (en) 2005-10-11 2012-12-18 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8337927B2 (en) 2005-10-11 2012-12-25 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8414952B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie diet cookies containing the same
US8414948B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie ice cream containing the same
US8414951B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie soy sauce containing the same
US8414949B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie yogurt containing the same
US8414950B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie table top tablet containing the same
US8420146B2 (en) 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie bread containing the same
US8420147B2 (en) 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie cake containing the same
US8507022B2 (en) 2009-10-15 2013-08-13 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same
US8512790B2 (en) 2009-10-15 2013-08-20 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie chocolate containing the same
US8568818B2 (en) 2009-10-15 2013-10-29 Pure Circle Sdn Bhd High-purity Rebaudioside D and low-calorie carbonated drink containing the same
US8574656B2 (en) 2009-10-15 2013-11-05 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie fruit juice containing the same
EP2708548A2 (en) 2009-10-15 2014-03-19 Purecircle SDN BHD High-Purity Rebaudioside D and Applications
US8790730B2 (en) 2005-10-11 2014-07-29 Purecircle Usa Process for manufacturing a sweetener and use thereof
US8916138B2 (en) 2009-10-15 2014-12-23 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie tooth paste composition containing the same
US9012626B2 (en) 2006-06-19 2015-04-21 The Coca-Cola Company Rebaudioside a composition and method for purifying rebaudioside a
US9101160B2 (en) 2005-11-23 2015-08-11 The Coca-Cola Company Condiments with high-potency sweetener
US9131718B2 (en) 2009-06-16 2015-09-15 Epc (Beijing) Natural Products Co., Ltd. Process for rebaudioside D
CN105722533A (en) * 2013-07-12 2016-06-29 可口可乐公司 Compositions and methods for improving rebaudioside M solubility
US9578895B2 (en) 2010-08-23 2017-02-28 Epc (Beijing) Natural Products Co., Ltd. Rebaudioside A and stevioside compositions
US9752174B2 (en) 2013-05-28 2017-09-05 Purecircle Sdn Bhd High-purity steviol glycosides
US9771434B2 (en) 2011-06-23 2017-09-26 Purecircle Sdn Bhd Products from stevia rebaudiana
US9795156B2 (en) 2011-03-17 2017-10-24 E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd Rebaudioside B and derivatives
US9877501B2 (en) 2011-06-03 2018-01-30 Purecircle Sdn Bhd Stevia composition
US9894922B2 (en) 2011-05-18 2018-02-20 Purecircle Sdn Bhd Glucosyl rebaudioside C
US10004245B2 (en) 2009-11-12 2018-06-26 Purecircle Sdn Bhd Granulation of a stevia sweetener
US10021899B2 (en) 2011-05-31 2018-07-17 Purecircle Sdn Bhd Stevia composition
US10264811B2 (en) 2014-05-19 2019-04-23 Epc Natural Products Co., Ltd. Stevia sweetener with improved solubility
US10357052B2 (en) 2014-06-16 2019-07-23 Sweet Green Fields USA LLC Rebaudioside A and stevioside with improved solubilities
US10362797B2 (en) 2011-02-10 2019-07-30 Purecircle Sdn Bhd Stevia composition
US10480019B2 (en) 2011-08-10 2019-11-19 Purecircle Sdn Bhd Process for producing high-purity rubusoside
US10485256B2 (en) 2014-06-20 2019-11-26 Sweet Green Fields International Co., Limited Stevia sweetener with improved solubility with a cyclodextrin
US10485257B2 (en) 2012-05-22 2019-11-26 Purecircle Sdn Bhd Method of making steviol glycosides
