DE2222033C2 - Redispergierbares Copolymerpulver - Google Patents
Redispergierbares CopolymerpulverInfo
- Publication number
- DE2222033C2 DE2222033C2 DE2222033A DE2222033A DE2222033C2 DE 2222033 C2 DE2222033 C2 DE 2222033C2 DE 2222033 A DE2222033 A DE 2222033A DE 2222033 A DE2222033 A DE 2222033A DE 2222033 C2 DE2222033 C2 DE 2222033C2
- Authority
- DE
- Germany
- Prior art keywords
- dispersion
- drying
- percent
- weight
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000843 powder Substances 0.000 title claims description 22
- 229920001577 copolymer Polymers 0.000 title claims description 12
- 239000006185 dispersion Substances 0.000 claims description 27
- 238000001035 drying Methods 0.000 claims description 12
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 6
- 239000005977 Ethylene Substances 0.000 claims description 6
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
- 239000011230 binding agent Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 238000003860 storage Methods 0.000 claims description 4
- 238000000889 atomisation Methods 0.000 claims description 3
- 239000011256 inorganic filler Substances 0.000 claims description 3
- 229910003475 inorganic filler Inorganic materials 0.000 claims description 3
- 229920000642 polymer Polymers 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 claims description 2
- 230000001070 adhesive effect Effects 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000007789 gas Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- 239000003973 paint Substances 0.000 claims description 2
- 238000006116 polymerization reaction Methods 0.000 claims description 2
- 239000001692 EU approved anti-caking agent Substances 0.000 claims 6
- 239000000945 filler Substances 0.000 claims 6
- 238000001694 spray drying Methods 0.000 claims 4
- 229920001567 vinyl ester resin Polymers 0.000 claims 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 3
- -1 acyl radical Chemical class 0.000 claims 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 2
- 238000004108 freeze drying Methods 0.000 claims 2
- 229920003023 plastic Polymers 0.000 claims 2
- 239000004033 plastic Substances 0.000 claims 2
- 239000000126 substance Substances 0.000 claims 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims 2
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims 1
- 150000003926 acrylamides Chemical class 0.000 claims 1
- 239000000654 additive Substances 0.000 claims 1
- 230000000996 additive effect Effects 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 239000012736 aqueous medium Substances 0.000 claims 1
- 238000010276 construction Methods 0.000 claims 1
- HDERJYVLTPVNRI-UHFFFAOYSA-N ethene;ethenyl acetate Chemical group C=C.CC(=O)OC=C HDERJYVLTPVNRI-UHFFFAOYSA-N 0.000 claims 1
- GLVVKKSPKXTQRB-UHFFFAOYSA-N ethenyl dodecanoate Chemical compound CCCCCCCCCCCC(=O)OC=C GLVVKKSPKXTQRB-UHFFFAOYSA-N 0.000 claims 1
- AFSIMBWBBOJPJG-UHFFFAOYSA-N ethenyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC=C AFSIMBWBBOJPJG-UHFFFAOYSA-N 0.000 claims 1
- UIWXSTHGICQLQT-UHFFFAOYSA-N ethenyl propanoate Chemical compound CCC(=O)OC=C UIWXSTHGICQLQT-UHFFFAOYSA-N 0.000 claims 1
- 229920001038 ethylene copolymer Polymers 0.000 claims 1
- 238000005469 granulation Methods 0.000 claims 1
- 230000003179 granulation Effects 0.000 claims 1
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical group CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 claims 1
- WCYWZMWISLQXQU-UHFFFAOYSA-N methyl Chemical group [CH3] WCYWZMWISLQXQU-UHFFFAOYSA-N 0.000 claims 1
- 239000000178 monomer Substances 0.000 claims 1
- 239000007921 spray Substances 0.000 claims 1
- 238000011282 treatment Methods 0.000 claims 1
