DE2145321C3 - Verfahren zur Herstellung von Kaliumperoxydi sulfat - Google Patents
Verfahren zur Herstellung von Kaliumperoxydi sulfatInfo
- Publication number
- DE2145321C3 DE2145321C3 DE2145321A DE2145321A DE2145321C3 DE 2145321 C3 DE2145321 C3 DE 2145321C3 DE 2145321 A DE2145321 A DE 2145321A DE 2145321 A DE2145321 A DE 2145321A DE 2145321 C3 DE2145321 C3 DE 2145321C3
- Authority
- DE
- Germany
- Prior art keywords
- potassium
- peroxydisulfate
- solution
- reaction
- sulfate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 20
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 title claims description 16
- 235000019394 potassium persulphate Nutrition 0.000 title claims description 14
- 238000004519 manufacturing process Methods 0.000 title claims 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 19
- 238000006243 chemical reaction Methods 0.000 claims description 15
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 6
- 239000012452 mother liquor Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims 17
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims 10
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims 8
- 229910052939 potassium sulfate Inorganic materials 0.000 claims 8
- 235000011151 potassium sulphates Nutrition 0.000 claims 8
- JRKICGRDRMAZLK-UHFFFAOYSA-L peroxydisulfate Chemical compound [O-]S(=O)(=O)OOS([O-])(=O)=O JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 claims 7
- 229910001870 ammonium persulfate Inorganic materials 0.000 claims 5
- 235000019395 ammonium persulphate Nutrition 0.000 claims 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- 229910052700 potassium Inorganic materials 0.000 claims 3
- 239000011591 potassium Substances 0.000 claims 3
- 239000000047 product Substances 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- 239000007864 aqueous solution Substances 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 2
- 239000001120 potassium sulphate Substances 0.000 claims 2
- 238000000926 separation method Methods 0.000 claims 2
- 239000011734 sodium Substances 0.000 claims 2
- 239000007858 starting material Substances 0.000 claims 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 230000002421 anti-septic effect Effects 0.000 claims 1
- 239000007844 bleaching agent Substances 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 230000008021 deposition Effects 0.000 claims 1
- 239000000706 filtrate Substances 0.000 claims 1
- 239000004615 ingredient Substances 0.000 claims 1
- 230000000802 nitrating effect Effects 0.000 claims 1
- 239000007800 oxidant agent Substances 0.000 claims 1
- BITYAPCSNKJESK-UHFFFAOYSA-N potassiosodium Chemical compound [Na].[K] BITYAPCSNKJESK-UHFFFAOYSA-N 0.000 claims 1
- 238000001556 precipitation Methods 0.000 claims 1
- 239000000344 soap Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims 1
- 229910021653 sulphate ion Inorganic materials 0.000 claims 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 229910001415 sodium ion Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/06—Peroxyhydrates; Peroxyacids or salts thereof containing sulfur
- C01B15/08—Peroxysulfates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US7127170A | 1970-09-10 | 1970-09-10 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2145321A1 DE2145321A1 (de) | 1972-03-16 |
| DE2145321B2 DE2145321B2 (de) | 1973-02-22 |
| DE2145321C3 true DE2145321C3 (de) | 1973-09-27 |
Family
ID=22100304
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2145321A Expired DE2145321C3 (de) | 1970-09-10 | 1971-09-10 | Verfahren zur Herstellung von Kaliumperoxydi sulfat |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3716629A (enExample) |
| JP (1) | JPS5035516B1 (enExample) |
| CA (1) | CA956434A (enExample) |
| DE (1) | DE2145321C3 (enExample) |
| ES (1) | ES394535A1 (enExample) |
| FR (1) | FR2106415B1 (enExample) |
| GB (1) | GB1320433A (enExample) |
| NL (1) | NL7112456A (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3954952A (en) * | 1975-03-24 | 1976-05-04 | Fmc Corporation | Continuous chemical process for the manufacture of sodium and potassium peroxydisulfate |
| US4144144A (en) * | 1976-12-23 | 1979-03-13 | Fmc Corporation | Electrolytic production of sodium persulfate |
| DE3264680D1 (en) * | 1981-11-10 | 1985-08-14 | Fmc Corp | Method for producing sodium persulfate |
| JPH0292811A (ja) * | 1988-09-28 | 1990-04-03 | Tokai Denka Kogyo Kk | 高純度過硫酸カリウムの製造方法 |
| CN112850653A (zh) * | 2021-01-29 | 2021-05-28 | 优耐德引发剂合肥有限公司 | 一种提高过硫酸钠产量的方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA571378A (en) * | 1959-02-24 | R. Ryan Jospeph | Production of ammonium persulfate and potassium persulfate | |
| GB191023157A (en) * | 1909-10-09 | 1910-11-10 | Albert Pietzsch | Improved Manufacture of Potassium Persulphate. |
| US2899272A (en) * | 1957-11-04 | 1959-08-11 | Production of persulfates |
-
1970
- 1970-09-10 US US00071271A patent/US3716629A/en not_active Expired - Lifetime
-
1971
- 1971-08-04 CA CA119,777A patent/CA956434A/en not_active Expired
- 1971-08-26 ES ES394535A patent/ES394535A1/es not_active Expired
- 1971-09-06 JP JP46068142A patent/JPS5035516B1/ja active Pending
- 1971-09-06 GB GB4149871A patent/GB1320433A/en not_active Expired
- 1971-09-07 FR FR7132222A patent/FR2106415B1/fr not_active Expired
- 1971-09-09 NL NL7112456A patent/NL7112456A/xx unknown
- 1971-09-10 DE DE2145321A patent/DE2145321C3/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| ES394535A1 (es) | 1974-02-01 |
| DE2145321B2 (de) | 1973-02-22 |
| CA956434A (en) | 1974-10-22 |
| GB1320433A (en) | 1973-06-13 |
| FR2106415A1 (enExample) | 1972-05-05 |
| DE2145321A1 (de) | 1972-03-16 |
| FR2106415B1 (enExample) | 1974-03-29 |
| JPS5035516B1 (enExample) | 1975-11-17 |
| US3716629A (en) | 1973-02-13 |
| NL7112456A (enExample) | 1972-03-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| EHJ | Ceased/non-payment of the annual fee |