DE2519300C3 - Verfahren zur Herstellung von Perpropionsäurelösungen unter explosionssicheren Bedingungen - Google Patents
Verfahren zur Herstellung von Perpropionsäurelösungen unter explosionssicheren BedingungenInfo
- Publication number
- DE2519300C3 DE2519300C3 DE2519300A DE2519300A DE2519300C3 DE 2519300 C3 DE2519300 C3 DE 2519300C3 DE 2519300 A DE2519300 A DE 2519300A DE 2519300 A DE2519300 A DE 2519300A DE 2519300 C3 DE2519300 C3 DE 2519300C3
- Authority
- DE
- Germany
- Prior art keywords
- hydrogen peroxide
- reaction
- propionic acid
- acid
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- CZPZWMPYEINMCF-UHFFFAOYSA-N propaneperoxoic acid Chemical compound CCC(=O)OO CZPZWMPYEINMCF-UHFFFAOYSA-N 0.000 title claims description 8
- 238000000034 method Methods 0.000 title claims description 6
- 238000002360 preparation method Methods 0.000 title description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 46
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 42
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 21
- 235000019260 propionic acid Nutrition 0.000 claims description 21
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 21
- 238000006243 chemical reaction Methods 0.000 claims description 14
- 239000011541 reaction mixture Substances 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000000126 substance Substances 0.000 description 8
- 229910000831 Steel Inorganic materials 0.000 description 7
- 239000010959 steel Substances 0.000 description 7
- 239000002360 explosive Substances 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 4
- 229910052739 hydrogen Inorganic materials 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- 238000004880 explosion Methods 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 150000002978 peroxides Chemical class 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 230000008646 thermal stress Effects 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 2
- -1 polyethylene Polymers 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 150000008043 acidic salts Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 238000003421 catalytic decomposition reaction Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000005474 detonation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 150000002500 ions Chemical group 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 150000001451 organic peroxides Chemical class 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- WBHQBSYUUJJSRZ-UHFFFAOYSA-M sodium bisulfate Chemical compound [Na+].OS([O-])(=O)=O WBHQBSYUUJJSRZ-UHFFFAOYSA-M 0.000 description 1
- 229910000342 sodium bisulfate Inorganic materials 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000008542 thermal sensitivity Effects 0.000 description 1
- 239000013585 weight reducing agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/24—Peroxy compounds the —O—O— group being bound between a >C=O group and hydrogen, i.e. peroxy acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (27)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2519300A DE2519300C3 (de) | 1975-04-30 | 1975-04-30 | Verfahren zur Herstellung von Perpropionsäurelösungen unter explosionssicheren Bedingungen |
| SU762350695A SU858562A3 (ru) | 1975-04-30 | 1976-04-23 | Способ получени водных растворов надпропионовой кислоты |
| JP51047905A JPS51133225A (en) | 1975-04-30 | 1976-04-28 | Method of producing perpropionic acid containing solution |
| CS762789A CS189766B2 (en) | 1975-04-30 | 1976-04-28 | Method of preparing perpropionic acid |
| DD192571A DD125929A5 (https=) | 1975-04-30 | 1976-04-28 | |
| AU13417/76A AU494215B2 (en) | 1975-04-30 | 1976-04-28 | Process forthe preparation of perpropionic acid solutions |
