DE2507385C3 - Verfahren zur Herstellung eines Räuchermittels - Google Patents
Verfahren zur Herstellung eines RäuchermittelsInfo
- Publication number
- DE2507385C3 DE2507385C3 DE2507385A DE2507385A DE2507385C3 DE 2507385 C3 DE2507385 C3 DE 2507385C3 DE 2507385 A DE2507385 A DE 2507385A DE 2507385 A DE2507385 A DE 2507385A DE 2507385 C3 DE2507385 C3 DE 2507385C3
- Authority
- DE
- Germany
- Prior art keywords
- distillation
- tar
- weight
- smoke condensate
- fumigant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 28
- 239000002316 fumigant Substances 0.000 title claims description 23
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000004821 distillation Methods 0.000 claims description 28
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 24
- 239000000779 smoke Substances 0.000 claims description 21
- 238000009835 boiling Methods 0.000 claims description 16
- 230000000391 smoking effect Effects 0.000 claims description 15
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 14
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 14
- 150000001875 compounds Chemical class 0.000 claims description 14
- 239000000243 solution Substances 0.000 claims description 13
- 238000000605 extraction Methods 0.000 claims description 11
- 235000011187 glycerol Nutrition 0.000 claims description 11
- 125000001477 organic nitrogen group Chemical group 0.000 claims description 11
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 8
- 239000000126 substance Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 7
- 239000012298 atmosphere Substances 0.000 claims description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 235000011007 phosphoric acid Nutrition 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- 238000001179 sorption measurement Methods 0.000 claims description 6
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 4
- 239000001913 cellulose Substances 0.000 claims description 4
- 229920002678 cellulose Polymers 0.000 claims description 4
- 238000000354 decomposition reaction Methods 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 4
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 3
- -1 aliphatic Alcohols Chemical class 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 239000000428 dust Substances 0.000 claims description 3
- 239000011261 inert gas Substances 0.000 claims description 3
- 229910052753 mercury Inorganic materials 0.000 claims description 3
- 239000003960 organic solvent Substances 0.000 claims description 3
- 229920006395 saturated elastomer Polymers 0.000 claims description 3
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- 239000011701 zinc Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 150000001983 dialkylethers Chemical class 0.000 claims description 2
- 150000008282 halocarbons Chemical class 0.000 claims description 2
- 229920005610 lignin Polymers 0.000 claims description 2
- 239000002808 molecular sieve Substances 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 239000000741 silica gel Substances 0.000 claims description 2
- 229910002027 silica gel Inorganic materials 0.000 claims description 2
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 2
- 235000013325 dietary fiber Nutrition 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 238000005191 phase separation Methods 0.000 claims 1
- 239000011269 tar Substances 0.000 description 19
- 239000000047 product Substances 0.000 description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 235000013305 food Nutrition 0.000 description 8
- 239000000203 mixture Substances 0.000 description 8
- 239000002023 wood Substances 0.000 description 7
- 239000007858 starting material Substances 0.000 description 6
- 230000000711 cancerogenic effect Effects 0.000 description 5
- 231100000315 carcinogenic Toxicity 0.000 description 5
- 238000000197 pyrolysis Methods 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 150000005846 sugar alcohols Polymers 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 235000019441 ethanol Nutrition 0.000 description 3
- 239000003925 fat Substances 0.000 description 3
- 235000019197 fats Nutrition 0.000 description 3
- 150000002989 phenols Chemical class 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 235000002639 sodium chloride Nutrition 0.000 description 3
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 241000219495 Betulaceae Species 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 241001070947 Fagus Species 0.000 description 2
- 235000010099 Fagus sylvatica Nutrition 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 235000006708 antioxidants Nutrition 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000000895 extractive distillation Methods 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 235000007586 terpenes Nutrition 0.000 description 2
- 239000003981 vehicle Substances 0.000 description 2
- KRQUFUKTQHISJB-YYADALCUSA-N 2-[(E)-N-[2-(4-chlorophenoxy)propoxy]-C-propylcarbonimidoyl]-3-hydroxy-5-(thian-3-yl)cyclohex-2-en-1-one Chemical compound CCC\C(=N/OCC(C)OC1=CC=C(Cl)C=C1)C1=C(O)CC(CC1=O)C1CCCSC1 KRQUFUKTQHISJB-YYADALCUSA-N 0.000 description 1
- FMMWHPNWAFZXNH-UHFFFAOYSA-N Benz[a]pyrene Chemical compound C1=C2C3=CC=CC=C3C=C(C=C3)C2=C2C3=CC=CC2=C1 FMMWHPNWAFZXNH-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- RAASUWZPTOJQAY-UHFFFAOYSA-N Dibenz[a,c]anthracene Chemical compound C1=CC=C2C3=CC4=CC=CC=C4C=C3C3=CC=CC=C3C2=C1 RAASUWZPTOJQAY-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241000589614 Pseudomonas stutzeri Species 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000012223 aqueous fraction Substances 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- TXVHTIQJNYSSKO-UHFFFAOYSA-N benzo[e]pyrene Chemical class C1=CC=C2C3=CC=CC=C3C3=CC=CC4=CC=C1C2=C34 TXVHTIQJNYSSKO-UHFFFAOYSA-N 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000005686 electrostatic field Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 238000012643 polycondensation polymerization Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- SLGBZMMZGDRARJ-UHFFFAOYSA-N triphenylene Chemical compound C1=CC=C2C3=CC=CC=C3C3=CC=CC=C3C2=C1 SLGBZMMZGDRARJ-UHFFFAOYSA-N 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000011276 wood tar Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/20—Synthetic spices, flavouring agents or condiments
- A23L27/27—Smoke flavours
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compounds Of Unknown Constitution (AREA)
- Seasonings (AREA)
- Medicines Containing Plant Substances (AREA)
- Indole Compounds (AREA)
- General Preparation And Processing Of Foods (AREA)
- Meat, Egg Or Seafood Products (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL1974169004A PL96145B3 (pl) | 1974-02-22 | 1974-02-22 | Sposob wytwarzania srodka aromatyzujacego i/lub antyseptycznego i/lub przeciwdzialajacego utlenianiu |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2507385A1 DE2507385A1 (de) | 1975-08-28 |
| DE2507385B2 DE2507385B2 (de) | 1979-10-25 |
| DE2507385C3 true DE2507385C3 (de) | 1980-07-03 |
Family
ID=19966186
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2507385A Expired DE2507385C3 (de) | 1974-02-22 | 1975-02-20 | Verfahren zur Herstellung eines Räuchermittels |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS517159A (en:Method) |
| AR (1) | AR209293A1 (en:Method) |
| CA (1) | CA1056645A (en:Method) |
| CH (1) | CH614845A5 (en:Method) |
| DE (1) | DE2507385C3 (en:Method) |
| DK (1) | DK68575A (en:Method) |
| FI (1) | FI57689C (en:Method) |
| FR (1) | FR2262100B1 (en:Method) |
| GB (1) | GB1504406A (en:Method) |
| IE (1) | IE40680B1 (en:Method) |
| NL (1) | NL7502109A (en:Method) |
| NO (1) | NO140365C (en:Method) |
| PL (1) | PL96145B3 (en:Method) |
| SE (1) | SE405929B (en:Method) |
| SU (1) | SU575008A3 (en:Method) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4154866A (en) * | 1976-08-24 | 1979-05-15 | Stange Co. | Method of producing from wood tar a liquid smoke product for use in food processing, and product of said method |
| US4594251A (en) * | 1983-04-08 | 1986-06-10 | Union Carbide Corporation | Preparation of tar-depleted liquid smoke treated casings |
| WO2005117612A1 (en) * | 2004-06-04 | 2005-12-15 | Kim Plaschke | Preparation of smoke extract |
| CN111165869B (zh) * | 2020-01-17 | 2021-11-05 | 湖南中烟工业有限责任公司 | 一种经低危害增烟处理的卷烟 |
-
1974
- 1974-02-22 PL PL1974169004A patent/PL96145B3/xx unknown
-
1975
- 1975-02-17 FI FI750433A patent/FI57689C/fi not_active IP Right Cessation
- 1975-02-18 NO NO750544A patent/NO140365C/no unknown
- 1975-02-20 DE DE2507385A patent/DE2507385C3/de not_active Expired
- 1975-02-20 SE SE7501926A patent/SE405929B/xx unknown
- 1975-02-21 GB GB7434/75A patent/GB1504406A/en not_active Expired
- 1975-02-21 NL NL7502109A patent/NL7502109A/xx not_active Application Discontinuation
- 1975-02-21 JP JP50021789A patent/JPS517159A/ja active Pending
- 1975-02-21 DK DK68575*#A patent/DK68575A/da not_active Application Discontinuation
- 1975-02-21 IE IE361/75A patent/IE40680B1/xx unknown
- 1975-02-21 CA CA220,598A patent/CA1056645A/en not_active Expired
- 1975-02-21 SU SU7502110025A patent/SU575008A3/ru active
- 1975-02-21 CH CH217075A patent/CH614845A5/xx not_active IP Right Cessation
- 1975-02-24 AR AR257729A patent/AR209293A1/es active
- 1975-02-24 FR FR7505669A patent/FR2262100B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA1056645A (en) | 1979-06-19 |
| SE405929B (sv) | 1979-01-15 |
| FI750433A7 (en:Method) | 1975-08-23 |
| SE7501926L (en:Method) | 1975-08-25 |
| AU7848275A (en) | 1976-08-26 |
| IE40680B1 (en) | 1979-08-01 |
| JPS517159A (en) | 1976-01-21 |
| NO750544L (en:Method) | 1975-08-25 |
| DE2507385B2 (de) | 1979-10-25 |
| FR2262100A1 (en:Method) | 1975-09-19 |
| NO140365B (no) | 1979-05-14 |
| NL7502109A (nl) | 1975-08-26 |
| FI57689C (fi) | 1980-10-10 |
| FI57689B (fi) | 1980-06-30 |
| CH614845A5 (en) | 1979-12-28 |
| DE2507385A1 (de) | 1975-08-28 |
| AR209293A1 (es) | 1977-04-15 |
| NO140365C (no) | 1979-08-22 |
| GB1504406A (en) | 1978-03-22 |
| FR2262100B1 (en:Method) | 1978-10-27 |
| DK68575A (en:Method) | 1975-10-27 |
| IE40680L (en) | 1975-08-22 |
| PL96145B3 (pl) | 1977-12-31 |
| SU575008A3 (ru) | 1977-09-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |