DE602004002570T2 - Herstellverfahren für amininitiierte polyetherpolyole - Google Patents

Herstellverfahren für amininitiierte polyetherpolyole Download PDF

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Publication number
DE602004002570T2
DE602004002570T2 DE602004002570T DE602004002570T DE602004002570T2 DE 602004002570 T2 DE602004002570 T2 DE 602004002570T2 DE 602004002570 T DE602004002570 T DE 602004002570T DE 602004002570 T DE602004002570 T DE 602004002570T DE 602004002570 T2 DE602004002570 T2 DE 602004002570T2
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Germany
Prior art keywords
polyol
amount
amine
added
catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Revoked
Application number
DE602004002570T
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German (de)
English (en)
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DE602004002570D1 (de
Inventor
L. Nathan Charleston ANDERSON
W. Karl Hurricane HAIDER
J. Keith Paden City HEADLEY
A. Kerry Pittsburgh INGOLD
P. Herman Sedona DOERGE
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Covestro LLC
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Bayer MaterialScience LLC
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Application filed by Bayer MaterialScience LLC filed Critical Bayer MaterialScience LLC
Publication of DE602004002570D1 publication Critical patent/DE602004002570D1/de
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Publication of DE602004002570T2 publication Critical patent/DE602004002570T2/de
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40High-molecular-weight compounds
    • C08G18/48Polyethers
    • C08G18/50Polyethers having heteroatoms other than oxygen
    • C08G18/5021Polyethers having heteroatoms other than oxygen having nitrogen
    • C08G18/5024Polyethers having heteroatoms other than oxygen having nitrogen containing primary and/or secondary amino groups
    • C08G18/5027Polyethers having heteroatoms other than oxygen having nitrogen containing primary and/or secondary amino groups directly linked to carbocyclic groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • C08G18/166Catalysts not provided for in the groups C08G18/18 - C08G18/26
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40High-molecular-weight compounds
    • C08G18/4009Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
    • C08G18/4018Mixtures of compounds of group C08G18/42 with compounds of group C08G18/48
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40High-molecular-weight compounds
    • C08G18/48Polyethers
    • C08G18/50Polyethers having heteroatoms other than oxygen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • C08G18/77Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
    • C08G18/78Nitrogen
    • C08G18/79Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/68Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the catalysts used
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2618Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing nitrogen
    • C08G65/2621Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing nitrogen containing amine groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2618Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing nitrogen
    • C08G65/2621Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing nitrogen containing amine groups
    • C08G65/2627Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing nitrogen containing amine groups containing aromatic or arylaliphatic amine groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30Post-polymerisation treatment, e.g. recovery, purification, drying
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00Foam properties
    • C08G2110/0025Foam properties rigid
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/05Polymer mixtures characterised by other features containing polymer components which can react with one another

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyethers (AREA)
  • Epoxy Resins (AREA)
DE602004002570T 2003-02-21 2004-02-19 Herstellverfahren für amininitiierte polyetherpolyole Revoked DE602004002570T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US372361 2003-02-21
US10/372,361 US6869543B2 (en) 2003-02-21 2003-02-21 Amine-initiated polyether polyols and a process for their production
PCT/US2004/004895 WO2004076529A1 (en) 2003-02-21 2004-02-19 Amine-initiated polyether polyols and a process for their production

Publications (2)

Publication Number Publication Date
DE602004002570D1 DE602004002570D1 (de) 2006-11-09
DE602004002570T2 true DE602004002570T2 (de) 2007-09-06

Family

ID=32868513

Family Applications (1)

Application Number Title Priority Date Filing Date
DE602004002570T Revoked DE602004002570T2 (de) 2003-02-21 2004-02-19 Herstellverfahren für amininitiierte polyetherpolyole

Country Status (15)

