DE69727963T2 - Verfahren zur kristallisation von 2,4,6,8,10,12,-hexanitro-2,4,6,8,10,12,-hexaazatetrazyklo- [5.5.0.05,9 0 3,11]-dodecan durch ausfällen - Google Patents

Verfahren zur kristallisation von 2,4,6,8,10,12,-hexanitro-2,4,6,8,10,12,-hexaazatetrazyklo- [5.5.0.05,9 0 3,11]-dodecan durch ausfällen Download PDF

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Publication number
DE69727963T2
DE69727963T2 DE69727963T DE69727963T DE69727963T2 DE 69727963 T2 DE69727963 T2 DE 69727963T2 DE 69727963 T DE69727963 T DE 69727963T DE 69727963 T DE69727963 T DE 69727963T DE 69727963 T2 DE69727963 T2 DE 69727963T2
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DE
Germany
Prior art keywords
solvent
crystallization
polymorphic
wet
water
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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DE69727963T
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German (de)
English (en)
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DE69727963D1 (de
Inventor
Eugene H. JOHNSTON
B. Robert WARDLE
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Northrop Grumman Innovation Systems LLC
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Alliant Techsystems Inc
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Publication of DE69727963D1 publication Critical patent/DE69727963D1/de
Publication of DE69727963T2 publication Critical patent/DE69727963T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D259/00—Heterocyclic compounds containing rings having more than four nitrogen atoms as the only ring hetero atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/22—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains four or more hetero rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
DE69727963T 1996-12-17 1997-12-12 Verfahren zur kristallisation von 2,4,6,8,10,12,-hexanitro-2,4,6,8,10,12,-hexaazatetrazyklo- [5.5.0.05,9 0 3,11]-dodecan durch ausfällen Expired - Fee Related DE69727963T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US33392 1993-03-19
US3339296P 1996-12-17 1996-12-17
PCT/US1997/022298 WO1998027072A1 (en) 1996-12-17 1997-12-12 Salting-out process of crystallizing 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0?5,903,11¿]-dodecane

Publications (2)

Publication Number Publication Date
DE69727963D1 DE69727963D1 (de) 2004-04-08
DE69727963T2 true DE69727963T2 (de) 2004-07-22

Family

ID=21870159

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69727963T Expired - Fee Related DE69727963T2 (de) 1996-12-17 1997-12-12 Verfahren zur kristallisation von 2,4,6,8,10,12,-hexanitro-2,4,6,8,10,12,-hexaazatetrazyklo- [5.5.0.05,9 0 3,11]-dodecan durch ausfällen

Country Status (10)

Country Link
US (1) US5874574A (enExample)
EP (1) EP0946527B1 (enExample)
JP (1) JP2001510465A (enExample)
KR (1) KR20000069513A (enExample)
AU (1) AU5374398A (enExample)
CA (1) CA2275317A1 (enExample)
DE (1) DE69727963T2 (enExample)
IL (1) IL130308A0 (enExample)
NO (1) NO313698B1 (enExample)
WO (1) WO1998027072A1 (enExample)

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US6214988B1 (en) 1999-01-03 2001-04-10 Schlumberger Technology Corporation Process for making an HMX product
JP2002538160A (ja) 1999-02-16 2002-11-12 アライアント・テクシステムズ・インコーポレーテッド ２，４，６，８，１０，１２−ヘキサニトロ−２，４，６，８，１０，１２−ヘキサアザテトラシクロ［５．５．０．０５，９．０３，１１］−ドデカンの製造方法
US6265573B1 (en) 1999-05-26 2001-07-24 Schlumberger Technology Corporation Purification process
US6201117B1 (en) 1999-05-26 2001-03-13 Schlumberger Technology Corporation Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane
US6194571B1 (en) 1999-05-26 2001-02-27 Schlumberger Technology Corporation HMX compositions and processes for their preparation
US6428724B1 (en) 1999-05-26 2002-08-06 Schlumberger Technology Corporation Granulation process
US6841016B1 (en) * 2000-03-02 2005-01-11 Nederlandse Organisatie Voor Toegepast-Natuurwetenschappelijk Onderzoek Tno Process for the production of crystalline energetic materials
US6350871B1 (en) 2000-03-31 2002-02-26 Alliant Techsystems Inc. Crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US7288648B2 (en) 2000-10-06 2007-10-30 Alliant Techsystems Inc. High temperature crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US6884436B2 (en) * 2000-12-22 2005-04-26 Baxter International Inc. Method for preparing submicron particle suspensions
US20050048126A1 (en) * 2000-12-22 2005-03-03 Barrett Rabinow Formulation to render an antimicrobial drug potent against organisms normally considered to be resistant to the drug
US20030096013A1 (en) * 2000-12-22 2003-05-22 Jane Werling Preparation of submicron sized particles with polymorph control
CA2437797A1 (en) * 2001-02-09 2002-10-03 Alliant Techsystems Inc. Reformulation of composition c-4 explosive
EP1412308A2 (en) * 2001-08-01 2004-04-28 Alliant Techsystems Inc. Low sensitivity explosive compositions and method for making explosive compositions
IL160570A0 (en) * 2001-09-26 2004-07-25 Baxter Int Preparation of submicron sized nanoparticles via dispersion and solvent or liquid phase removal
US7112340B2 (en) * 2001-10-19 2006-09-26 Baxter International Inc. Compositions of and method for preparing stable particles in a frozen aqueous matrix
US6992185B2 (en) * 2002-01-09 2006-01-31 Alliant Techsystems Inc. Crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
WO2006138202A2 (en) * 2005-06-14 2006-12-28 Baxter International Inc. Pharmaceutical formulations for minimizing drug-drug interactions
EP1954245A2 (en) * 2005-11-15 2008-08-13 Baxter International Inc. Compositions of lipoxygenase inhibitors
WO2008080047A2 (en) * 2006-12-23 2008-07-03 Baxter International Inc. Magnetic separation of fine particles from compositions
US8722736B2 (en) * 2007-05-22 2014-05-13 Baxter International Inc. Multi-dose concentrate esmolol with benzyl alcohol
US20080293814A1 (en) * 2007-05-22 2008-11-27 Deepak Tiwari Concentrate esmolol
US8426467B2 (en) * 2007-05-22 2013-04-23 Baxter International Inc. Colored esmolol concentrate
FR2950623B1 (fr) * 2009-09-29 2011-10-21 Snpe Materiaux Energetiques Suspension de cristaux d'hexanitrohexaazaisowurtzitane, obtention desdites suspensions et fabrication d'objets pyrotechniques.
RU2447075C9 (ru) * 2011-01-11 2012-11-20 Открытое акционерное общество "Федеральный научно-производственный центр "Алтай" Способ получения гамма-полиморфной модификации 2,4,6,8,10,12-гексанитро-2,4,6,8,10,12-гексаазатетрацикло[5,5,0,03,11,05,9]додекана
CZ303686B6 (cs) 2011-09-29 2013-03-06 Univerzita Pardubice Zpusob prípravy epsilon-2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitanu se snízenou citlivostí k nárazu
CN105418619B (zh) * 2015-12-29 2017-12-12 山西北化关铝化工有限公司 一种特质六硝基六氮杂异伍兹烷的制备方法
CN105693734B (zh) * 2016-03-15 2018-11-09 北京理工大学 一种特质ε-HNIW晶体及其制备方法
US10626061B2 (en) * 2017-08-03 2020-04-21 National Technology & Engineering Solutions Of Sandia, Llc Synthesis of energetic material particles with controlled morphology
CN119425143A (zh) * 2024-10-11 2025-02-14 西安近代化学研究所 一种基于微流控技术的ε-HNIW粒度调控方法

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SE451718B (sv) * 1984-04-04 1987-10-26 Nobel Kemi Ab Sett att omkristallisera sprengemnena oktogen och hexogen
DE3617408C1 (de) * 1986-05-23 1987-06-11 Dynamit Nobel Ag Verfahren zur Herstellung von feinkoernigem beta-Oktogen
US4785094A (en) * 1986-09-26 1988-11-15 Morton Thiokol, Inc. Crystallization of beta HMX
US5132409A (en) * 1987-01-12 1992-07-21 Bracco Industria Chimica S.P.A. Macrocyclic chelating agents and chelates thereof
US5693794A (en) * 1988-09-30 1997-12-02 The United States Of America As Represented By The Secretary Of The Navy Caged polynitramine compound
KR0132576B1 (ko) * 1988-10-05 1998-04-17 로렌스 티. 웰츠 항-용매 내로의 침전을 통한 미분 고형물 결정 분말의 제조 방법
US5707634A (en) * 1988-10-05 1998-01-13 Pharmacia & Upjohn Company Finely divided solid crystalline powders via precipitation into an anti-solvent
DE4200743C2 (de) * 1991-09-18 1994-04-07 Wasagchemie Sythen Gmbh Verfahren und Vorrichtung zur Verringerung der Korngröße von kristallinem Explosivstoff
US5124493A (en) * 1991-10-15 1992-06-23 The United States Of America As Represented By The Secretary Of The Army Process of producing XMX in 100% yield and purity
US5268469A (en) * 1991-10-15 1993-12-07 The United States Of America As Represented By The Secretary Of The Army Process of making impact insensitive Alpha-HMX
US5723604A (en) * 1995-06-22 1998-03-03 Thiokol Corporation Synthesis of 2,4,6,8,10,12-hexabenzyl-2,4,6,8,10,12-hexaazatetracyclo 5.5.0.05,9.03,11!dodecane
US5739325A (en) * 1995-12-07 1998-04-14 Thiokol Corporation Hydrogenolysis of 2,4,6,8,10,12-Hexabenzyl-2,4,6,8,10,12-Hexaazatetracyclo 5.5.0.05,9.03,11 !dodecane

Also Published As

Publication number Publication date
US5874574A (en) 1999-02-23
EP0946527A1 (en) 1999-10-06
CA2275317A1 (en) 1998-06-25
NO313698B1 (no) 2002-11-18
WO1998027072A1 (en) 1998-06-25
KR20000069513A (ko) 2000-11-25
EP0946527B1 (en) 2004-03-03
NO992929L (no) 1999-06-16
JP2001510465A (ja) 2001-07-31
IL130308A0 (en) 2000-06-01
DE69727963D1 (de) 2004-04-08
NO992929D0 (no) 1999-06-16
AU5374398A (en) 1998-07-15

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