DE282819C - - Google Patents
Info
- Publication number
- DE282819C DE282819C DENDAT282819D DE282819DA DE282819C DE 282819 C DE282819 C DE 282819C DE NDAT282819 D DENDAT282819 D DE NDAT282819D DE 282819D A DE282819D A DE 282819DA DE 282819 C DE282819 C DE 282819C
- Authority
- DE
- Germany
- Prior art keywords
- acid
- formic acid
- water
- sodium
- boric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 12
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 8
- 239000004327 boric acid Substances 0.000 claims description 8
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 6
- 235000019253 formic acid Nutrition 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 5
- 150000001447 alkali salts Chemical class 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000011734 sodium Substances 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000002253 acid Substances 0.000 description 6
- XQCKCZWQCHDODF-UHFFFAOYSA-N OC=O.OB(O)O Chemical class OC=O.OB(O)O XQCKCZWQCHDODF-UHFFFAOYSA-N 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 159000000000 sodium salts Chemical class 0.000 description 4
- 239000004280 Sodium formate Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- HLBBKKJFGFRGMU-UHFFFAOYSA-M sodium formate Chemical compound [Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 description 3
- 235000019254 sodium formate Nutrition 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/02—Boron compounds
- C07F5/022—Boron compounds without C-boron linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
Publications (1)
Publication Number | Publication Date |
---|---|
DE282819C true DE282819C (xx) |
Family
ID=538439
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DENDAT282819D Active DE282819C (xx) |
Country Status (1)
Country | Link |
---|---|
DE (1) | DE282819C (xx) |
-
0
- DE DENDAT282819D patent/DE282819C/de active Active
Similar Documents
Publication | Publication Date | Title |
---|---|---|
DE282819C (xx) | ||
DE675817C (de) | Verfahren zur Herstellung leicht wasserloeslicher Salze von Diarylaminoalkylcarbinoldn | |
DE125988C (xx) | ||
DE546354C (de) | Verfahren zur Darstellung von Trijodmethansulfonsaeure und deren Salzen | |
DE273221C (xx) | ||
DE586446C (de) | Verfahren zur Darstellung von Guanidinsalzen | |
AT78703B (de) | Verfahren zur Darstellung von therapeutisch wertvollen Verbindungen der Alkaloide der Morphiumgruppe. | |
DE560394C (de) | Verfahren zur Beschleunigung der Kautschukvulkanisation | |
DE216072C (xx) | ||
DE1568773C (de) | Verfahren zur Herstellung des 1-Oxa-S-allyl-S-allophanyl-S-methyl-cyclopentan-2-ons | |
DE633981C (de) | Verfahren zur Herstellung wohldefinierter kristalliner Nitrate des Phenylquecksilberhydroxyds | |
DE454697C (de) | Verfahren zur Darstellung von Verbindungen der 1-Aryl-2-alkyl- und 1-Aryl-2-aralkyl-3, 4-cyclotrimethylen-5-pyrazolone mit Dialkyl- und Arylalkylbarbitursaeuren | |
DE370380C (de) | Verfahren zur Herstellung von Arsensalzen | |
DE511810C (de) | Verfahren zur Darstellung von Gallensauren Salzen der Thiazine | |
DE305855C (de) | Verfahren zum gerben tierischer häute | |
DE858455C (de) | Verfahren zur Herstellung neutraler oder schwach saurer Loesungen von substituierten Xanthinen | |
DE290210C (xx) | ||
DE713079C (de) | Verfahren zur Darstellung von Abkoemmlingen der 4-Aminobenzolsulfonamide | |
DE818047C (de) | Verfahren zur Herstellung von konzentrierten neutralen Loesungen des Theophyllins | |
AT159318B (de) | Verfahren zur Darstellung leicht wasserlöslicher Verbindungen von Dialkylaminoalkyldiarylcarbinolen. | |
DE447352C (de) | Verfahren zur Darstellung von komplexen Antimonverbindungen | |
DE501280C (de) | Verfahren zur Darstellung von 4-(B-Oxyaethylamino-) 1-oxybenzol | |
DE855119C (de) | Verfahren zur Herstellung von Salzen der Ester aus N-substituierten Aminoalkanolen und substituierter oder unsubstituierter p-Aminobenzoesaeure | |
DE117268C (xx) | ||
AT151657B (de) | Verfahren zur Darstellung von Formaldehydnatriumsulfoxylaten von Arsenobenzolverbindungen. |