DE60228122D1 - Verfahren zur herstellung von polytrimethylenterephthalat - Google Patents
Verfahren zur herstellung von polytrimethylenterephthalatInfo
- Publication number
- DE60228122D1 DE60228122D1 DE60228122T DE60228122T DE60228122D1 DE 60228122 D1 DE60228122 D1 DE 60228122D1 DE 60228122 T DE60228122 T DE 60228122T DE 60228122 T DE60228122 T DE 60228122T DE 60228122 D1 DE60228122 D1 DE 60228122D1
- Authority
- DE
- Germany
- Prior art keywords
- esterification
- product
- pdo
- precondensation
- ppm
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 230000032050 esterification Effects 0.000 abstract 3
- 238000005886 esterification reaction Methods 0.000 abstract 3
- 239000000047 product Substances 0.000 abstract 3
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 abstract 2
- 239000006227 byproduct Substances 0.000 abstract 2
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- 238000006068 polycondensation reaction Methods 0.000 abstract 2
- 238000006116 polymerization reaction Methods 0.000 abstract 2
- -1 polytrimethylene terephthalate Polymers 0.000 abstract 2
- 229920002215 polytrimethylene terephthalate Polymers 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 abstract 1
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 150000002736 metal compounds Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000000737 periodic effect Effects 0.000 abstract 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
- C08G63/82—Preparation processes characterised by the catalyst used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
- C08G63/785—Preparation processes characterised by the apparatus used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/16—Dicarboxylic acids and dihydroxy compounds
- C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
- C08G63/181—Acids containing aromatic rings
- C08G63/183—Terephthalic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyesters Or Polycarbonates (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US34100001P | 2001-10-30 | 2001-10-30 | |
| PCT/EP2002/012181 WO2003037958A1 (en) | 2001-10-30 | 2002-10-29 | Process for making polytrimethylene terephthalate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE60228122D1 true DE60228122D1 (de) | 2008-09-18 |
Family
ID=23335843
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE60228122T Expired - Fee Related DE60228122D1 (de) | 2001-10-30 | 2002-10-29 | Verfahren zur herstellung von polytrimethylenterephthalat |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US6657044B1 (enExample) |
| EP (1) | EP1456276B1 (enExample) |
| JP (1) | JP4074250B2 (enExample) |
| KR (1) | KR20050040830A (enExample) |
| CN (1) | CN1273514C (enExample) |
| AT (1) | ATE403689T1 (enExample) |
| BR (1) | BR0213547A (enExample) |
| CA (1) | CA2465281A1 (enExample) |
| DE (1) | DE60228122D1 (enExample) |
| ES (1) | ES2311646T3 (enExample) |
| MX (1) | MXPA04004014A (enExample) |
| MY (1) | MY129191A (enExample) |
| SA (1) | SA03240057B1 (enExample) |
| TW (1) | TWI255276B (enExample) |
| WO (1) | WO2003037958A1 (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ATE265486T1 (de) * | 2000-02-11 | 2004-05-15 | Du Pont | Kontinuierliches verfahren zur herstellung von polytrimethylenterephthalat |
| TWI255821B (en) * | 2003-01-22 | 2006-06-01 | Asahi Kasei Chemicals Corp | Polytrimethylene terephthalate resin and method for production thereof |
| JP4552462B2 (ja) * | 2003-04-07 | 2010-09-29 | 三菱化学株式会社 | ポリエステル重縮合反応留出物の処理方法 |
| US7504474B2 (en) * | 2005-12-21 | 2009-03-17 | E. I. Du Pont De Nemours And Company | Poly(trimethylene therephthalate) continuous manufacturing process |
| US7524921B2 (en) * | 2005-12-21 | 2009-04-28 | E. I. Du Pont De Nemours And Company | Continuous manufacture of poly(trimethylene terephthalate) |
| US7531617B2 (en) * | 2005-12-21 | 2009-05-12 | E. I. Du Pont De Nemours And Company | Continuous process for producing poly(trimethylene terephthalate) |
| US7772362B2 (en) * | 2007-07-16 | 2010-08-10 | Texas State University | Treatment method for imparting self-healing and shape memory properties to certain CBDO copolymers |
| US20090043021A1 (en) * | 2007-08-06 | 2009-02-12 | Jing-Chung Chang | Flame retardant polytrimethylene terephthalate composition |
| US7855244B2 (en) * | 2007-08-06 | 2010-12-21 | E.I. Du Pont De Nemours And Company | Flame retardant polytrimethylene terephthalate composition |
| US20090043016A1 (en) * | 2007-08-06 | 2009-02-12 | Jing-Chung Chang | Flame retardant polytrimethylene terephthalate composition |
| US20090043019A1 (en) * | 2007-08-06 | 2009-02-12 | Jing-Chung Chang | Flame retardant polytrimethylene terephthalate composition |
| US20090043017A1 (en) * | 2007-08-06 | 2009-02-12 | Jing-Chung Chang | Flame retardant polytrimethylene terephthalate composition |
| JP2012505953A (ja) * | 2008-10-16 | 2012-03-08 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | 難燃性ポリ（トリメチレンテレフタレート）組成物 |
| US20100152411A1 (en) | 2008-12-17 | 2010-06-17 | E.I. Du Pont De Nemours And Company | Poly(trimethylene terephthalate) with reduced whitening |
| WO2010077937A1 (en) | 2008-12-17 | 2010-07-08 | E. I. Du Pont De Nemours And Company | Reduction of whitening of poly(trimethylene terephthalate) parts by solvent exposure |
| US20100152329A1 (en) | 2008-12-17 | 2010-06-17 | E. I. Du Pont De Nemours And Company | Poly(trimethylene terephthalate) polymer blends that have reduced whitening |
| BRPI1006518A2 (pt) | 2009-03-03 | 2016-02-10 | Du Pont | processo para a redução de teor de oligômero de péletes de polímero de poli (trimetileno tereftalato), processo para medir da redução de teor de oligômero de polímero de poli(trimetileno tereftalato), péletes, artigo produzido por péletes moldados e fibra produzida por péletes de fiação derretida |
| CN103228699A (zh) | 2010-11-22 | 2013-07-31 | 纳幕尔杜邦公司 | 包含聚(对苯二甲酸1,3-丙二醇酯)和聚(2,6-萘二甲酸1,3-丙二醇酯)的嵌段共聚物 |
| KR20160047218A (ko) * | 2014-10-22 | 2016-05-02 | 에스케이케미칼주식회사 | 부산물의 함량이 낮은 폴리(트리메틸렌 테레프탈레이트)의 연속 제조 방법 |
| CN104629021B (zh) * | 2015-02-15 | 2017-07-07 | 张家港美景荣化学工业有限公司 | 一种聚对苯二甲酸丙二醇酯及其生产方法 |
| CN105622907A (zh) * | 2016-04-08 | 2016-06-01 | 张家港美景荣化学工业有限公司 | 高粘聚对苯二甲酸丙二醇酯及其共聚酯的制备方法 |
| KR20180035522A (ko) * | 2016-09-29 | 2018-04-06 | 주식회사 엘지화학 | 폴리에테르에스테르 공중합체의 제조방법 |
| CN112639183A (zh) | 2018-06-28 | 2021-04-09 | 杜邦工业生物科学美国有限责任公司 | 包含聚酯短纤维的纺纱以及包含所述纺纱的织物 |
| JP2020050820A (ja) * | 2018-09-28 | 2020-04-02 | 東レ株式会社 | 高収率ポリエステルの製造方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4418188A (en) | 1982-09-07 | 1983-11-29 | The Goodyear Tire & Rubber Company | Polyethylene isophthalate having reduced cyclic dimer content and process therefore |
| US4424337A (en) | 1982-09-07 | 1984-01-03 | The Goodyear Tire & Rubber Company | Polyisophthalate and copolymers thereof having reduced cyclic dimer content, and a process for making the same |
| US4835247A (en) | 1988-08-08 | 1989-05-30 | The Goodyear Tire & Rubber Company | Process for the synthesis of a copolyester adhesive resin |
| US4921929A (en) | 1988-08-08 | 1990-05-01 | The Goodyear Tire & Rubber Company | Process for the synthesis of a copolyester adhesive resin |
| MY118950A (en) | 1997-04-30 | 2005-02-28 | Shell Int Research | Purification of by- product stream in preparation of polytrimethylene terephthalate |
| US6245879B1 (en) | 1999-01-29 | 2001-06-12 | Shell Oil Company | Purification of 1,3-propanediol in carbonyl-containing stream |
| US6277947B1 (en) | 2000-04-21 | 2001-08-21 | Shell Oil Company | Process of producing polytrimethylene terephthalate (PTT) |
| ATE234336T1 (de) | 1999-04-22 | 2003-03-15 | Zimmer Ag | Verfahren zur herstellung von polytrimethylenterephthalat (ptt) |
| MXPA02001942A (es) * | 1999-08-25 | 2002-10-31 | Du Pont | Preparacion de poli(trimetilen tereftalato) con bajo nivel de di(1,3-propilenglicol). |
| US20020123606A1 (en) * | 1999-08-26 | 2002-09-05 | Kurian Joseph Varapadavil | Poly(trimethylene terephthalate) with low level of DI(1,3-propylene glycol) |
-
2002
- 2002-10-18 US US10/274,317 patent/US6657044B1/en not_active Expired - Fee Related
- 2002-10-29 ES ES02802309T patent/ES2311646T3/es not_active Expired - Lifetime
- 2002-10-29 MX MXPA04004014A patent/MXPA04004014A/es active IP Right Grant
- 2002-10-29 CN CNB028215737A patent/CN1273514C/zh not_active Expired - Fee Related
- 2002-10-29 KR KR1020047006349A patent/KR20050040830A/ko not_active Ceased
- 2002-10-29 DE DE60228122T patent/DE60228122D1/de not_active Expired - Fee Related
- 2002-10-29 MY MYPI20024047A patent/MY129191A/en unknown
- 2002-10-29 CA CA002465281A patent/CA2465281A1/en not_active Abandoned
- 2002-10-29 WO PCT/EP2002/012181 patent/WO2003037958A1/en not_active Ceased
- 2002-10-29 JP JP2003540233A patent/JP4074250B2/ja not_active Expired - Fee Related
- 2002-10-29 AT AT02802309T patent/ATE403689T1/de not_active IP Right Cessation
- 2002-10-29 EP EP02802309A patent/EP1456276B1/en not_active Expired - Lifetime
- 2002-10-29 BR BR0213547-7A patent/BR0213547A/pt not_active IP Right Cessation
- 2002-10-29 TW TW091132056A patent/TWI255276B/zh not_active IP Right Cessation
-
2003
- 2003-03-29 SA SA03240057A patent/SA03240057B1/ar unknown
Also Published As
| Publication number | Publication date |
|---|---|
| SA03240057B1 (ar) | 2007-05-09 |
| ATE403689T1 (de) | 2008-08-15 |
| TW200302839A (en) | 2003-08-16 |
| BR0213547A (pt) | 2004-10-26 |
| CN1273514C (zh) | 2006-09-06 |
| ES2311646T3 (es) | 2009-02-16 |
| CN1578800A (zh) | 2005-02-09 |
| KR20050040830A (ko) | 2005-05-03 |
| WO2003037958A1 (en) | 2003-05-08 |
| TWI255276B (en) | 2006-05-21 |
| EP1456276B1 (en) | 2008-08-06 |
| MXPA04004014A (es) | 2004-07-23 |
| MY129191A (en) | 2007-03-30 |
| US6657044B1 (en) | 2003-12-02 |
| EP1456276A1 (en) | 2004-09-15 |
| JP2005536574A (ja) | 2005-12-02 |
| JP4074250B2 (ja) | 2008-04-09 |
| CA2465281A1 (en) | 2003-05-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |