DE3339051A1 - Verfahren zur verbesserten destillativen aufarbeitung von glycerin - Google Patents
Verfahren zur verbesserten destillativen aufarbeitung von glycerinInfo
- Publication number
- DE3339051A1 DE3339051A1 DE19833339051 DE3339051A DE3339051A1 DE 3339051 A1 DE3339051 A1 DE 3339051A1 DE 19833339051 DE19833339051 DE 19833339051 DE 3339051 A DE3339051 A DE 3339051A DE 3339051 A1 DE3339051 A1 DE 3339051A1
- Authority
- DE
- Germany
- Prior art keywords
- column
- glycerine
- condenser
- glycerol
- pressure loss
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title claims description 129
- 235000011187 glycerol Nutrition 0.000 title claims description 59
- 238000000034 method Methods 0.000 title claims description 26
- 238000000926 separation method Methods 0.000 claims description 20
- 239000000126 substance Substances 0.000 claims description 17
- 239000000203 mixture Substances 0.000 claims description 16
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 238000004821 distillation Methods 0.000 claims description 12
- 239000003925 fat Substances 0.000 claims description 12
- 150000003839 salts Chemical class 0.000 claims description 9
- 238000007127 saponification reaction Methods 0.000 claims description 8
- 239000010409 thin film Substances 0.000 claims description 8
- 238000004061 bleaching Methods 0.000 claims description 7
- 239000011552 falling film Substances 0.000 claims description 7
- 238000009835 boiling Methods 0.000 claims description 6
- 238000001704 evaporation Methods 0.000 claims description 6
- 230000008020 evaporation Effects 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 5
- 238000005809 transesterification reaction Methods 0.000 claims description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
- 239000007844 bleaching agent Substances 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- 238000010626 work up procedure Methods 0.000 claims description 4
- 238000003776 cleavage reaction Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 230000007017 scission Effects 0.000 claims description 3
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
- 230000000994 depressogenic effect Effects 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 239000000047 product Substances 0.000 description 14
- 235000019197 fats Nutrition 0.000 description 11
- 235000019198 oils Nutrition 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 150000002314 glycerols Chemical class 0.000 description 3
- 239000000344 soap Substances 0.000 description 3
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 description 2
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 2
- PSJBSUHYCGQTHZ-UHFFFAOYSA-N 3-Methoxy-1,2-propanediol Chemical compound COCC(O)CO PSJBSUHYCGQTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 235000019864 coconut oil Nutrition 0.000 description 2
- 239000003240 coconut oil Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 230000008646 thermal stress Effects 0.000 description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- WBVHXPUFAVGIAT-UHFFFAOYSA-N [C].OCC(O)CO Chemical compound [C].OCC(O)CO WBVHXPUFAVGIAT-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000003113 alkalizing effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 235000011116 calcium hydroxide Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000002144 chemical decomposition reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
