DE19605778C1 - Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden - Google Patents

Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden

Info

Publication number
DE19605778C1
DE19605778C1 DE19605778A DE19605778A DE19605778C1 DE 19605778 C1 DE19605778 C1 DE 19605778C1 DE 19605778 A DE19605778 A DE 19605778A DE 19605778 A DE19605778 A DE 19605778A DE 19605778 C1 DE19605778 C1 DE 19605778C1
Authority
DE
Germany
Prior art keywords
alkyl
chloride
magnesium
alkoxyphenyl
alkoxy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE19605778A
Other languages
German (de)
English (en)
Inventor
Michael Dipl Chem Dr Finkam
Thomas Dipl Ing Kohnen
Werner Prof Dipl Chem D Winter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Grünenthal GmbH
Original Assignee
Grünenthal GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Grünenthal GmbH filed Critical Grünenthal GmbH
Priority to DE19605778A priority Critical patent/DE19605778C1/de
Priority to NZ299965A priority patent/NZ299965A/en
Priority to MYPI96005468A priority patent/MY113636A/en
Priority to SI9730477T priority patent/SI0790251T1/xx
Priority to DK97101270T priority patent/DK0790251T3/da
Priority to DE59708849T priority patent/DE59708849D1/de
Priority to ES97101270T priority patent/ES2187690T3/es
Priority to AT97101270T priority patent/ATE229025T1/de
Priority to PT97101270T priority patent/PT790251E/pt
Priority to EP97101270A priority patent/EP0790251B1/de
Priority to PE1997000069A priority patent/PE1098A1/es
Priority to BR9700208A priority patent/BR9700208A/pt
Priority to ARP970100524A priority patent/AR005775A1/es
Priority to CO97006908A priority patent/CO4770991A1/es
Priority to CZ1997430A priority patent/CZ290270B6/cs
Priority to SK202-97A priority patent/SK282190B6/sk
Priority to IN247CA1997 priority patent/IN192277B/en
Priority to ZA9701232A priority patent/ZA971232B/xx
Priority to UA97020620A priority patent/UA46740C2/uk
Priority to JP03083397A priority patent/JP3893180B2/ja
Priority to CN97102454A priority patent/CN1075075C/zh
Priority to UY24460A priority patent/UY24460A1/es
Priority to CA002197616A priority patent/CA2197616C/en
Priority to IL12022497A priority patent/IL120224A/en
Priority to US08/800,879 priority patent/US5852216A/en
Priority to NO19970698A priority patent/NO315943B1/no
Priority to HU9700441A priority patent/HU219060B/hu
Priority to AU14715/97A priority patent/AU707621B2/en
Priority to KR1019970004335A priority patent/KR100521062B1/ko
Priority to PL97318486A priority patent/PL185309B1/pl
Priority to RU97102339/04A priority patent/RU2177931C2/ru
Application granted granted Critical
Publication of DE19605778C1 publication Critical patent/DE19605778C1/de
Priority to HK98104001.2A priority patent/HK1004812B/xx
Priority to KR1020050032652A priority patent/KR100541786B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B49/00—Grignard reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/10—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C217/00—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton
    • C07C217/54—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having etherified hydroxy groups bound to carbon atoms of at least one six-membered aromatic ring and amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings of the same carbon skeleton
    • C07C217/74—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having etherified hydroxy groups bound to carbon atoms of at least one six-membered aromatic ring and amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings of the same carbon skeleton with rings other than six-membered aromatic rings being part of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C221/00—Preparation of compounds containing amino groups and doubly-bound oxygen atoms bound to the same carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
    • C07F3/02—Magnesium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE19605778A 1996-02-16 1996-02-16 Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden Expired - Fee Related DE19605778C1 (de)

Priority Applications (33)