US10501817B2 (en) 2010-03-16 2019-12-10 Imperial Sugar Company Process for the manufacture of co-crystallized sucrose natural sweeteners and the products thereof
US10602762B2 (en) 2011-02-17 2020-03-31 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US10696706B2 (en) 2010-03-12 2020-06-30 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
CN111662344A (en) * 2020-06-29 2020-09-15 四川大学 Method for recovering rebaudioside A from primary crystallization mother liquor of stevioside
US10780170B2 (en) 2013-06-07 2020-09-22 Purecircle Sdn Bhd Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10952458B2 (en) 2013-06-07 2021-03-23 Purecircle Usa Inc Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US11202461B2 (en) 2014-09-02 2021-12-21 Purecircle Sdn Bhd Stevia extracts
US11291232B2 (en) 2010-12-13 2022-04-05 Purecircle Sdn Bhd Highly soluble Rebaudioside D
US11464246B2 (en) 2011-09-07 2022-10-11 Purecircle Sdn Bhd Highly soluble Stevia sweetener
US11647771B2 (en) 2015-10-26 2023-05-16 Purecircle Usa Inc. Steviol glycoside compositions
US11653686B2 (en) 2015-12-15 2023-05-23 Purecircle Usa Inc. Steviol glycoside compositions
US11678685B2 (en) 2011-02-17 2023-06-20 Purecircle Sdn Bhd Glucosyl stevia composition
US11690391B2 (en) 2011-02-17 2023-07-04 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US11871771B2 (en) 2011-02-17 2024-01-16 Purecircle Sdn Bhd Glucosyl Stevia composition

Cited By (88)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6075252A (en) * 1983-09-30 1985-04-27 Sekisui Chem Co Ltd Low-calorie sweetener composition
US5962678A (en) * 1996-09-13 1999-10-05 Alberta Research Council Method of extracting selected sweet glycosides from the Stevia rebaudiana plant
US8337927B2 (en) 2005-10-11 2012-12-25 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8334006B2 (en) 2005-10-11 2012-12-18 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8790730B2 (en) 2005-10-11 2014-07-29 Purecircle Usa Process for manufacturing a sweetener and use thereof
US10531683B2 (en) 2005-10-11 2020-01-14 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US9101160B2 (en) 2005-11-23 2015-08-11 The Coca-Cola Company Condiments with high-potency sweetener
US8791253B2 (en) 2006-06-19 2014-07-29 The Coca-Cola Company Rebaudioside A composition and method for purifying rebaudioside A
US9012626B2 (en) 2006-06-19 2015-04-21 The Coca-Cola Company Rebaudioside a composition and method for purifying rebaudioside a
WO2007149672A3 (en) * 2006-06-19 2008-04-10 Coca Cola Co Rebaudioside a composition and method for purifying rebaudioside a
US8017168B2 (en) 2006-11-02 2011-09-13 The Coca-Cola Company High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith
WO2008091547A2 (en) 2007-01-22 2008-07-31 Cargill, Incorporated Method of producing purified rebaudioside a compositions using solvent/antisolvent crystallization
US8937168B2 (en) 2007-01-22 2015-01-20 Cargill, Incorporated Method of producing purified rebaudioside A compositions using solvent/antisolvent crystallization
JP2010516764A (en) * 2007-01-22 2010-05-20 カーギル・インコーポレイテッド Process for the preparation of a purified rebaudioside A composition using solvent / antisolvent crystallization
US8030481B2 (en) 2007-05-21 2011-10-04 The Coca-Cola Company Stevioside polymorphic and amorphous forms, methods for their formulation, and uses
US9131718B2 (en) 2009-06-16 2015-09-15 Epc (Beijing) Natural Products Co., Ltd. Process for rebaudioside D
US9635878B2 (en) 2009-06-16 2017-05-02 Epc (Beijing) Natural Products Co., Ltd. Process for rebaudioside D
WO2011016558A1 (en) * 2009-08-06 2011-02-10 丸大食品株式会社 Method for producing glucosylceramide-containing material
US8507022B2 (en) 2009-10-15 2013-08-13 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same
US8414948B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie ice cream containing the same
US8420146B2 (en) 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie bread containing the same
US8512790B2 (en) 2009-10-15 2013-08-20 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie chocolate containing the same
US8568818B2 (en) 2009-10-15 2013-10-29 Pure Circle Sdn Bhd High-purity Rebaudioside D and low-calorie carbonated drink containing the same
US8574656B2 (en) 2009-10-15 2013-11-05 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie fruit juice containing the same
EP2708548A2 (en) 2009-10-15 2014-03-19 Purecircle SDN BHD High-Purity Rebaudioside D and Applications
US8414950B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie table top tablet containing the same
US8414949B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie yogurt containing the same
US8916138B2 (en) 2009-10-15 2014-12-23 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie tooth paste composition containing the same
US8414951B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie soy sauce containing the same
US8420147B2 (en) 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie cake containing the same
US8414952B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie diet cookies containing the same
US8299224B2 (en) 2009-10-15 2012-10-30 Purecircle Sdn Bhd High-purity Rebaudioside D
US10004245B2 (en) 2009-11-12 2018-06-26 Purecircle Sdn Bhd Granulation of a stevia sweetener
US11155570B2 (en) 2010-03-12 2021-10-26 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
US11773125B2 (en) 2010-03-12 2023-10-03 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
US10696706B2 (en) 2010-03-12 2020-06-30 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
US10501817B2 (en) 2010-03-16 2019-12-10 Imperial Sugar Company Process for the manufacture of co-crystallized sucrose natural sweeteners and the products thereof
US11202462B2 (en) 2010-08-23 2021-12-21 Sweet Green Fields International Co., Limited Rebaudioside A and stevioside compositions
US9578895B2 (en) 2010-08-23 2017-02-28 Epc (Beijing) Natural Products Co., Ltd. Rebaudioside A and stevioside compositions
US10285425B2 (en) 2010-08-23 2019-05-14 Epc Natural Products Co. Ltd Rebaudioside A and stevioside compositions
US11291232B2 (en) 2010-12-13 2022-04-05 Purecircle Sdn Bhd Highly soluble Rebaudioside D
US11950611B2 (en) 2010-12-13 2024-04-09 Purecircle Sdn Bhd Highly soluble Rebaudioside D
US11856974B2 (en) 2011-02-10 2024-01-02 Purecircle Sdn Bhd Highly soluble stevia sweetener
US10362797B2 (en) 2011-02-10 2019-07-30 Purecircle Sdn Bhd Stevia composition
US11812771B2 (en) 2011-02-10 2023-11-14 Purecircle Sdn Bhd Stevia composition
US10602762B2 (en) 2011-02-17 2020-03-31 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US11678685B2 (en) 2011-02-17 2023-06-20 Purecircle Sdn Bhd Glucosyl stevia composition
US8257948B1 (en) 2011-02-17 2012-09-04 Purecircle Usa Method of preparing alpha-glucosyl Stevia composition
US11690391B2 (en) 2011-02-17 2023-07-04 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US11229228B2 (en) 2011-02-17 2022-01-25 Purecircle Sdn Bhd Glucosyl stevia composition
US8318459B2 (en) 2011-02-17 2012-11-27 Purecircle Usa Glucosyl stevia composition
US9615599B2 (en) 2011-02-17 2017-04-11 Purecircle Sdn Bhd Glucosyl stevia composition
US11871771B2 (en) 2011-02-17 2024-01-16 Purecircle Sdn Bhd Glucosyl Stevia composition