- B01D3/322—Reboiler specifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/148—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/20—Power plant
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19833339051 DE3339051A1 (de) | 1983-10-28 | 1983-10-28 | Verfahren zur verbesserten destillativen aufarbeitung von glycerin |
| GB08424248A GB2148886B (en) | 1983-10-28 | 1984-09-26 | Working up of glycerin by distillation |
| DE8484112685T DE3467751D1 (en) | 1983-10-28 | 1984-10-20 | Process for the treatment of glycerine by distillation |
| EP84112685A EP0141358B1 (de) | 1983-10-28 | 1984-10-20 | Verfahren zur verbesserten destillativen Aufarbeitung von Glycerin |
| US06/664,902 US4655879A (en) | 1983-10-28 | 1984-10-26 | Glycerol distillation process |
| JP59226624A JPS60109534A (ja) | 1983-10-28 | 1984-10-27 | 蒸留によるグリセリンの処理方法 |
| MYPI87000631A MY102443A (en) | 1983-10-28 | 1987-05-11 | A process for the improved working up of glycerin by distillation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19833339051 DE3339051A1 (de) | 1983-10-28 | 1983-10-28 | Verfahren zur verbesserten destillativen aufarbeitung von glycerin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3339051A1 true DE3339051A1 (de) | 1985-05-09 |
Family
ID=6212891
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19833339051 Withdrawn DE3339051A1 (de) | 1983-10-28 | 1983-10-28 | Verfahren zur verbesserten destillativen aufarbeitung von glycerin |
| DE8484112685T Expired DE3467751D1 (en) | 1983-10-28 | 1984-10-20 | Process for the treatment of glycerine by distillation |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8484112685T Expired DE3467751D1 (en) | 1983-10-28 | 1984-10-20 | Process for the treatment of glycerine by distillation |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4655879A (forum.php) |
| EP (1) | EP0141358B1 (forum.php) |
| JP (1) | JPS60109534A (forum.php) |
| DE (2) | DE3339051A1 (forum.php) |
| GB (1) | GB2148886B (forum.php) |
| MY (1) | MY102443A (forum.php) |
Families Citing this family (66)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5271811A (en) * | 1988-01-29 | 1993-12-21 | Hoechst Celanese Corporation | Process for purifying 2-(4-isobutylphenyl)-propionic acid by vacuum distillation |
| US5061348A (en) * | 1988-08-12 | 1991-10-29 | Alameda Instruments | Sulfuric acid reprocessor with continuous purge of second distillation vessel |
| US4980032A (en) * | 1988-08-12 | 1990-12-25 | Alameda Instruments, Inc. | Distillation method and apparatus for reprocessing sulfuric acid |
| US4936955A (en) * | 1988-08-12 | 1990-06-26 | Alameda Instruments, Inc. | Hydrofluoric acid reprocessing for semiconductor standards |
| DE3832340A1 (de) * | 1988-09-23 | 1990-03-29 | Krupp Koppers Gmbh | Verfahren und vorrichtung zur optimierung des betriebes einer mit einem seitenkocher versehenen abtriebskolonne |
| US4935555A (en) * | 1988-11-25 | 1990-06-19 | Elias Carole L | Purification of neopentyl glycol |
| US4975158A (en) * | 1989-12-27 | 1990-12-04 | Lloyd Bert | Recovery of glycerine from polyols by azeotropic distillation |