Country Link
US (1) US6869543B2 (https=)
EP (1) EP1597300B1 (https=)
JP (1) JP2006518417A (https=)
KR (1) KR101021766B1 (https=)
CN (1) CN100543064C (https=)
AT (1) ATE340818T1 (https=)
BR (1) BRPI0407623B1 (https=)
CA (1) CA2514935C (https=)
DE (1) DE602004002570T2 (https=)
ES (1) ES2273222T3 (https=)
MX (1) MXPA05008806A (https=)
PL (1) PL378062A1 (https=)
PT (1) PT1597300E (https=)
RU (1) RU2359980C2 (https=)
WO (1) WO2004076529A1 (https=)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1817356B2 (en) 2004-11-17 2020-08-19 Dow Global Technologies LLC Acid blocked, amine based, autocatalytic polyols and polyurethane foams made therefrom
JP4813894B2 (ja) * 2005-06-02 2011-11-09 ライオン株式会社 脂肪族第1級アミンアルキレンオキサイド付加物の製造方法、及び乳化剤
JP4629604B2 (ja) * 2006-03-29 2011-02-09 三洋化成工業株式会社 脂肪族アミンアルキレンオキサイド付加物の製造方法
JP2007262250A (ja) * 2006-03-29 2007-10-11 Sanyo Chem Ind Ltd 脂肪族アミンアルキレンオキサイド付加物の製造方法
JP4778925B2 (ja) * 2007-03-29 2011-09-21 三洋化成工業株式会社 液体洗浄剤組成物
DE102007038436A1 (de) 2007-08-16 2009-02-19 Bayer Materialscience Ag Verfahren zur Herstellung von Polyolen
DE102008011683A1 (de) 2008-02-28 2009-09-03 Bayer Materialscience Ag Verfahren zur Herstellung von Polyolen
DE102008028555A1 (de) 2008-06-16 2009-12-17 Bayer Materialscience Ag Verfahren zur Herstellung von Polyolen
DE102009043616A1 (de) 2009-09-29 2011-03-31 Bayer Materialscience Ag Verfahren zur Herstellung von aminogruppenhaltigen Polyolen
EP2365019A1 (de) 2010-03-13 2011-09-14 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
JP5711648B2 (ja) * 2011-11-16 2015-05-07 ライオン株式会社 アルキレンオキシド付加物の製造方法
SG2014014567A (en) 2013-02-22 2014-09-26 Bayer Materialscience Ag Process for preparing polyether polyols
MX337785B (es) 2013-02-22 2016-03-18 Bayer Materialscience Ag Procedimiento de preparacion de polioles de polieter.
JP6931362B2 (ja) 2016-05-13 2021-09-01 コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag ポリオキシアルキレンポリオールの製造方法
CN108250388A (zh) * 2017-12-29 2018-07-06 浙江省三门中鑫实业有限公司 一种低气味低voc全水发泡材料及其制造方法
EP3741788A1 (de) 2019-05-24 2020-11-25 Covestro Deutschland AG Verfahren zur herstellung von polyoxyalkylenpolyol-mischungen
EP3838963A1 (de) 2019-12-17 2021-06-23 Covestro Deutschland AG Verfahren zur herstellung von polyoxyalkylenpolyesterpolyolen
CN111690110B (zh) * 2020-06-22 2022-03-11 上海墨梵新材料科技有限公司 包括含活性基团的聚氨酯催化剂的组合聚醚多元醇及其制备方法
US11529657B2 (en) 2021-03-09 2022-12-20 Covestro Llc Methods for removing amine contaminants from equipment used in the production of polyether polyols
WO2023021103A1 (en) * 2021-08-19 2023-02-23 Basf Se Modified alkoxylated oligoalkylene imines and modified alkoxylated oligoamines
EP4413056B1 (de) 2021-10-07 2025-07-23 Covestro Deutschland AG Verfahren zur herstellung von polyoxyalkylenpolyesterpolyolen
CN117327267A (zh) * 2023-09-07 2024-01-02 山东一诺威新材料有限公司 低粘度苯胺聚醚多元醇及其制备方法和应用
WO2026011280A1 (en) * 2024-07-08 2026-01-15 Dow Global Technologies Llc Methods of controlling cloud point of alkaline catalyzed nonionic surfactants

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GB1311095A (en) * 1969-04-09 1973-03-21 Ici Ltd Alkylene oxide orthotolylene diamine compositions
JPS56112931A (en) * 1980-02-12 1981-09-05 Sanyo Chem Ind Ltd Polyol composition
JPS5770124A (en) * 1980-10-20 1982-04-30 Dai Ichi Kogyo Seiyaku Co Ltd Purification of polyether-polyol
US4391728A (en) 1981-12-01 1983-07-05 Basf Wyandotte Corporation Propylene oxide adducts of toluenediamine
US4562290A (en) 1981-12-01 1985-12-31 Basf Wyandotte Corporation Alkylene oxide adducts of vicinal toluenediamine
US4430490A (en) 1982-08-10 1984-02-07 Ppg Industries, Inc. Polyether polyols and their method of preparation
GB2199504A (en) 1987-01-06 1988-07-13 Peter Egan Directional dice
JPH07108939B2 (ja) * 1988-10-28 1995-11-22 武田薬品工業株式会社 ポリエーテルポリオールの製造法
DE69324427T2 (de) * 1992-03-24 1999-08-05 The Dow Chemical Co., Midland, Mich. Neues endbehandlungsverfahren für hydroxyfunktionelle polythethern
JP3403530B2 (ja) * 1994-12-26 2003-05-06 三井化学株式会社 ポリウレタン用新規ポリエーテルポリオールおよびその製造方法
US5786405A (en) * 1996-11-01 1998-07-28 Bayer Corporation Amine-initiated polyether polyols and a process for their production
PL333050A1 (en) * 1996-11-04 1999-11-08 Ici Plc Rigid polyurethane foams
DE19742012A1 (de) * 1997-09-24 1999-03-25 Basf Ag Temperaturstabile Hartschaumstoffe auf Isocyanatbasis mit geringer Sprödigkeit und niedriger Wärmeleitfähigkeit
US20030158450A1 (en) * 2000-05-15 2003-08-21 Melis Hasselaar Process for the preparation of polyether polyols

Also Published As

Publication number Publication date
CN1759134A (zh) 2006-04-12
US6869543B2 (en) 2005-03-22
EP1597300A1 (en) 2005-11-23
BRPI0407623A (pt) 2006-02-21
BRPI0407623B1 (pt) 2013-12-10
EP1597300B1 (en) 2006-09-27
PL378062A1 (pl) 2006-02-20
CA2514935A1 (en) 2004-09-10
KR101021766B1 (ko) 2011-03-15
MXPA05008806A (es) 2005-10-18
US20040167316A1 (en) 2004-08-26
CN100543064C (zh) 2009-09-23
RU2359980C2 (ru) 2009-06-27
ATE340818T1 (de) 2006-10-15
WO2004076529A1 (en) 2004-09-10
KR20050106017A (ko) 2005-11-08
PT1597300E (pt) 2006-12-29
RU2005129124A (ru) 2006-04-27
ES2273222T3 (es) 2007-05-01
JP2006518417A (ja) 2006-08-10
CA2514935C (en) 2012-01-03
DE602004002570D1 (de) 2006-11-09

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