BR0213547A - Processo de produção de tereftalato de politrimetileno - Google Patents

Processo de produção de tereftalato de politrimetileno

Info

Publication number
BR0213547A
BR0213547A BR0213547-7A BR0213547A BR0213547A BR 0213547 A BR0213547 A BR 0213547A BR 0213547 A BR0213547 A BR 0213547A BR 0213547 A BR0213547 A BR 0213547A
Authority
BR
Brazil
Prior art keywords
polytrimethylene terephthalate
esterification
product
pdo
precondensation
Prior art date
Application number
BR0213547-7A
Other languages
English (en)
Inventor
Donald Ross Kelsey
Kathleen Suzanne Kiibler
Wen Tzung Tang
Original Assignee
Shell Int Research
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Int Research filed Critical Shell Int Research
Publication of BR0213547A publication Critical patent/BR0213547A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/82—Preparation processes characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/785—Preparation processes characterised by the apparatus used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16—Dicarboxylic acids and dihydroxy compounds
    • C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/181—Acids containing aromatic rings
    • C08G63/183—Terephthalic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

"PROCESSO DE PRODUçãO DE TEREFTALATO DE POLITRIMETILENO". Um processo melhorado para a polimerização de tereftalato de politrimetileno por esterificação do ácido tereftálico ou do tereftalato de dimetila com 1,3-propanodiol (PDO), pré-condensação do produto de esterificação para produzir um produto de pré-condensação e policondensação do produto de pré-condensação par produzir tereftalato de politrimetileno em que o excesso de PDO é removido do estágio de esterificação e/ou de policondensação e o vapor de PDO é separado da fração de alto ponto de ebulição (produto secundário sólido). O melhoramento compreende: a) o aquecimento do produto secundário sólido na presença de 5 ppm a 5000 ppm, com base no metal, de um catalisador metálico selecionado do grupo que consiste em um ou mais dos compostos de metais da terceira, quarta ou quinta carreira dos Grupos 3-12 e Grupos 14-15 da Tabela Periódica (IUPAC 1989) a uma temperatura que vai de 100<198>C até 240<198>C durante um período que vai de 5 minutos a 24 horas, opcionalmente na presença de um diluente e b) opcionalmente a reciclagem do produto de reação ao processo de polimerização.
BR0213547-7A 2001-10-30 2002-10-29 Processo de produção de tereftalato de politrimetileno BR0213547A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US34100001P 2001-10-30 2001-10-30
PCT/EP2002/012181 WO2003037958A1 (en) 2001-10-30 2002-10-29 Process for making polytrimethylene terephthalate

Publications (1)

Publication Number Publication Date
BR0213547A true BR0213547A (pt) 2004-10-26

Family

ID=23335843

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0213547-7A BR0213547A (pt) 2001-10-30 2002-10-29 Processo de produção de tereftalato de politrimetileno

Country Status (15)

Country Link
US (1) US6657044B1 (pt)
EP (1) EP1456276B1 (pt)
JP (1) JP4074250B2 (pt)
KR (1) KR20050040830A (pt)
CN (1) CN1273514C (pt)
AT (1) ATE403689T1 (pt)
BR (1) BR0213547A (pt)
CA (1) CA2465281A1 (pt)
DE (1) DE60228122D1 (pt)
ES (1) ES2311646T3 (pt)
MX (1) MXPA04004014A (pt)
MY (1) MY129191A (pt)
SA (1) SA03240057B1 (pt)
TW (1) TWI255276B (pt)
WO (1) WO2003037958A1 (pt)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2396469C (en) * 2000-02-11 2010-01-26 E.I. Du Pont De Nemours And Company Continuous process for producing poly(trimethylene terephthalate)
TWI255821B (en) * 2003-01-22 2006-06-01 Asahi Kasei Chemicals Corp Polytrimethylene terephthalate resin and method for production thereof
JP4552462B2 (ja) * 2003-04-07 2010-09-29 三菱化学株式会社 ポリエステル重縮合反応留出物の処理方法
US7531617B2 (en) * 2005-12-21 2009-05-12 E. I. Du Pont De Nemours And Company Continuous process for producing poly(trimethylene terephthalate)
US7524921B2 (en) * 2005-12-21 2009-04-28 E. I. Du Pont De Nemours And Company Continuous manufacture of poly(trimethylene terephthalate)
US7504474B2 (en) * 2005-12-21 2009-03-17 E. I. Du Pont De Nemours And Company Poly(trimethylene therephthalate) continuous manufacturing process
US7772362B2 (en) * 2007-07-16 2010-08-10 Texas State University Treatment method for imparting self-healing and shape memory properties to certain CBDO copolymers
US20090043019A1 (en) * 2007-08-06 2009-02-12 Jing-Chung Chang Flame retardant polytrimethylene terephthalate composition
US20090043021A1 (en) * 2007-08-06 2009-02-12 Jing-Chung Chang Flame retardant polytrimethylene terephthalate composition
US20090043016A1 (en) * 2007-08-06 2009-02-12 Jing-Chung Chang Flame retardant polytrimethylene terephthalate composition
US20090043017A1 (en) * 2007-08-06 2009-02-12 Jing-Chung Chang Flame retardant polytrimethylene terephthalate composition
US7855244B2 (en) * 2007-08-06 2010-12-21 E.I. Du Pont De Nemours And Company Flame retardant polytrimethylene terephthalate composition
WO2010045181A1 (en) * 2008-10-16 2010-04-22 E. I. Du Pont De Nemours And Company Flame retardant poly(trimethylene terephthalate) composition
WO2010077905A1 (en) 2008-12-17 2010-07-08 E. I. Du Pont De Nemours And Company Poly(trimethylene terephthalate) polymer blends that have reduced whitening
US20100152411A1 (en) 2008-12-17 2010-06-17 E.I. Du Pont De Nemours And Company Poly(trimethylene terephthalate) with reduced whitening
US20100152412A1 (en) 2008-12-17 2010-06-17 E. I. Du Pont De Nemours And Company Reduction of whitening of poly(trimethylene terephthalate) parts by solvent exposure
JP2012519756A (ja) 2009-03-03 2012-08-30 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー オリゴマーが低減したポリ（トリメチレンテレフタレート）ペレット及びオリゴマーの低減を測定する方法
JP2014501810A (ja) 2010-11-22 2014-01-23 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ポリ（１，３−トリメチレンテレフタレート）とポリ（１，３−トリメチレン２，６−ナフタレート）とを含むブロックコポリマー
KR20160047218A (ko) 2014-10-22 2016-05-02 에스케이케미칼주식회사 부산물의 함량이 낮은 폴리(트리메틸렌 테레프탈레이트)의 연속 제조 방법
CN104629021B (zh) * 2015-02-15 2017-07-07 张家港美景荣化学工业有限公司 一种聚对苯二甲酸丙二醇酯及其生产方法
CN105622907A (zh) * 2016-04-08 2016-06-01 张家港美景荣化学工业有限公司 高粘聚对苯二甲酸丙二醇酯及其共聚酯的制备方法
KR20180035522A (ko) * 2016-09-29 2018-04-06 주식회사 엘지화학 폴리에테르에스테르 공중합체의 제조방법
US20210164131A1 (en) 2018-06-28 2021-06-03 Dupont Industrial Biosciences Usa, Llc Fabrics and spun yarns comprising polyester staple fiber
JP2020050820A (ja) * 2018-09-28 2020-04-02 東レ株式会社 高収率ポリエステルの製造方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4424337A (en) 1982-09-07 1984-01-03 The Goodyear Tire & Rubber Company Polyisophthalate and copolymers thereof having reduced cyclic dimer content, and a process for making the same
US4418188A (en) 1982-09-07 1983-11-29 The Goodyear Tire & Rubber Company Polyethylene isophthalate having reduced cyclic dimer content and process therefore
US4835247A (en) 1988-08-08 1989-05-30 The Goodyear Tire & Rubber Company Process for the synthesis of a copolyester adhesive resin
US4921929A (en) 1988-08-08 1990-05-01 The Goodyear Tire & Rubber Company Process for the synthesis of a copolyester adhesive resin
MY118950A (en) 1997-04-30 2005-02-28 Shell Int Research Purification of by- product stream in preparation of polytrimethylene terephthalate
US6245879B1 (en) 1999-01-29 2001-06-12 Shell Oil Company Purification of 1,3-propanediol in carbonyl-containing stream
ES2195465T3 (es) 1999-04-22 2003-12-01 Zimmer Ag Procedimiento para producir poli(tereftalato de trimetileno) (ptt).
US6277947B1 (en) 2000-04-21 2001-08-21 Shell Oil Company Process of producing polytrimethylene terephthalate (PTT)
TR200200463T2 (tr) * 1999-08-25 2003-02-21 E.I. Du Pont De Nemours And Company Düşük seviyeli di(1,3-propilen glikol) ile poli(trimetilen tereftalat) hazırlanması.
US20020123606A1 (en) * 1999-08-26 2002-09-05 Kurian Joseph Varapadavil Poly(trimethylene terephthalate) with low level of DI(1,3-propylene glycol)

Also Published As

Publication number Publication date
EP1456276A1 (en) 2004-09-15
CA2465281A1 (en) 2003-05-08
EP1456276B1 (en) 2008-08-06
JP4074250B2 (ja) 2008-04-09
WO2003037958A1 (en) 2003-05-08
SA03240057B1 (ar) 2007-05-09
CN1273514C (zh) 2006-09-06
TW200302839A (en) 2003-08-16
ATE403689T1 (de) 2008-08-15
MY129191A (en) 2007-03-30
MXPA04004014A (es) 2004-07-23
ES2311646T3 (es) 2009-02-16
DE60228122D1 (de) 2008-09-18
JP2005536574A (ja) 2005-12-02
TWI255276B (en) 2006-05-21
US6657044B1 (en) 2003-12-02
KR20050040830A (ko) 2005-05-03
CN1578800A (zh) 2005-02-09

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Legal Events

Date Code Title Description
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]

Free format text: REFERENTE A 8A ANUI DADE.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: REFERENTE 8.6 DA RPI 2112 DE 28/06/2011.