EP2011848A1 - Procédé de stabilisation d'huile de chauffage ou d'huile diesel, en particulier à partir de la dépolymérisation de résidus contenant des hydrocarbures ou d'huile de pyrolyse - Google Patents

Procédé de stabilisation d'huile de chauffage ou d'huile diesel, en particulier à partir de la dépolymérisation de résidus contenant des hydrocarbures ou d'huile de pyrolyse Download PDF

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Publication number
EP2011848A1
EP2011848A1 EP08012226A EP08012226A EP2011848A1 EP 2011848 A1 EP2011848 A1 EP 2011848A1 EP 08012226 A EP08012226 A EP 08012226A EP 08012226 A EP08012226 A EP 08012226A EP 2011848 A1 EP2011848 A1 EP 2011848A1
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EP
European Patent Office
Prior art keywords
oil
diesel
heating
pyrolysis
degrees
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP08012226A
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German (de)
English (en)
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EP2011848B1 (fr
Inventor
Manfred Sappok
Dieter Wagels
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WAGELS, DIETER
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Sappok Manfred
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Publication of EP2011848A1 publication Critical patent/EP2011848A1/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/10—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal from rubber or rubber waste
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G27/00—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation
    • C10G27/04—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G53/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more refining processes
    • C10G53/02—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more refining processes plural serial stages only
    • C10G53/14—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more refining processes plural serial stages only including at least one oxidation step
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G7/00—Distillation of hydrocarbon oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/04—Diesel oil
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/06—Gasoil

Definitions

  • the invention relates to a method having the features of the preamble of claim 1. Thereafter, the invention first relates to a method for stabilizing fuel oil and diesel oil, which, in particular after depolimerizing hydrocarbonaceous residues, was obtained by fractional distillation .. In addition, the method is used to stabilize of pyrolysis oils, so that they can be used after the stabilization process as a fuel in heavy oil-driven units (machines).
  • machines heavy oil-driven units
  • a pyrolysis oil is produced.
  • Pyrolysis is the heating of organic matter under exclusion of oxygen. Delimits the pyrolysis against a thermolysis undertakes M.Krapf in Z. Angew. Chemistry 98, 1986, 413-429 .
  • the pyrolysis process takes place in the case of so-called high-temperature pyrolysis at temperatures between 600 ° C and 800 ° C.
  • the product oil (pyrolysis oil) produced in this way has the same problem as products obtained by depolimerization, because even the pyrolysis oil is darkened by the presence of unsaturated hydrocarbons. In order to make it suitable for use in heavy-duty engines, a further process step is necessary.
  • the object of the invention is to remove the dark coloring of diesel and heating oil, in particular if it has been obtained by depolimerization of hydrocarbon-containing residues, or of pyrolysis oil in a simple way.
  • complex hydrogenation processes should be avoided.
  • the coloring process of the starting oil can largely be prevented or slowed down considerably if the starting oil is stored, for example, under inert gas and / or in the dark in a tank, preferably with the exclusion of air and not too high temperatures.
  • the aging or inking process then proceeds very slowly, or is stopped. If, for example, air is admitted into a base oil tank, it may take several weeks, for example B. take 2 or 3 weeks until a significant change in color occurs. It may therefore be useful to store the fresh produced starting oil accordingly, in order to delay the aging process.
  • an oxidative treatment e.g. performed with air.
  • the dark color can be set in a few seconds.
  • the Enrfärbungsdestillation can be carried out both in a conventional distillation column and in a so-called thin-film evaporator.
  • the discolored starting oil is heated to a temperature between 350 and 390 degrees C, preferably 360 to 380 degrees C, and distilled at about 280 to 320 degrees C, preferably at 290 to 310 degrees C.
  • the discolored starting oil is passed in a thin-layer evaporator, preferably under reduced pressure, over about 180 to 240 ° C., preferably at 200 to 230 ° C. hot evaporator surface, and subsequently the resulting vapor component, in particular as diesel or heating oil condensed.
  • the thin-film evaporation takes place under a pressure of absolutely about 1 to 500 mbar, preferably from 2 to 100 mbar.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
EP08012226.0A 2007-07-05 2008-07-07 Procédé de stabilisation d'huile de chauffage ou d'huile diesel, en particulier à partir de la dépolymérisation de résidus contenant des hydrocarbures, ou d'huile de pyrolyse Active EP2011848B1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102007031461A DE102007031461A1 (de) 2007-07-05 2007-07-05 Verfahren zum Stabilisieren von Heizöl oder Dieselöl, insbesondere aus der Depolimerisation von kohlenwasserstoffhaltigen Rückständen

Publications (2)

Publication Number Publication Date
EP2011848A1 true EP2011848A1 (fr) 2009-01-07
EP2011848B1 EP2011848B1 (fr) 2017-06-07

Family

ID=39764080

Family Applications (1)

Application Number Title Priority Date Filing Date
EP08012226.0A Active EP2011848B1 (fr) 2007-07-05 2008-07-07 Procédé de stabilisation d'huile de chauffage ou d'huile diesel, en particulier à partir de la dépolymérisation de résidus contenant des hydrocarbures, ou d'huile de pyrolyse

Country Status (6)

Country Link
US (1) US8394264B2 (fr)
EP (1) EP2011848B1 (fr)
AU (1) AU2008202986A1 (fr)
CA (1) CA2636956A1 (fr)
DE (1) DE102007031461A1 (fr)
ES (1) ES2638433T3 (fr)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101460473A (zh) 2006-04-03 2009-06-17 药物热化学品公司 热提取方法和产物
US20110284359A1 (en) 2010-05-20 2011-11-24 Uop Llc Processes for controlling afterburn in a reheater and for controlling loss of entrained solid particles in combustion product flue gas
US8499702B2 (en) 2010-07-15 2013-08-06 Ensyn Renewables, Inc. Char-handling processes in a pyrolysis system
US9441887B2 (en) 2011-02-22 2016-09-13 Ensyn Renewables, Inc. Heat removal and recovery in biomass pyrolysis
US9347005B2 (en) 2011-09-13 2016-05-24 Ensyn Renewables, Inc. Methods and apparatuses for rapid thermal processing of carbonaceous material
US10400175B2 (en) 2011-09-22 2019-09-03 Ensyn Renewables, Inc. Apparatuses and methods for controlling heat for rapid thermal processing of carbonaceous material
US9109177B2 (en) 2011-12-12 2015-08-18 Ensyn Renewables, Inc. Systems and methods for renewable fuel
US9670413B2 (en) 2012-06-28 2017-06-06 Ensyn Renewables, Inc. Methods and apparatuses for thermally converting biomass
WO2014031965A2 (fr) * 2012-08-24 2014-02-27 Ensyn Renewables, Inc. Systèmes et procédés pour la dévolatilisation de liquides produits thermiquement
TWI645026B (zh) 2013-06-26 2018-12-21 安信再生公司 可再生燃料之系統及方法
CA2995845A1 (fr) 2015-08-21 2017-03-02 Ensyn Renewables, Inc. Systeme de chauffage a biomasse liquide
CA3048681A1 (fr) 2016-12-29 2018-07-05 Ensyn Renewables, Inc. Demetallisation de biomasse liquide
CA3188369A1 (fr) 2020-09-14 2022-03-17 Ecolab Usa Inc. Additifs d'ecoulement a froid pour charge de depart synthetique derivee de matiere plastique

Citations (6)

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US2002902A (en) * 1932-01-08 1935-05-28 Gulf Refining Co Process for removing gum and gum forming constituents from cracked petroleum distillates
US2726194A (en) * 1951-12-28 1955-12-06 Shell Dev Removing gum-forming components from hydrocarbon distillates
GB839552A (en) * 1955-08-29 1960-06-29 Exxon Research Engineering Co Stabilization of petroleum distillates
US3597173A (en) * 1966-01-03 1971-08-03 Exxon Research Engineering Co Oxidative treatment of petroleum distillate fuels containing olefinic unsaturated components
CN1446883A (zh) * 2003-04-04 2003-10-08 清华大学 利用微藻快速热解制备生物柴油的方法
DE102005010151B3 (de) 2005-03-02 2006-09-14 Clyvia Technology Gmbh Verfahren zum katalytischen Depolymerisieren von kohlenwasserstoffhaltigen Rückständen sowie Vorrichtung zum Durchführen dieses Verfahrens

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US1823994A (en) * 1928-01-13 1931-09-22 Texas Co Treating hydrocarbon oil
US1797513A (en) * 1928-02-02 1931-03-24 Pure Oil Co Method of refining
US1927823A (en) * 1928-11-23 1933-09-26 Continental Oil Co Method of treating lubricating oil stocks
US2056978A (en) * 1930-04-26 1936-10-13 Pure Oil Co Polymerization of hydrocarbon oils
US1974301A (en) * 1931-03-16 1934-09-18 Universal Oil Prod Co Treatment of hydrocarbon oils
NL93590C (fr) * 1953-05-13
US3091587A (en) * 1960-11-25 1963-05-28 Pure Oil Co Method for treating hydrocarbon mixtures
US4222884A (en) * 1978-12-04 1980-09-16 Ethyl Corporation Antioxidant
FR2540739A1 (fr) * 1983-02-11 1984-08-17 Elf France Dispositif et installations pour la distillation par evaporation en couches minces, en particulier pour hydrocarbures, et procede de mise en oeuvre de ce dispositif
NL8900329A (nl) 1989-02-10 1990-09-03 Pharmachemie Bv Cyclische triketonverbindingen en trimethylsilyloxybutadieenverbindingen en hun toepassing bij het bereiden van daunomycinonderivaten.
CA2010183A1 (fr) 1989-03-02 1990-09-02 John G. Bostick Distillat moyen a stabilite au stockage amelioree

Patent Citations (6)

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Publication number Priority date Publication date Assignee Title
US2002902A (en) * 1932-01-08 1935-05-28 Gulf Refining Co Process for removing gum and gum forming constituents from cracked petroleum distillates
US2726194A (en) * 1951-12-28 1955-12-06 Shell Dev Removing gum-forming components from hydrocarbon distillates
GB839552A (en) * 1955-08-29 1960-06-29 Exxon Research Engineering Co Stabilization of petroleum distillates
US3597173A (en) * 1966-01-03 1971-08-03 Exxon Research Engineering Co Oxidative treatment of petroleum distillate fuels containing olefinic unsaturated components
CN1446883A (zh) * 2003-04-04 2003-10-08 清华大学 利用微藻快速热解制备生物柴油的方法
DE102005010151B3 (de) 2005-03-02 2006-09-14 Clyvia Technology Gmbh Verfahren zum katalytischen Depolymerisieren von kohlenwasserstoffhaltigen Rückständen sowie Vorrichtung zum Durchführen dieses Verfahrens

Non-Patent Citations (1)

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Title
M.KRAPF, Z. ANGEW. CHEMIE, vol. 98, 1986, pages 413 - 429

Also Published As

Publication number Publication date
DE102007031461A1 (de) 2009-01-08
CA2636956A1 (fr) 2009-01-05
AU2008202986A1 (en) 2009-01-22
US8394264B2 (en) 2013-03-12
EP2011848B1 (fr) 2017-06-07
US20090008296A1 (en) 2009-01-08
ES2638433T3 (es) 2017-10-20

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