- 229920002554 vinyl polymer Polymers 0.000 claims 1
- 239000010408 film Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 229920006254 polymer film Polymers 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- LSXWFXONGKSEMY-UHFFFAOYSA-N di-tert-butyl peroxide Chemical compound CC(C)(C)OOC(C)(C)C LSXWFXONGKSEMY-UHFFFAOYSA-N 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 description 1
- 235000010262 sodium metabisulphite Nutrition 0.000 description 1
- 229940048086 sodium pyrophosphate Drugs 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- 238000009988 textile finishing Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F218/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid or of a haloformic acid
- C08F218/02—Esters of monocarboxylic acids
- C08F218/04—Vinyl esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L31/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid or of a haloformic acid; Compositions of derivatives of such polymers
- C08L31/02—Homopolymers or copolymers of esters of monocarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2331/00—Characterised by the use of copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, or carbonic acid, or of a haloformic acid
- C08J2331/02—Characterised by the use of omopolymers or copolymers of esters of monocarboxylic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Graft Or Block Polymers (AREA)
Priority Applications (20)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2222033A DE2222033C2 (de) | 1972-05-05 | 1972-05-05 | Redispergierbares Copolymerpulver |
| NL7305939A NL7305939A (en:Method) | 1972-05-05 | 1973-04-27 | |
| ZA732865A ZA732865B (en) | 1972-05-05 | 1973-04-27 | Dispersible copolymer power |
| ES414254A ES414254A1 (es) | 1972-05-05 | 1973-04-30 | Procedimiento para la obtencion de polvo copolimero de dis-persion. |
| JP4857173A JPS5734293B2 (en:Method) | 1972-05-05 | 1973-05-02 | |
| US05/356,405 US3950302A (en) | 1972-05-05 | 1973-05-02 | Dispersible copolymer powder |
| CH624773A CH584239A5 (en:Method) | 1972-05-05 | 1973-05-02 | |
| AR247810A AR197225A1 (es) | 1972-05-05 | 1973-05-03 | Polvo copolimero de dispersion y procedimiento para su obtencion |
| AT389173A AT329860B (de) | 1972-05-05 | 1973-05-03 | Verfahren zur herstellung eines dispersionspulvers |
| IT23682/73A IT987116B (it) | 1972-05-05 | 1973-05-03 | Polvere a dispersione copolimera |
| AU55164/73A AU478427B2 (en) | 1972-05-05 | 1973-05-03 | Dispersible copolymer powder |
| FI1406/73A FI59108C (fi) | 1972-05-05 | 1973-05-03 | Aoterdispergerbart copolymerpulver foer framstaellning av emulgatorfria stabila vattenhaltiga dispersioner och foerfarande foer framstaellning av detsamma |
| BR3184/73A BR7303184D0 (pt) | 1972-05-05 | 1973-05-03 | Composicao de po de dispersao copolimero |
| SE7306298A SE392473B (sv) | 1972-05-05 | 1973-05-04 | Aterdispergerbart sampolymerpulver och forfarande for framstellning herav |
| CA170,503A CA1011039A (en) | 1972-05-05 | 1973-05-04 | Dispersible copolymer powder |
| NO1855/73A NO142753C (no) | 1972-05-05 | 1973-05-04 | Redispergerbart kopolymerpulver og fremgangsmaate til fremstilling derav. |
| GB2135573A GB1408361A (en) | 1972-05-05 | 1973-05-04 | Water-dispersible copolymer powder |
| FR7316153A FR2183810B1 (en:Method) | 1972-05-05 | 1973-05-04 | |
| DK247373A DK146322C (da) | 1972-05-05 | 1973-05-04 | Redispergerbart copolymerpulver til fremstilling af vandige emulgatorfri copolymerdispersioner |
| BE130833A BE799199A (fr) | 1972-05-05 | 1973-05-07 | Poudres de copolymeres, obtenues a partir de dispersions et redispersables |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2222033A DE2222033C2 (de) | 1972-05-05 | 1972-05-05 | Redispergierbares Copolymerpulver |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2222033A1 DE2222033A1 (de) | 1973-11-22 |