Application Number Priority Date Filing Date Title
DE19605778A DE19605778C1 (de) 1996-02-16 1996-02-16 Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden
NZ299965A NZ299965A (en) 1996-02-16 1996-12-18 Process for preparation of (3-alkoxyphenyl)magnesium chlorides from corresponding (3-alkoxyphenyl) chlorides by reduction of magnesium halides
MYPI96005468A MY113636A (en) 1996-02-16 1996-12-26 The preparation and use of (3-alkoxyphenyl) magnesium chlorides
DK97101270T DK0790251T3 (da) 1996-02-16 1997-01-28 Fremstilling og anvendelse af (3-alkoxyphenyl)magnesiumchlorider
DE59708849T DE59708849D1 (de) 1996-02-16 1997-01-28 Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden
ES97101270T ES2187690T3 (es) 1996-02-16 1997-01-28 Preparacion y utilizacion de cloruros de (3-alcoxi-fenil)-magnesio.
SI9730477T SI0790251T1 (en) 1996-02-16 1997-01-28 Preparation and use of (3-alkoxyphenyl) magnesium chlorides
AT97101270T ATE229025T1 (de) 1996-02-16 1997-01-28 Herstellung und verwendung von (3- alkoxyphenyl)magnesiumchloriden
PT97101270T PT790251E (pt) 1996-02-16 1997-01-28 Producao e utilizacao de cloretos de (3-alcoxifenil)magnesio
EP97101270A EP0790251B1 (de) 1996-02-16 1997-01-28 Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden
PE1997000069A PE1098A1 (es) 1996-02-16 1997-02-04 Procedimiento de preparacion de cloruro de (3-alcoxifenil) magnesio y proceso de sintesis que lo emplea
BR9700208A BR9700208A (pt) 1996-02-16 1997-02-06 Etodo para produção de cloretos de (3-alcoxi-fenil) magnésio e emprego de um cloreto de (3-alcoxi-fenil) magnésio
ARP970100524A AR005775A1 (es) 1996-02-16 1997-02-10 Procedimiento de preparacion de cloruro de (3-alcoxifenil)-magnesio y su uso en la reaccion
CO97006908A CO4770991A1 (es) 1996-02-16 1997-02-11 Procedimiento de preparacion de alcoholes por reaccion de un b -aminoaldehido o una b -aminocetona con aldehido o una cetona
SK202-97A SK282190B6 (sk) 1996-02-16 1997-02-12 Spôsob výroby alkoholov
CZ1997430A CZ290270B6 (cs) 1996-02-16 1997-02-12 Způsob výroby alkoholů
IN247CA1997 IN192277B (enExample) 1996-02-16 1997-02-13
UA97020620A UA46740C2 (uk) 1996-02-16 1997-02-13 Спосіб одержання спиртів
ZA9701232A ZA971232B (en) 1996-02-16 1997-02-13 The preparation and use of (3-alkoxy-phenyl)magnesium chlorides.
KR1019970004335A KR100521062B1 (ko) 1996-02-16 1997-02-14 (3-알콕시페닐)마그네슘클로라이드의제조방법및당해클로라이드를사용한알콜제조방법
UY24460A UY24460A1 (es) 1996-02-16 1997-02-14 Procedimiento de preparaciones de alcoholes por reaccion con cloruros de (3-alcoxifenil) magnesio
CA002197616A CA2197616C (en) 1996-02-16 1997-02-14 The preparation and use of (3-alkoxy-phenyl) magnesium chlorides
IL12022497A IL120224A (en) 1996-02-16 1997-02-14 Process for the preparation of alcohols by redoxification of a carbonyl group of aldehydes, ketones, b-aminoaldehydes or b-amino octons with the help of (3-alkoxifenil) magnesium chlorides
US08/800,879 US5852216A (en) 1996-02-16 1997-02-14 Preparation and use of (3-alkoxy-phenyl) magnesium chlorides
NO19970698A NO315943B1 (no) 1996-02-16 1997-02-14 Fremstilling og anvendelse av (3- alkoksyfenyl)magnesiumklorider
HU9700441A HU219060B (hu) 1996-02-16 1997-02-14 Eljárás (3-alkoxi-fenil)-magnézium-kloridok előállítására és felhasználására
JP03083397A JP3893180B2 (ja) 1996-02-16 1997-02-14 （３−アルコキシフエニル）マグネシウムクロライドの製造方法及びその使用方法
CN97102454A CN1075075C (zh) 1996-02-16 1997-02-14 氯化(3－烷氧基苯基)镁的制备和用途
PL97318486A PL185309B1 (pl) 1996-02-16 1997-02-14 Sposób wytwarzania chlorków (3-alkoksyfenylo)-magnezu oraz odpowiednio 1-podstawionych związków z aldehydów lub ketonów
RU97102339/04A RU2177931C2 (ru) 1996-02-16 1997-02-14 Способ получения спиртов с использованием (3-алкоксифенил)магнийхлорида
AU14715/97A AU707621B2 (en) 1996-02-16 1997-02-14 The preparation and use of (3-alkoxy-phenyl) magnesium chlorides
HK98104001.2A HK1004812B (en) 1996-02-16 1998-05-08 The preparating and use of (3-alkoxy-phenyl)magnesium chlorides
KR1020050032652A KR100541786B1 (ko) 1996-02-16 2005-04-20 (3-알콕시페닐)마그네슘 클로라이드를 사용한 알콜의 제조방법

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19605778A DE19605778C1 (de) 1996-02-16 1996-02-16 Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden

Publications (1)

Publication Number Publication Date
DE19605778C1 true DE19605778C1 (de) 1997-04-17

Family

ID=7785591

Family Applications (2)

Application Number Title Priority Date Filing Date
DE19605778A Expired - Fee Related DE19605778C1 (de) 1996-02-16 1996-02-16 Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden
DE59708849T Expired - Lifetime DE59708849D1 (de) 1996-02-16 1997-01-28 Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE59708849T Expired - Lifetime DE59708849D1 (de) 1996-02-16 1997-01-28 Herstellung und Verwendung von (3-Alkoxyphenyl)magnesiumchloriden

Country Status (30)

Country Link
US (1) US5852216A (enExample)
EP (1) EP0790251B1 (enExample)
JP (1) JP3893180B2 (enExample)
KR (2) KR100521062B1 (enExample)
CN (1) CN1075075C (enExample)
AR (1) AR005775A1 (enExample)
AT (1) ATE229025T1 (enExample)
AU (1) AU707621B2 (enExample)
BR (1) BR9700208A (enExample)
CA (1) CA2197616C (enExample)
CO (1) CO4770991A1 (enExample)
CZ (1) CZ290270B6 (enExample)
DE (2) DE19605778C1 (enExample)
DK (1) DK0790251T3 (enExample)
ES (1) ES2187690T3 (enExample)
HU (1) HU219060B (enExample)
IL (1) IL120224A (enExample)
IN (1) IN192277B (enExample)
MY (1) MY113636A (enExample)
NO (1) NO315943B1 (enExample)
NZ (1) NZ299965A (enExample)
PE (1) PE1098A1 (enExample)
PL (1) PL185309B1 (enExample)
PT (1) PT790251E (enExample)
RU (1) RU2177931C2 (enExample)
SI (1) SI0790251T1 (enExample)
SK (1) SK282190B6 (enExample)
UA (1) UA46740C2 (enExample)
UY (1) UY24460A1 (enExample)
ZA (1) ZA971232B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19757499A1 (de) * 1997-12-23 1999-06-24 Studiengesellschaft Kohle Mbh Verfahren zur Synthese von Organomagnesium-Verbindungen unter Einsatz von Katalysatoren