| BR2597/76A BR7602597A (pt) | 1975-04-30 | 1976-04-28 | Processo para a preparacao de acido perpropionico |
| IL49485A IL49485A (en) | 1975-04-30 | 1976-04-28 | Prparation of perpropionic acid |
| US05/678,820 US4088679A (en) | 1975-04-30 | 1976-04-28 | Process for the preparation of perpropionic acid solutions |
| ES447412A ES447412A1 (es) | 1975-04-30 | 1976-04-28 | Procedimiento para preparar acido perpropionico. |
| ZA19762527D ZA7602527D (en) | 1975-04-30 | 1976-04-28 | Process for the preparation of perpropionic acid solution |
| GB17183/76A GB1518008A (en) | 1975-04-30 | 1976-04-28 | Process for the preparation of perpropionic acid solution |
| NL7604533A NL7604533A (nl) | 1975-04-30 | 1976-04-28 | Werkwijze ter bereiding van perpropionzuuroplos- singen. |
| BG033052A BG27364A3 (bg) | 1975-04-30 | 1976-04-28 | Метод за получаване на разтвори на перпропионовата киселина |
| IT49231/76A IT1061689B (it) | 1975-04-30 | 1976-04-28 | Procedimento per produrre soluzioni di acido perpropionico |
| PL1976189123A PL98406B1 (pl) | 1975-04-30 | 1976-04-28 | Sposob wytwarzania kwasu nadpropionowego |
| CA251,292A CA1058212A (en) | 1975-04-30 | 1976-04-28 | Process for the preparation of perpropionic acid solutions |
| CH536176A CH601223A5 (https=) | 1975-04-30 | 1976-04-28 | |
| RO7685936A RO74966A (ro) | 1975-04-30 | 1976-04-28 | Procedeu de preparare a acidului perpropionic |
| NO761474A NO142121C (no) | 1975-04-30 | 1976-04-28 | Fremgangsmaate til fremstilling av perpropionsyreopploesoninger |
| FI761182A FI761182A7 (https=) | 1975-04-30 | 1976-04-28 | |
| SE7604888A SE418081B (sv) | 1975-04-30 | 1976-04-28 | Sett att framstella perpropionsyralosningar |
| FR7612613A FR2309532A1 (fr) | 1975-04-30 | 1976-04-28 | Procede de preparation de solutions d'acide perpropionique |
| IE894/76A IE42802B1 (en) | 1975-04-30 | 1976-04-28 | Process for the preparation of perpropionic acid solutions |
| AR263147A AR212705A1 (es) | 1975-04-30 | 1976-04-28 | Procedimiento para la produccion de soluciones de acido perpropionico |
| BE2054993A BE841210A (fr) | 1975-04-30 | 1976-04-28 | Procede de preparation de solutions d'acide perpropionique |
| AT311076A AT344676B (de) | 1975-04-30 | 1976-04-28 | Verfahren zur herstellung einer perpropionsaeureloesung |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2519300A DE2519300C3 (de) | 1975-04-30 | 1975-04-30 | Verfahren zur Herstellung von Perpropionsäurelösungen unter explosionssicheren Bedingungen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2519300A1 DE2519300A1 (de) | 1976-11-11 |
| DE2519300B2 DE2519300B2 (de) | 1978-10-19 |
| DE2519300C3 true DE2519300C3 (de) | 1979-06-13 |
Family
ID=5945453
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2519300A Expired DE2519300C3 (de) | 1975-04-30 | 1975-04-30 | Verfahren zur Herstellung von Perpropionsäurelösungen unter explosionssicheren Bedingungen |
Country Status (25)
| Country | Link |
|---|---|
| US (1) | US4088679A (https=) |
| JP (1) | JPS51133225A (https=) |
| AR (1) | AR212705A1 (https=) |
| AT (1) | AT344676B (https=) |
| BE (1) | BE841210A (https=) |
| BG (1) | BG27364A3 (https=) |
| BR (1) | BR7602597A (https=) |
| CA (1) | CA1058212A (https=) |
| CH (1) | CH601223A5 (https=) |
| CS (1) | CS189766B2 (https=) |
| DD (1) | DD125929A5 (https=) |
| DE (1) | DE2519300C3 (https=) |
| ES (1) | ES447412A1 (https=) |
| FI (1) | FI761182A7 (https=) |
| FR (1) | FR2309532A1 (https=) |
| GB (1) | GB1518008A (https=) |
| IE (1) | IE42802B1 (https=) |
| IL (1) | IL49485A (https=) |
| IT (1) | IT1061689B (https=) |
| NL (1) | NL7604533A (https=) |
| NO (1) | NO142121C (https=) |
| PL (1) | PL98406B1 (https=) |
| RO (1) | RO74966A (https=) |
| SE (1) | SE418081B (https=) |
| ZA (1) | ZA7602527D (https=) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2462425A1 (fr) * | 1979-08-01 | 1981-02-13 | Air Liquide | Procede de fabrication de solutions diluees stables de peracides carboxyliques aliphatiques |
| JPH05100648A (ja) * | 1991-10-04 | 1993-04-23 | Mitsubishi Electric Corp | テストパターン発生装置 |
| GB2548137A (en) * | 2016-03-09 | 2017-09-13 | Perstorp Ab | Production equipment (I) for production of a caprolactone |
| GB2548138A (en) * | 2016-03-09 | 2017-09-13 | Perstorp Ab | Production equipment (II) for production of a caprolactone |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA735489A (en) * | 1966-05-31 | Weiberg Otto | Process of producing solutions of pure aliphatic percarboxylic acids | |
| CA744391A (en) * | 1966-10-11 | J. Wenzke Carroll | Method of producing peracids | |
| NL267716A (https=) * | 1960-08-06 | |||
| FR1352479A (fr) * | 1962-04-04 | 1964-02-14 | Fmc Corp | Procédé de production de peracides aliphatiques inférieurs |
-
1975
- 1975-04-30 DE DE2519300A patent/DE2519300C3/de not_active Expired
-
1976
- 1976-04-28 CH CH536176A patent/CH601223A5/xx not_active IP Right Cessation
- 1976-04-28 GB GB17183/76A patent/GB1518008A/en not_active Expired
- 1976-04-28 BG BG033052A patent/BG27364A3/xx unknown
- 1976-04-28 ES ES447412A patent/ES447412A1/es not_active Expired
- 1976-04-28 CS CS762789A patent/CS189766B2/cs unknown
- 1976-04-28 SE SE7604888A patent/SE418081B/xx not_active IP Right Cessation
- 1976-04-28 DD DD192571A patent/DD125929A5/xx unknown
- 1976-04-28 IL IL49485A patent/IL49485A/xx unknown
- 1976-04-28 FR FR7612613A patent/FR2309532A1/fr active Granted
- 1976-04-28 BE BE2054993A patent/BE841210A/xx not_active IP Right Cessation
- 1976-04-28 JP JP51047905A patent/JPS51133225A/ja active Granted
- 1976-04-28 IE IE894/76A patent/IE42802B1/en unknown
- 1976-04-28 PL PL1976189123A patent/PL98406B1/pl unknown
- 1976-04-28 RO RO7685936A patent/RO74966A/ro unknown
- 1976-04-28 ZA ZA19762527D patent/ZA7602527D/xx unknown
- 1976-04-28 NO NO761474A patent/NO142121C/no unknown
- 1976-04-28 IT IT49231/76A patent/IT1061689B/it active
- 1976-04-28 AT AT311076A patent/AT344676B/de not_active IP Right Cessation
- 1976-04-28 FI FI761182A patent/FI761182A7/fi not_active Application Discontinuation
- 1976-04-28 US US05/678,820 patent/US4088679A/en not_active Expired - Lifetime
- 1976-04-28 NL NL7604533A patent/NL7604533A/xx not_active Application Discontinuation
- 1976-04-28 AR AR263147A patent/AR212705A1/es active
- 1976-04-28 BR BR2597/76A patent/BR7602597A/pt unknown
- 1976-04-28 CA CA251,292A patent/CA1058212A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA1058212A (en) | 1979-07-10 |
| AT344676B (de) | 1978-08-10 |
| FR2309532B1 (https=) | 1981-04-30 |
| JPS51133225A (en) | 1976-11-18 |
| BR7602597A (pt) | 1976-11-23 |
| IE42802B1 (en) | 1980-10-22 |
| RO74966A (ro) | 1982-09-09 |
| AR212705A1 (es) | 1978-09-15 |
| AU1341776A (en) | 1977-11-03 |
| BE841210A (fr) | 1976-10-28 |
| DE2519300A1 (de) | 1976-11-11 |
| GB1518008A (en) | 1978-07-19 |
| DD125929A5 (https=) | 1977-06-01 |
| PL98406B1 (pl) | 1978-05-31 |
| SE7604888L (sv) | 1976-10-31 |
| CH601223A5 (https=) | 1978-06-30 |
| IT1061689B (it) | 1983-04-30 |
| ZA7602527D (en) | 1977-04-27 |
| IL49485A (en) | 1978-12-17 |
| CS189766B2 (en) | 1979-04-30 |
| DE2519300B2 (de) | 1978-10-19 |
| ATA311076A (de) | 1977-12-15 |
| JPS5753784B2 (https=) | 1982-11-15 |
| NL7604533A (nl) | 1976-11-02 |
| US4088679A (en) | 1978-05-09 |
| IE42802L (en) | 1976-10-30 |
| BG27364A3 (bg) | 1979-10-12 |
| FR2309532A1 (fr) | 1976-11-26 |
| IL49485A0 (en) | 1976-06-30 |
| NO761474L (https=) | 1976-11-02 |
| ES447412A1 (es) | 1977-07-01 |
| SE418081B (sv) | 1981-05-04 |
| NO142121B (no) | 1980-03-24 |
| NO142121C (no) | 1980-07-02 |
| FI761182A7 (https=) | 1976-10-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |