EA201170901A1 - Способ получения катализатора с кремнеземным носителем и способ производства ненасыщенной карбоновой кислоты или ненасыщенного нитрила - Google Patents

Способ получения катализатора с кремнеземным носителем и способ производства ненасыщенной карбоновой кислоты или ненасыщенного нитрила

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Publication number
EA201170901A1
EA201170901A1 EA201170901A EA201170901A EA201170901A1 EA 201170901 A1 EA201170901 A1 EA 201170901A1 EA 201170901 A EA201170901 A EA 201170901A EA 201170901 A EA201170901 A EA 201170901A EA 201170901 A1 EA201170901 A1 EA 201170901A1
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EA
Eurasian Patent Office
Prior art keywords
silica
unsaturated
catalyst
manufacture
carbonic acid
Prior art date
Application number
EA201170901A
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English (en)
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EA019683B1 (ru
Inventor
Юсуке Исии
Такааки Като
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Асахи Касеи Кемикалз Корпорейшн
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Publication of EA201170901A1 publication Critical patent/EA201170901A1/ru
Publication of EA019683B1 publication Critical patent/EA019683B1/ru

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten
    • B01J23/28—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten
    • B01J23/30—Tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/32—Manganese, technetium or rhenium
    • B01J23/34—Manganese
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/057—Selenium or tellurium; Compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/057—Selenium or tellurium; Compounds thereof
    • B01J27/0576—Tellurium; Compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/24—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Настоящее изобретение относится к получению катализатора, нанесенного на кремнезем, обладающего превосходным выходом целевого продукта и превосходной стойкостью катализатора к истиранию. Способ получения катализатора, нанесенного на кремнезем, включающий в себя Мо, V, Nb и компонент Х (Sb и/или Те), используемого в парофазном каталитическом окислении или аммоксидировании пропана, включающий стадии: (I) приготовления раствора сырьевой смеси путем смешивания Мо, V, Nb, компонента X, золя кремниевой кислоты и воды; (II) получения сухого порошка путем высушивания раствора сырьевой смеси; и (III) получения катализатора, нанесенного на кремнезем, путем прокаливания сухого порошка, причем золь кремниевой кислоты содержит 10-270 мас.ч. на миллион нитрат-ионов, исходя из содержания SiO.
EA201170901A 2009-01-30 2010-01-21 Способ получения катализатора с кремнеземным носителем и способ производства ненасыщенной карбоновой кислоты или ненасыщенного нитрила EA019683B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2009020066 2009-01-30
PCT/JP2010/050679 WO2010087262A1 (ja) 2009-01-30 2010-01-21 シリカ担持触媒の製造方法、及び不飽和カルボン酸又は不飽和ニトリルの製造方法

Publications (2)

Publication Number Publication Date
EA201170901A1 true EA201170901A1 (ru) 2012-01-30
EA019683B1 EA019683B1 (ru) 2014-05-30

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EA201170901A EA019683B1 (ru) 2009-01-30 2010-01-21 Способ получения катализатора с кремнеземным носителем и способ производства ненасыщенной карбоновой кислоты или ненасыщенного нитрила

Country Status (9)

Country Link
US (2) US8772195B2 (ru)
EP (2) EP2392399B1 (ru)
JP (1) JP5372022B2 (ru)
KR (1) KR101346885B1 (ru)
CN (1) CN102300636B (ru)
EA (1) EA019683B1 (ru)
TR (1) TR201900712T4 (ru)
TW (1) TWI411469B (ru)
WO (1) WO2010087262A1 (ru)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2601990C1 (ru) * 2012-09-27 2016-11-10 Асахи Касеи Кемикалз Корпорейшн Многокомпонентный оксидный катализатор, способ его изготовления и способ изготовления ненасыщенного нитрила

