DE561521C - Verfahren zur Herstellung organischer Sulfopersaeureverbindungen - Google Patents
Verfahren zur Herstellung organischer SulfopersaeureverbindungenInfo
- Publication number
- DE561521C DE561521C DE1930F0104530 DEF0104530D DE561521C DE 561521 C DE561521 C DE 561521C DE 1930F0104530 DE1930F0104530 DE 1930F0104530 DE F0104530 D DEF0104530 D DE F0104530D DE 561521 C DE561521 C DE 561521C
- Authority
- DE
- Germany
- Prior art keywords
- organic
- compounds
- acid
- sulfoperacid
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000001875 compounds Chemical class 0.000 title claims description 7
- 238000000034 method Methods 0.000 title claims description 5
- 238000002360 preparation method Methods 0.000 title claims description 3
- XTHPWXDJESJLNJ-UHFFFAOYSA-N sulfurochloridic acid Chemical class OS(Cl)(=O)=O XTHPWXDJESJLNJ-UHFFFAOYSA-N 0.000 claims description 5
- 150000002978 peroxides Chemical class 0.000 claims description 2
- 239000002253 acid Substances 0.000 description 10
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000001816 cooling Methods 0.000 description 5
- PFUVRDFDKPNGAV-UHFFFAOYSA-N sodium peroxide Chemical compound [Na+].[Na+].[O-][O-] PFUVRDFDKPNGAV-UHFFFAOYSA-N 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 159000000000 sodium salts Chemical class 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 235000021355 Stearic acid Nutrition 0.000 description 2
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 2
- 235000019441 ethanol Nutrition 0.000 description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000008117 stearic acid Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- KEQGZUUPPQEDPF-UHFFFAOYSA-N 1,3-dichloro-5,5-dimethylimidazolidine-2,4-dione Chemical compound CC1(C)N(Cl)C(=O)N(Cl)C1=O KEQGZUUPPQEDPF-UHFFFAOYSA-N 0.000 description 1
- FDHDUXOBMHHFFJ-UHFFFAOYSA-N 1-pentylnaphthalene Chemical compound C1=CC=C2C(CCCCC)=CC=CC2=C1 FDHDUXOBMHHFFJ-UHFFFAOYSA-N 0.000 description 1
- AZQZIJMANBCIPC-UHFFFAOYSA-N 1-pentylnaphthalene sulfurochloridic acid Chemical compound S(=O)(=O)(O)Cl.C(CCCC)C1=CC=CC2=CC=CC=C12 AZQZIJMANBCIPC-UHFFFAOYSA-N 0.000 description 1
- YYROPELSRYBVMQ-UHFFFAOYSA-N 4-toluenesulfonyl chloride Chemical compound CC1=CC=C(S(Cl)(=O)=O)C=C1 YYROPELSRYBVMQ-UHFFFAOYSA-N 0.000 description 1
- 239000004343 Calcium peroxide Substances 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- OUUQCZGPVNCOIJ-UHFFFAOYSA-M Superoxide Chemical compound [O-][O] OUUQCZGPVNCOIJ-UHFFFAOYSA-M 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- LHJQIRIGXXHNLA-UHFFFAOYSA-N calcium peroxide Chemical compound [Ca+2].[O-][O-] LHJQIRIGXXHNLA-UHFFFAOYSA-N 0.000 description 1
- 235000019402 calcium peroxide Nutrition 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000000645 desinfectant Substances 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 235000011180 diphosphates Nutrition 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- AYDPPJFUTOOTRP-UHFFFAOYSA-N naphthalene;sulfurochloridic acid Chemical compound OS(Cl)(=O)=O.C1=CC=CC2=CC=CC=C21 AYDPPJFUTOOTRP-UHFFFAOYSA-N 0.000 description 1
- KBZHCQZECYSILO-UHFFFAOYSA-N octadecanoic acid sulfurochloridic acid Chemical compound S(=O)(=O)(O)Cl.C(CCCCCCCCCCCCCCCCC)(=O)O KBZHCQZECYSILO-UHFFFAOYSA-N 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 150000004967 organic peroxy acids Chemical class 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000012476 oxidizable substance Substances 0.000 description 1