| US4980033A (en) * | 1990-09-04 | 1990-12-25 | Lloyd Berg | Recovery of triethylene glycol from triols by azeotropic distillation |
| US5421965A (en) * | 1994-08-01 | 1995-06-06 | Lloyd Berg | Separation of glycerine from bis(hydroxymethyl)tetrahydrofuran by azeotropic distillation |
| US7071913B2 (en) * | 1995-07-20 | 2006-07-04 | E Ink Corporation | Retroreflective electrophoretic displays and materials for making the same |
| EA002043B1 (ru) * | 1997-11-24 | 2001-12-24 | Энергеа Умвельттехнологи Гмбх | Способ получения метилового сложного эфира жирной кислоты и установка для осуществления способа |
| NL1013682C2 (nl) * | 1999-11-26 | 2001-05-30 | Purac Biochem Bv | Werkwijze en inrichting voor het zuiveren van een waterige oplossing van melkzuur. |
| JP3712903B2 (ja) | 2000-01-28 | 2005-11-02 | 花王株式会社 | グリセリンの製造方法 |
| DE10020766B4 (de) * | 2000-04-27 | 2009-11-05 | Cognis Ip Management Gmbh | Verfahren zur Aufbereitung oleochemischer Mehrkomponentengemische |
| DE10140846A1 (de) * | 2001-08-21 | 2003-03-06 | Cognis Deutschland Gmbh | Verfahren zur Herstellung von Dialkylcarbonaten |
| AT504727A1 (de) * | 2002-04-12 | 2008-07-15 | Energea Umwelttechnologie Gmbh | Verfahren und anlage zur veresterung von fettsäuren |
| FR2846964B1 (fr) * | 2002-11-12 | 2006-07-21 | Procede de fabrication de 1,2-epoxy-3-chloropropane | |
| CN101921175B (zh) * | 2003-11-20 | 2012-07-25 | 索尔维公司 | 用于生产有机化合物的方法 |
| US7169946B1 (en) | 2004-03-05 | 2007-01-30 | Twin Rivers Technologies, L.P. | Alternatives to distilled oleo chemicals in derivatives and production thereof |
| KR20080037613A (ko) | 2005-05-20 | 2008-04-30 | 솔베이(소시에떼아노님) | 폴리히드록실화 지방족 탄화수소의 클로로히드린으로의전환 방법 |
| JP5419446B2 (ja) * | 2005-05-20 | 2014-02-19 | ソルヴェイ（ソシエテ アノニム） | 耐腐食性装置内でのクロロヒドリンの調製方法 |
| CN102249859A (zh) | 2005-11-08 | 2011-11-23 | 索尔维公司 | 通过甘油的氯化制备二氯丙醇的方法 |
| EA018774B1 (ru) * | 2006-03-03 | 2013-10-30 | Басф Се | Способ получения 1,2-пропандиола |
| CA2654717A1 (en) * | 2006-06-14 | 2007-12-21 | Solvay (Societe Anonyme) | Crude glycerol-based product, process for its purification and its use in the manufacture of dichloropropanol |
| US20100032617A1 (en) * | 2007-02-20 | 2010-02-11 | Solvay (Societe Anonyme) | Process for manufacturing epichlorohydrin |
| FR2913421B1 (fr) * | 2007-03-07 | 2009-05-15 | Solvay | Procede de fabrication de dichloropropanol. |
| FR2913684B1 (fr) * | 2007-03-14 | 2012-09-14 | Solvay | Procede de fabrication de dichloropropanol |
| FR2913974A1 (fr) * | 2007-03-19 | 2008-09-26 | Arkema France | Procede de vaporisation de glycerol |
| KR101175841B1 (ko) * | 2007-05-15 | 2012-08-24 | 미츠비시 레이온 가부시키가이샤 | 메타크롤레인 또는 (메트)아크릴산의 제조 방법 |
| TW200911740A (en) * | 2007-06-01 | 2009-03-16 | Solvay | Process for manufacturing a chlorohydrin |
| TW200911773A (en) * | 2007-06-12 | 2009-03-16 | Solvay | Epichlorohydrin, manufacturing process and use |
| TW200911693A (en) * | 2007-06-12 | 2009-03-16 | Solvay | Aqueous composition containing a salt, manufacturing process and use |
| FR2918058A1 (fr) * | 2007-06-28 | 2009-01-02 | Solvay | Produit a base de glycerol, procede pour sa purification et son utilisation dans la fabrication de dichloropropanol |
| DE102007034621A1 (de) * | 2007-07-25 | 2009-01-29 | Lanxess Deutschland Gmbh | Polyolreinigung |
| WO2009043796A1 (en) * | 2007-10-02 | 2009-04-09 | Solvay (Société Anonyme) | Use of compositions containing silicon for improving the corrosion resistance of vessels |
| FR2925045B1 (fr) * | 2007-12-17 | 2012-02-24 | Solvay | Produit a base de glycerol, procede pour son obtention et son utilisation dans la fabrication de dichloropropanol |
| DE102007062409A1 (de) | 2007-12-20 | 2009-06-25 | New Environmental Technology Gmbh | Verfahren zur Reinigung von Rohglyzerin |
| TWI478875B (zh) * | 2008-01-31 | 2015-04-01 | Solvay | 使水性組成物中之有機物質降解之方法 |
| US20090198088A1 (en) * | 2008-02-01 | 2009-08-06 | Lanxess Sybron Chemicals Inc. | Process for the purification of crude glycerin utilizing ion exclusion chromatorgraphy and glycerin concentration |
| MX2010010851A (es) * | 2008-04-03 | 2010-11-12 | Solvay | Composicion que comprende glicerol, proceso para obtenerla, y su uso en la elaboracion de dicloropropanol. |
| TWI405749B (zh) * | 2008-07-23 | 2013-08-21 | Wei Ming Chang | 一種由生質柴油製程的副產物製備（醫藥級）甘油的方法 |
| GB0816285D0 (en) * | 2008-09-05 | 2008-10-15 | Chang Wei Ming | Glycerol(medical grade) preperation method using a by-product of a bio-diesel process |
| US7998317B2 (en) * | 2008-09-05 | 2011-08-16 | Wei Ming Chang | Glycerol (medical grade) preparation method using a by-product of a bio-diesel process |
| FR2935968B1 (fr) * | 2008-09-12 | 2010-09-10 | Solvay | Procede pour la purification de chlorure d'hydrogene |
| FR2939434B1 (fr) * | 2008-12-08 | 2012-05-18 | Solvay | Procede de traitement de glycerol. |
| BRPI0902550B1 (pt) * | 2009-01-05 | 2018-04-24 | Senai/dr-ba-serviço Nacional De Aprendizagem Industrial, Departamento Regional Da Bahia | Processo de purificação da glicerina loura, oriunda da transesterificação do biodiesel |
| DE102009017098B3 (de) * | 2009-04-15 | 2010-08-12 | Lurgi Gmbh | Verfahren zur kontinuierlichen Herstellung von Reinglycerin aus Kaliumsulfat enthaltendem Rohglycerin |
| WO2011000976A2 (es) * | 2009-07-01 | 2011-01-06 | Desarrollos Tecnicos Mc, S.L. | Planta para la destilación de glicerina cruda proveniente de la producción de biodiesel |
| EP2295394A1 (en) | 2009-09-11 | 2011-03-16 | Rhodia Poliamida E Especialidades Ltda | Process for the purification of crude glycerol |
| DE102010010738A1 (de) * | 2010-03-09 | 2011-09-15 | Linde Ag | Vergasung von Rohglycerin |
| FR2964657B1 (fr) | 2010-09-15 | 2013-01-18 | Rhodia Operations | Procede de purification du glycerol brut |
| KR20140009163A (ko) | 2010-09-30 | 2014-01-22 | 솔베이(소시에떼아노님) | 천연유래 에피클로로히드린의 유도체 |
| CN103261135A (zh) * | 2010-12-20 | 2013-08-21 | 花王株式会社 | 浓缩甘油的制造方法 |
| US8759595B2 (en) | 2011-10-12 | 2014-06-24 | Vertichem Corporation | Method of biobased chemical production from crude bioglycerin |
| WO2014042937A1 (en) * | 2012-09-14 | 2014-03-20 | Archer Daniels Midland Company | Processes for removing monochloropropanediols and/or glycidol from glycerol |
| US9919991B1 (en) | 2013-11-13 | 2018-03-20 | Whole Energy Fuels Corporation | Systems and methods for purification of glycerin |
| WO2017119007A1 (en) | 2016-01-07 | 2017-07-13 | Institute Of Chemical Technology | Process for purification and refining of glycerol |
| CN106187689B (zh) * | 2016-08-10 | 2019-02-22 | 天津大学 | 一种连续纯化粗甘油的方法 |
| CN106518617A (zh) * | 2016-12-15 | 2017-03-22 | 天长市康宁甘油科技有限公司 | 一种粗甘油的精制回收工艺 |
| KR101969530B1 (ko) * | 2017-08-02 | 2019-04-16 | 지에스칼텍스 주식회사 | 다가 알코올의 탈색 및 탈취 방법 |
| CN109293476B (zh) * | 2018-11-29 | 2021-08-10 | 浙江工业大学 | 一种甘油酯化生产废水中甘油分离工艺及装置 |
| US10773192B1 (en) * | 2019-04-09 | 2020-09-15 | Bitfury Ip B.V. | Method and apparatus for recovering dielectric fluids used for immersion cooling |
| US20240009591A1 (en) * | 2020-11-23 | 2024-01-11 | Covestro Deutschland Ag | Distillation unit and method for separating a liquid substance mixture into two to six liquid product flows with different compositions |
| CN112827204A (zh) * | 2021-02-07 | 2021-05-25 | 吉林凯莱英医药化学有限公司 | 真空提纯装置及提纯系统 |
| CN116510412B (zh) * | 2023-05-24 | 2023-11-17 | 南通凯塔化工科技有限公司 | 一种全角度甘油精炼提纯装置 |
| CN119330539B (zh) * | 2024-11-25 | 2025-04-18 | 青岛丰达利新材料有限公司 | 一种甘油废液一体化回收系统 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA674001A (en) * | 1963-11-12 | I. Denton William | Glycerol manufacture | |
| US1474750A (en) * | 1919-09-20 | 1923-11-20 | Us Ind Alcohol Co | Process of recovering glycerine |
| US1357138A (en) * | 1919-11-03 | 1920-10-26 | Harry P Bassett | Process of treating distillers' slops |
| GB278703A (en) * | 1926-10-11 | 1928-12-13 | Ver Chemische Werke Ag | An improved process for eliminating the unpleasant smell attached to glycerine obtained by fermentation |
| US1936497A (en) * | 1930-10-11 | 1933-11-21 | Du Pont | Method of manufacturing fermentation glycerol |
| US2578816A (en) * | 1949-03-07 | 1951-12-18 | Swift & Co | Glycerin refining |
| GB737570A (en) * | 1952-06-23 | 1955-09-28 | Ici Ltd | Improvements in or relating to the recovery of glycerol from industrial liquors by evaporation |
| FR1138886A (fr) * | 1955-06-21 | 1957-06-20 | Stage Hermann | Procédé et dispositif d'épuration et de concentration de la glycérine par distillation |
| US2960447A (en) * | 1957-07-15 | 1960-11-15 | Shell Oil Co | Purification of synthetic glycerol |
| FR1557590A (forum.php) * | 1968-03-29 | 1969-02-14 | ||
| IT1027410B (it) * | 1974-02-25 | 1978-11-20 | Degussa | Procedimento continuc per la produzione di glicide |
| US4225394A (en) * | 1976-04-14 | 1980-09-30 | Ppg Industries, Inc. | Reclamation of spent glycol by treatment with alkali metal hydroxide and distillation |
-
1983
- 1983-10-28 DE DE19833339051 patent/DE3339051A1/de not_active Withdrawn
-
1984
- 1984-09-26 GB GB08424248A patent/GB2148886B/en not_active Expired
- 1984-10-20 EP EP84112685A patent/EP0141358B1/de not_active Expired
- 1984-10-20 DE DE8484112685T patent/DE3467751D1/de not_active Expired
- 1984-10-26 US US06/664,902 patent/US4655879A/en not_active Expired - Lifetime
- 1984-10-27 JP JP59226624A patent/JPS60109534A/ja active Granted
-
1987
- 1987-05-11 MY MYPI87000631A patent/MY102443A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GB8424248D0 (en) | 1984-10-31 |
| US4655879A (en) | 1987-04-07 |
| EP0141358A1 (de) | 1985-05-15 |
| JPS60109534A (ja) | 1985-06-15 |
| DE3467751D1 (en) | 1988-01-07 |
| EP0141358B1 (de) | 1987-11-25 |
| GB2148886A (en) | 1985-06-05 |
| MY102443A (en) | 1992-06-20 |
| JPH0455180B2 (forum.php) | 1992-09-02 |
| GB2148886B (en) | 1987-09-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| 8130 | Withdrawal |