DE867688C - Verfahren zur Herstellung von Bernsteinsaeure - Google Patents
Verfahren zur Herstellung von BernsteinsaeureInfo
- Publication number
- DE867688C DE867688C DEB6609D DEB0006609D DE867688C DE 867688 C DE867688 C DE 867688C DE B6609 D DEB6609 D DE B6609D DE B0006609 D DEB0006609 D DE B0006609D DE 867688 C DE867688 C DE 867688C
- Authority
- DE
- Germany
- Prior art keywords
- vessel
- succinic acid
- oxidation
- nitric acid
- tetrahydrofuran
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 title claims description 33
- 239000001384 succinic acid Substances 0.000 title claims description 15
- 238000000034 method Methods 0.000 title claims description 4
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 22
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 19
- 229910017604 nitric acid Inorganic materials 0.000 claims description 19
- 230000003647 oxidation Effects 0.000 claims description 19
- 238000007254 oxidation reaction Methods 0.000 claims description 19
- 238000006243 chemical reaction Methods 0.000 claims description 12
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 8
- 239000012452 mother liquor Substances 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 5
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 claims description 3
- 239000007800 oxidant agent Substances 0.000 claims description 3
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 24
- 239000007789 gas Substances 0.000 description 14
- 238000001816 cooling Methods 0.000 description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 7
- 239000001301 oxygen Substances 0.000 description 7
- 229910052760 oxygen Inorganic materials 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000011541 reaction mixture Substances 0.000 description 4
- 239000012530 fluid Substances 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 239000004063 acid-resistant material Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- UUHHOIMXURPAAJ-UHFFFAOYSA-N nitric acid oxolane Chemical compound O[N+]([O-])=O.C1CCOC1 UUHHOIMXURPAAJ-UHFFFAOYSA-N 0.000 description 1
- 229910017464 nitrogen compound Inorganic materials 0.000 description 1
- 150000002830 nitrogen compounds Chemical class 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
- C07C51/316—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with oxides of nitrogen or nitrogen-containing mineral acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEB6609D DE867688C (de) | 1939-12-15 | 1941-07-04 | Verfahren zur Herstellung von Bernsteinsaeure |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2312468X | 1939-12-15 | ||
| DEB6609D DE867688C (de) | 1939-12-15 | 1941-07-04 | Verfahren zur Herstellung von Bernsteinsaeure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE867688C true DE867688C (de) | 1953-02-19 |
Family
ID=7994513
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEB6609D Expired DE867688C (de) | 1939-12-15 | 1941-07-04 | Verfahren zur Herstellung von Bernsteinsaeure |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US2312468A (en:Method) |
| BE (2) | BE445957A (en:Method) |
| DE (1) | DE867688C (en:Method) |
| FR (2) | FR879534A (en:Method) |
| NL (2) | NL60065C (en:Method) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2459690A (en) * | 1945-05-02 | 1949-01-18 | Union Oil Co | Oxidation of cycloaliphatic hydrocarbons and alcohols |
| US2463776A (en) * | 1946-03-29 | 1949-03-08 | Ici Ltd | Production of lactones |
| US2497889A (en) * | 1948-03-26 | 1950-02-21 | Eastman Kodak Co | Oxidation of ethers using aldehyde-activated catalysts |
| BE485408A (en:Method) * | 1948-04-24 | |||
| US2862942A (en) * | 1957-10-01 | 1958-12-02 | Jordan P Snyder | Method of oxidizing and cleaving compounds to form acidic products |
| US3100798A (en) * | 1960-12-27 | 1963-08-13 | Exxon Research Engineering Co | Process for preparation of succinic acid |
| US4978785A (en) * | 1989-12-11 | 1990-12-18 | Texaco Chemical Company | Oxidation of polyoxypropylene glycols to acids and ketones |
-
0
- BE BE444240D patent/BE444240A/xx unknown
- NL NL58783D patent/NL58783C/xx active
- NL NL60065D patent/NL60065C/xx active
- BE BE445957D patent/BE445957A/xx unknown
-
1941
- 1941-03-08 US US382447A patent/US2312468A/en not_active Expired - Lifetime
- 1941-07-04 DE DEB6609D patent/DE867688C/de not_active Expired
-
1942
- 1942-02-21 FR FR879534D patent/FR879534A/fr not_active Expired
- 1942-06-09 FR FR52179D patent/FR52179E/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US2312468A (en) | 1943-03-02 |
| NL58783C (en:Method) | |
| FR879534A (fr) | 1943-02-25 |
| BE445957A (en:Method) | |
| BE444240A (en:Method) | |
| NL60065C (en:Method) | |
| FR52179E (fr) | 1943-09-15 |
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