- FHHJDRFHHWUPDG-UHFFFAOYSA-N peroxysulfuric acid Chemical compound OOS(O)(=O)=O FHHJDRFHHWUPDG-UHFFFAOYSA-N 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 229910000108 silver(I,III) oxide Inorganic materials 0.000 description 1
- ZBNMBCAMIKHDAA-UHFFFAOYSA-N sodium superoxide Chemical compound [Na+].O=O ZBNMBCAMIKHDAA-UHFFFAOYSA-N 0.000 description 1
- 229910000144 sodium(I) superoxide Inorganic materials 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- HIFJUMGIHIZEPX-UHFFFAOYSA-N sulfuric acid;sulfur trioxide Chemical compound O=S(=O)=O.OS(O)(=O)=O HIFJUMGIHIZEPX-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE1930F0104530 DE561521C (de) | 1930-11-28 | 1930-11-28 | Verfahren zur Herstellung organischer Sulfopersaeureverbindungen |
| DEF70407D DE600293C (de) | 1930-11-28 | 1931-02-28 | Verfahren zur Herstellung von organischen Sulfopersaeureverbindungen |
| BE384081D BE384081A (enEXAMPLES) | 1930-11-28 | 1931-11-10 | |
| FR726140D FR726140A (fr) | 1930-11-28 | 1931-11-10 | Procédé pour l'obtention de combinaisons organiques de l'acide persulfurique |
| GB1731033A GB396395A (en) | 1930-11-28 | 1931-11-27 | Processes for the production and employment of organic persulpho compounds |
| GB3288831A GB394989A (en) | 1930-11-28 | 1931-11-27 | Process for the production of organic persulpho compounds |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE1930F0104530 DE561521C (de) | 1930-11-28 | 1930-11-28 | Verfahren zur Herstellung organischer Sulfopersaeureverbindungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE561521C true DE561521C (de) | 1932-10-15 |
Family
ID=34559067
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1930F0104530 Expired DE561521C (de) | 1930-11-28 | 1930-11-28 | Verfahren zur Herstellung organischer Sulfopersaeureverbindungen |
| DEF70407D Expired DE600293C (de) | 1930-11-28 | 1931-02-28 | Verfahren zur Herstellung von organischen Sulfopersaeureverbindungen |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF70407D Expired DE600293C (de) | 1930-11-28 | 1931-02-28 | Verfahren zur Herstellung von organischen Sulfopersaeureverbindungen |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE384081A (enEXAMPLES) |
| DE (2) | DE561521C (enEXAMPLES) |
| FR (1) | FR726140A (enEXAMPLES) |
| GB (2) | GB394989A (enEXAMPLES) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2701178A (en) * | 1951-05-24 | 1955-02-01 | Stevenson Dyers Ltd | Permonosulfuric acid treatment of wool, for shrink resistance |
| US2774355A (en) * | 1955-03-23 | 1956-12-18 | Du Pont | Permanent hair waving neutralization by monopersulfate |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2426142A (en) * | 1943-09-01 | 1947-08-19 | Du Pont | Bleaching cotton textile goods |
-
1930
- 1930-11-28 DE DE1930F0104530 patent/DE561521C/de not_active Expired
-
1931
- 1931-02-28 DE DEF70407D patent/DE600293C/de not_active Expired
- 1931-11-10 FR FR726140D patent/FR726140A/fr not_active Expired
- 1931-11-10 BE BE384081D patent/BE384081A/xx unknown
- 1931-11-27 GB GB3288831A patent/GB394989A/en not_active Expired
- 1931-11-27 GB GB1731033A patent/GB396395A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2701178A (en) * | 1951-05-24 | 1955-02-01 | Stevenson Dyers Ltd | Permonosulfuric acid treatment of wool, for shrink resistance |
| US2774355A (en) * | 1955-03-23 | 1956-12-18 | Du Pont | Permanent hair waving neutralization by monopersulfate |
Also Published As
| Publication number | Publication date |
|---|---|
| DE600293C (de) | 1934-07-23 |
| FR726140A (fr) | 1932-05-21 |
| GB394989A (en) | 1933-06-27 |
| GB396395A (en) | 1933-07-27 |
| BE384081A (enEXAMPLES) | 1931-12-31 |
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