US10743572B2 (en) 2011-02-17 2020-08-18 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US9795156B2 (en) 2011-03-17 2017-10-24 E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd Rebaudioside B and derivatives
US11510428B2 (en) 2011-03-17 2022-11-29 Sweet Green Fields International Co., Limited Rebaudioside B and derivatives
US9894922B2 (en) 2011-05-18 2018-02-20 Purecircle Sdn Bhd Glucosyl rebaudioside C
US11950610B2 (en) 2011-05-18 2024-04-09 Purecircle Sdn Bhd Glucosyl Rebaudioside C
US11712055B2 (en) 2011-05-31 2023-08-01 Purecircle Sdn Bhd Stevia composition
US10021899B2 (en) 2011-05-31 2018-07-17 Purecircle Sdn Bhd Stevia composition
US9877501B2 (en) 2011-06-03 2018-01-30 Purecircle Sdn Bhd Stevia composition
US11825867B2 (en) 2011-06-03 2023-11-28 Purecircle Sdn Bhd Stevia composition
US11279773B2 (en) 2011-06-23 2022-03-22 Purecircle Sdn Bhd Products from Stevia rabaudiana
US9771434B2 (en) 2011-06-23 2017-09-26 Purecircle Sdn Bhd Products from stevia rebaudiana
US10480019B2 (en) 2011-08-10 2019-11-19 Purecircle Sdn Bhd Process for producing high-purity rubusoside
US11464246B2 (en) 2011-09-07 2022-10-11 Purecircle Sdn Bhd Highly soluble Stevia sweetener
US10485257B2 (en) 2012-05-22 2019-11-26 Purecircle Sdn Bhd Method of making steviol glycosides
US11542537B2 (en) 2012-05-22 2023-01-03 Purecircle Sdn Bhd High-purity steviol glycosides
US9752174B2 (en) 2013-05-28 2017-09-05 Purecircle Sdn Bhd High-purity steviol glycosides
US11312984B2 (en) 2013-05-28 2022-04-26 Purecircle Sdn Bhd High-purity steviol glycosides
US10952458B2 (en) 2013-06-07 2021-03-23 Purecircle Usa Inc Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10780170B2 (en) 2013-06-07 2020-09-22 Purecircle Sdn Bhd Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
CN105722533B (en) * 2013-07-12 2020-10-16 可口可乐公司 Compositions and methods for enhancing rebaudioside M solubility
CN105722533A (en) * 2013-07-12 2016-06-29 可口可乐公司 Compositions and methods for improving rebaudioside M solubility
US10264811B2 (en) 2014-05-19 2019-04-23 Epc Natural Products Co., Ltd. Stevia sweetener with improved solubility
US10561165B2 (en) 2014-05-19 2020-02-18 Sweet Green Fields International Co., Limited Stevia sweetener with improved solubility
US11206857B2 (en) 2014-05-19 2021-12-28 Sweet Green Fields International Co., Limited Stevia sweetener with improved solubility
US10568351B2 (en) 2014-06-16 2020-02-25 Sweet Green Fields USA LLC Rebaudioside A and stevioside with improved solubilities
US10357052B2 (en) 2014-06-16 2019-07-23 Sweet Green Fields USA LLC Rebaudioside A and stevioside with improved solubilities
US11241031B2 (en) 2014-06-16 2022-02-08 Sweet Green Fields Usa, Llc Rebaudioside A and stevioside with improved solubilities
US10485256B2 (en) 2014-06-20 2019-11-26 Sweet Green Fields International Co., Limited Stevia sweetener with improved solubility with a cyclodextrin
US11202461B2 (en) 2014-09-02 2021-12-21 Purecircle Sdn Bhd Stevia extracts
US11856972B2 (en) 2014-09-02 2024-01-02 Purecircle Sdn Bhd Stevia extracts
US11230567B2 (en) 2014-09-02 2022-01-25 Purecircle Usa Inc. Stevia extracts enriched in rebaudioside D, E, N and/or O and process for the preparation thereof
US11647771B2 (en) 2015-10-26 2023-05-16 Purecircle Usa Inc. Steviol glycoside compositions
US11653686B2 (en) 2015-12-15 2023-05-23 Purecircle Usa Inc. Steviol glycoside compositions
CN111662344A (en) * 2020-06-29 2020-09-15 四川大学 Method for recovering rebaudioside A from primary crystallization mother liquor of stevioside
CN111662344B (en) * 2020-06-29 2022-10-14 四川大学 Method for recovering rebaudioside A from primary crystallization mother liquor of stevioside

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