| DE2222033C2 true DE2222033C2 (de) | 1982-11-25 |
Family
ID=5844133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2222033A Expired DE2222033C2 (de) | 1972-05-05 | 1972-05-05 | Redispergierbares Copolymerpulver |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US3950302A (en:Method) |
| JP (1) | JPS5734293B2 (en:Method) |
| AR (1) | AR197225A1 (en:Method) |
| AT (1) | AT329860B (en:Method) |
| BE (1) | BE799199A (en:Method) |
| BR (1) | BR7303184D0 (en:Method) |
| CA (1) | CA1011039A (en:Method) |
| CH (1) | CH584239A5 (en:Method) |
| DE (1) | DE2222033C2 (en:Method) |
| DK (1) | DK146322C (en:Method) |
| ES (1) | ES414254A1 (en:Method) |
| FI (1) | FI59108C (en:Method) |
| FR (1) | FR2183810B1 (en:Method) |
| GB (1) | GB1408361A (en:Method) |
| IT (1) | IT987116B (en:Method) |
| NL (1) | NL7305939A (en:Method) |
| NO (1) | NO142753C (en:Method) |
| SE (1) | SE392473B (en:Method) |
| ZA (1) | ZA732865B (en:Method) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0690278A1 (de) | 1994-06-29 | 1996-01-03 | Hoechst Aktiengesellschaft | Vorrichtung und Verfahren zum Eintrag von Zuschlagstoffen in Scheibenzerstäubungstrocknern |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3702997A1 (de) * | 1987-02-02 | 1988-08-11 | Roehm Gmbh | Verfahren zur herstellung eines redispergierbaren kunststoffpulvers |
| US4740394A (en) * | 1986-09-08 | 1988-04-26 | National Starch And Chemical Corporation | Textile coatings based on eva-maleate copolymers |
| US4737386A (en) * | 1986-09-08 | 1988-04-12 | National Starch And Chemical Corporation | Textile coating composition and textiles coated therewith |
| US4866119A (en) * | 1986-09-08 | 1989-09-12 | National Starch And Chemical Corporation | Textile coatings based on eva-maleate copolymers |
| US4963422A (en) * | 1987-10-28 | 1990-10-16 | National Starch And Chemical Investment Holding Corporation | Ethylene vinyl acetate alkyl acrylate compositions for flocking adhesives |
| US5416181A (en) * | 1989-02-10 | 1995-05-16 | Penford Products Company | Reinforced films made from water soluble polymers |
| US5173317A (en) * | 1991-10-29 | 1992-12-22 | Wm. Wrigley Jr. Company | Gum compositions containing vinyl laurate/vinyl acetate copolymer |
| DE4304313A1 (de) * | 1993-02-12 | 1994-08-18 | Hoechst Ag | Verwendung von Copolymeren auf Basis von Vinylmonomeren und Carbonsäureamiden als Waschmittelzusatz |
| DE4432899A1 (de) * | 1994-09-15 | 1996-03-21 | Wacker Chemie Gmbh | Vernetzbare Polymerpulver-Zusammensetzungen |
| DE69520423T2 (de) * | 1995-01-06 | 2001-10-18 | Rohm And Haas Co., Philadelphia | Wasserdispergierbare Pulverzusammensetzung für wasserbeständige Überzugsmittel |
| DE19709254A1 (de) | 1997-03-06 | 1998-09-10 | Wacker Chemie Gmbh | Verfahren zur Herstellung von schutzkolloidfreien Dispersionen und Dispersionspulvern |
| EP3126431B1 (en) | 2014-03-31 | 2019-12-25 | Wacker Chemical Corporation | Opacifying additive |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2194354A (en) * | 1933-10-25 | 1940-03-19 | Ici Ltd | Process for preparing polymeric vinyl esters in granular form |
| US2947735A (en) * | 1957-01-02 | 1960-08-02 | Bayer Ag | Process for the production of copolymers of ethylene |
| US3104234A (en) * | 1958-06-30 | 1963-09-17 | Products obtained thereby | |
| US3380851A (en) * | 1965-03-31 | 1968-04-30 | Air Reduction | Nonwoven fabric with vinyl acetateethylene-n-methylol acrylamide interpolymer as binder |
| FR1472857A (fr) * | 1965-03-31 | 1967-03-10 | Cumberland Chemical Company | Composition pour étoffes non tissées ou articles analogues et produits obtenus |
| US3463751A (en) * | 1965-06-16 | 1969-08-26 | Nippon Synthetic Chem Ind | Dry powdery nonblocking vinyl ester-ethylene copolymer compositions and process for the production thereof |
| US3451982A (en) * | 1965-08-04 | 1969-06-24 | Monsanto Co | Terpolymers of ethylene,a vinyl ester and an unsaturated amide |
| US3365409A (en) * | 1965-10-18 | 1968-01-23 | Shawinigan Chem Ltd | Vinyl acetate-acrylamide copolymer emulsions |
| US3577376A (en) * | 1967-12-06 | 1971-05-04 | Gulf Oil Canada Ltd | Interpolymerization of acrylamide,vinyl acetate and other monomers by using a solubilizing agent to dissolve the acrylamide in the vinyl acetate |
| US3725124A (en) * | 1968-10-01 | 1973-04-03 | Du Pont | Polymeric film coated with vinyl acetate/ethylene copolymer adhesive |
| DE1965740C3 (de) * | 1969-12-31 | 1979-11-22 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von pulverisierbaren Acryl-Harzen |
| US3714099A (en) * | 1970-09-03 | 1973-01-30 | Union Oil Co | Self-crosslinking vinyl acetate-ethylene latexes |
| DE2149820C3 (de) * | 1971-10-06 | 1975-05-15 | Roehm Gmbh, 6100 Darmstadt | Verfahren zur Herstellung von Polymerisaten in Pulverform aus wäßrigen Polymerisatdispersionen |
-
1972
- 1972-05-05 DE DE2222033A patent/DE2222033C2/de not_active Expired
-
1973
- 1973-04-27 NL NL7305939A patent/NL7305939A/xx not_active Application Discontinuation
- 1973-04-27 ZA ZA732865A patent/ZA732865B/xx unknown
- 1973-04-30 ES ES414254A patent/ES414254A1/es not_active Expired
- 1973-05-02 CH CH624773A patent/CH584239A5/xx not_active IP Right Cessation
- 1973-05-02 JP JP4857173A patent/JPS5734293B2/ja not_active Expired
- 1973-05-02 US US05/356,405 patent/US3950302A/en not_active Expired - Lifetime
- 1973-05-03 FI FI1406/73A patent/FI59108C/fi active
- 1973-05-03 IT IT23682/73A patent/IT987116B/it active
- 1973-05-03 BR BR3184/73A patent/BR7303184D0/pt unknown
- 1973-05-03 AT AT389173A patent/AT329860B/de not_active IP Right Cessation
- 1973-05-03 AR AR247810A patent/AR197225A1/es active
- 1973-05-04 GB GB2135573A patent/GB1408361A/en not_active Expired
- 1973-05-04 DK DK247373A patent/DK146322C/da not_active IP Right Cessation
- 1973-05-04 CA CA170,503A patent/CA1011039A/en not_active Expired
- 1973-05-04 SE SE7306298A patent/SE392473B/xx unknown
- 1973-05-04 FR FR7316153A patent/FR2183810B1/fr not_active Expired
- 1973-05-04 NO NO1855/73A patent/NO142753C/no unknown
- 1973-05-07 BE BE130833A patent/BE799199A/xx not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0690278A1 (de) | 1994-06-29 | 1996-01-03 | Hoechst Aktiengesellschaft | Vorrichtung und Verfahren zum Eintrag von Zuschlagstoffen in Scheibenzerstäubungstrocknern |
Also Published As
| Publication number | Publication date |
|---|---|
| ZA732865B (en) | 1974-04-24 |
| ES414254A1 (es) | 1976-01-16 |
| DK146322B (da) | 1983-09-05 |
| FR2183810A1 (en:Method) | 1973-12-21 |
| FR2183810B1 (en:Method) | 1976-11-12 |
| GB1408361A (en) | 1975-10-01 |
| US3950302A (en) | 1976-04-13 |
| BR7303184D0 (pt) | 1974-07-18 |
| CH584239A5 (en:Method) | 1977-01-31 |
| IT987116B (it) | 1975-02-20 |
| NO142753C (no) | 1980-10-08 |
| JPS5734293B2 (en:Method) | 1982-07-22 |
| AR197225A1 (es) | 1974-03-22 |
| NO142753B (no) | 1980-06-30 |
| DK146322C (da) | 1984-02-20 |
| AU5516473A (en) | 1974-11-14 |
| FI59108C (fi) | 1981-06-10 |
| BE799199A (fr) | 1973-11-07 |
| ATA389173A (de) | 1975-08-15 |
| NL7305939A (en:Method) | 1973-11-07 |
| AT329860B (de) | 1976-06-10 |
| SE392473B (sv) | 1977-03-28 |
| CA1011039A (en) | 1977-05-24 |
| JPS4941440A (en:Method) | 1974-04-18 |
| FI59108B (fi) | 1981-02-27 |
| DE2222033A1 (de) | 1973-11-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| D2 | Grant after examination |