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012081578A1 (ja) * 2010-12-17 2012-06-21 旭化成ケミカルズ株式会社 触媒の製造装置及び製造方法、並びに不飽和酸又は不飽和ニトリルの製造方法
US9855546B2 (en) 2010-12-27 2018-01-02 Asahi Kasei Chemicals Corporation Composite oxide catalyst and method for producing the same
WO2012111566A1 (ja) * 2011-02-18 2012-08-23 旭化成ケミカルズ株式会社 焼成装置、酸化物触媒の製造方法、及び、不飽和酸又は不飽和ニトリルの製造方法
EP2682385B1 (en) * 2011-03-02 2022-05-11 Asahi Kasei Kabushiki Kaisha Method for producing unsaturated nitrile
JP5710749B2 (ja) * 2011-04-21 2015-04-30 旭化成ケミカルズ株式会社 シリカ担持触媒
KR101837874B1 (ko) * 2014-03-31 2018-03-12 아사히 가세이 가부시키가이샤 산화물 촉매의 제조 방법 및 불포화 니트릴의 제조 방법
CN105771964A (zh) * 2014-12-23 2016-07-20 正大能源材料(大连)有限公司 一种甲醇氨氧化制取氢氰酸的催化剂及其应用
CN107530682B (zh) * 2015-03-31 2021-08-20 旭化成株式会社 氧化物催化剂的制造方法和不饱和腈的制造方法
EP3636631A4 (en) * 2017-06-09 2020-06-03 Asahi Kasei Kabushiki Kaisha PROCESS FOR PRODUCING UNSATURATED NITRILE

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4405498A (en) 1979-12-17 1983-09-20 Monsanto Company Oxidation and ammoxidation catalysts
JPS5954619A (ja) 1982-09-24 1984-03-29 Asahi Glass Co Ltd 珪酸塩粒状体の製造方法
JPS6021811A (ja) 1983-07-15 1985-02-04 Nippon Kensetsu Kikai Shoji Kk シリカゾルの製造方法
JPS60166037A (ja) * 1984-02-07 1985-08-29 Nitto Chem Ind Co Ltd シリカ担持アンチモン含有酸化物触媒の製法
JPS60166039A (ja) * 1984-02-07 1985-08-29 Nitto Chem Ind Co Ltd アンチモン含有酸化物触媒の製法
JPS627622A (ja) 1985-07-04 1987-01-14 Nissan Chem Ind Ltd 極小粒子径シリカゾルの製造法
DE3867249D1 (de) 1987-02-17 1992-02-13 Nippon Catalytic Chem Ind Katalysator zur oxydation von olefin oder tertiaerem alkohol und verfahren zu seiner herstellung.
CN1005404B (zh) 1987-03-02 1989-10-11 中国石油化工总公司上海石油化工研究所 可调节孔结构的遇水不裂硅胶的制法
JP3584485B2 (ja) 1993-03-03 2004-11-04 日産化学工業株式会社 シリカゾルの製造方法
CN1040845C (zh) * 1993-07-16 1998-11-25 中国石油化工总公司 微球状γ-氧化铝的制备方法
US6143690A (en) * 1998-05-07 2000-11-07 Asahi Kasei Kogyo Kabushiki Kaisha Ammoxidation catalyst for use in producing acrylonitrile or methacrylonitrile from propane or isobutane
US6037304A (en) 1999-01-11 2000-03-14 Saudi Basic Industries Corporation Highly active and selective catalysts for the production of unsaturated nitriles, methods of making and using the same
JP3631406B2 (ja) 1999-12-28 2005-03-23 株式会社日本触媒 接触気相酸化反応用の多管式反応器
US6486091B1 (en) 2000-03-14 2002-11-26 Saudi Basic Industries Corporation Process for making highly active and selective catalysts for the production of unsaturated nitriles
JP4413368B2 (ja) 2000-04-03 2010-02-10 旭化成ケミカルズ株式会社 酸化またはアンモ酸化用触媒
JP4530595B2 (ja) 2000-12-13 2010-08-25 旭化成ケミカルズ株式会社 酸化またはアンモ酸化用酸化物触媒
JP4878684B2 (ja) 2001-01-24 2012-02-15 旭化成ケミカルズ株式会社 低比重シリカ担持触媒
FR2821840B1 (fr) * 2001-03-07 2004-07-16 Atofina Procede de fabrication d'acide acrylique a partir de propane, en l'absence d'oxygene moleculaire
DE60210709T2 (de) * 2001-06-18 2007-01-11 Rohm And Haas Co. Herstellung von hydrothermal synthetisierten Mo-V-M-X-Oxid Katalysatoren für die Oxidation von Kohlenwasserstoffen
US6919295B2 (en) * 2002-05-01 2005-07-19 Rohm And Haas Company Supported mixed metal oxide catalyst
EP1407819A3 (en) * 2002-10-01 2004-06-23 Rohm And Haas Company Hydrothermally synthesized Mo-V-M-Nb-X oxide catalysts for the selective oxidation of hydrocarbons
US7229946B2 (en) * 2003-03-24 2007-06-12 Saudi Basic Industries Corporation Catalyst composition for the selective conversion of alkanes to unsaturated carboxylic acids, method of making and method of using thereof
US8193387B2 (en) * 2003-12-19 2012-06-05 Saudi Basic Industries Corporation Process for producing an unsaturated carboxylic acid from an alkane
US7009075B2 (en) * 2004-06-30 2006-03-07 Saudi Basic Industries Corporation Process for the selective conversion of alkanes to unsaturated carboxylic acids
WO2006019078A1 (ja) * 2004-08-17 2006-02-23 Asahi Kasei Chemicals Corporation 複合酸化物からなる触媒
US7645897B2 (en) * 2004-10-15 2010-01-12 Xinlin Tu Process for producing metal oxide catalyst
EP1704919A1 (en) * 2005-03-25 2006-09-27 Arkema France Process for preparing improved catalysts for selective oxidation of propane into acrylic acid
CN104475085B (zh) * 2006-03-20 2019-02-22 旭化成株式会社 氧化或氨氧化用催化剂及其制造方法
US7807601B2 (en) * 2006-12-27 2010-10-05 Exxonmobil Research And Engineering Company Mixed metal oxide catalysts and processes for their preparation and use
JP5529547B2 (ja) * 2007-01-19 2014-06-25 エバーヌ・テクノロジー・リミテッド・ライアビリティ・カンパニー アルカンおよび／またはアルケンの有益な酸素化物への選択的酸化
US20090042723A1 (en) * 2007-02-06 2009-02-12 Kun Wang Process for preparing mixed metal oxide catalysts
JP4961286B2 (ja) 2007-07-13 2012-06-27 東洋ゴム工業株式会社 ゴム製品の寿命予測方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2601990C1 (ru) * 2012-09-27 2016-11-10 Асахи Касеи Кемикалз Корпорейшн Многокомпонентный оксидный катализатор, способ его изготовления и способ изготовления ненасыщенного нитрила

Also Published As

Publication number Publication date
KR101346885B1 (ko) 2014-01-02
US20140256977A1 (en) 2014-09-11
CN102300636A (zh) 2011-12-28
WO2010087262A1 (ja) 2010-08-05
JPWO2010087262A1 (ja) 2012-08-02
EP3466533A1 (en) 2019-04-10
US8772195B2 (en) 2014-07-08
EP2392399B1 (en) 2018-12-19
US9000207B2 (en) 2015-04-07
JP5372022B2 (ja) 2013-12-18
TR201900712T4 (tr) 2019-02-21
EP2392399A4 (en) 2013-01-30
US20110288325A1 (en) 2011-11-24
EP2392399A1 (en) 2011-12-07
KR20110074910A (ko) 2011-07-04
TWI411469B (zh) 2013-10-11
CN102300636B (zh) 2015-01-07
TW201041649A (en) 2010-12-01
EA019683B1 (ru) 2014-05-30

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