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6531597B2 (en) * 2001-02-13 2003-03-11 Hoffmann-La Roche Inc. Process for preparation of 2-phenyl acetic acid derivatives
RU2345057C2 (ru) * 2003-10-13 2009-01-27 Митени, С.П.А. Способ получения 3,5-бис(трифторметил)бензилового спирта
EP1785412A1 (en) * 2005-11-14 2007-05-16 IPCA Laboratories Limited Tramadol recovery process
US9882245B2 (en) 2013-08-23 2018-01-30 Ut-Battelle, Llc Alkoxide-based magnesium electrolyte compositions for magnesium batteries

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2959596A (en) 1957-11-22 1960-11-08 Metal & Thermit Corp Aryl chloride-cyclic ether grignard reagents
US3706809A (en) * 1970-09-17 1972-12-19 Takasago Perfumery Co Ltd Process for preparing highly reactive organo-magnesium compounds
US4133824A (en) * 1977-08-17 1979-01-09 Texas Alkyls, Inc. Organo-magnesium complexes and process for their preparation
JPS5818323A (ja) * 1981-07-27 1983-02-02 Sumitomo Chem Co Ltd アルコ−ル類の製造方法
JPS6072833A (ja) * 1983-09-29 1985-04-24 Hokko Chem Ind Co Ltd 芳香族ビニル化合物の改良製造法
US4731203A (en) * 1983-11-09 1988-03-15 Studiengesellschaft Kohle Mbh Process for using finely divided highly reactive magnesium
CA1284665C (en) * 1984-07-26 1991-06-04 Eric George Delmar Process for hydroxymethylation
US5273686A (en) * 1987-07-11 1993-12-28 Studiengesellschaft Kohle Mbh Soluble magnesium hydrides, method of preparing them, and use thereof
EP0307106B1 (en) 1987-09-11 1992-01-15 Hokko Chemical Industry Co., Ltd P- or m-tert butoxyphenethyl alcohol and process for preparing the same
JP3107920B2 (ja) 1992-08-28 2000-11-13 花王株式会社 歯磨剤の製造方法
US5358670A (en) * 1993-07-02 1994-10-25 Ferro Corporation Process for preparing grignard reagents in diethylene glycol dibutyl ether

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
NICHTS ERMITTELT *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19757499A1 (de) * 1997-12-23 1999-06-24 Studiengesellschaft Kohle Mbh Verfahren zur Synthese von Organomagnesium-Verbindungen unter Einsatz von Katalysatoren

Also Published As

Publication number Publication date
US5852216A (en) 1998-12-22
KR970061902A (ko) 1997-09-12
UA46740C2 (uk) 2002-06-17
KR100541786B1 (ko) 2006-01-11
JPH09227575A (ja) 1997-09-02
MY113636A (en) 2002-04-30
CA2197616C (en) 2005-08-16
CZ43097A3 (en) 1997-09-17
AR005775A1 (es) 1999-07-14
CA2197616A1 (en) 1997-08-17
SK20297A3 (en) 1997-09-10
CN1075075C (zh) 2001-11-21
IL120224A (en) 2002-05-23
CZ290270B6 (cs) 2002-06-12
DE59708849D1 (de) 2003-01-16
SK282190B6 (sk) 2001-12-03
SI0790251T1 (en) 2003-06-30
HU9700441D0 (en) 1997-04-28
NZ299965A (en) 1998-01-26
NO970698D0 (no) 1997-02-14
HU219060B (hu) 2001-02-28
UY24460A1 (es) 1997-04-14
IL120224A0 (en) 1997-06-10
PE1098A1 (es) 1998-02-21
CO4770991A1 (es) 1999-04-30
PL318486A1 (en) 1997-08-18
ES2187690T3 (es) 2003-06-16
RU2177931C2 (ru) 2002-01-10
HUP9700441A2 (en) 1997-10-28
EP0790251B1 (de) 2002-12-04
KR100521062B1 (ko) 2006-01-12
DK0790251T3 (da) 2003-03-17
EP0790251A2 (de) 1997-08-20
AU1471597A (en) 1997-08-21
NO315943B1 (no) 2003-11-17
IN192277B (enExample) 2004-03-27
EP0790251A3 (de) 1999-09-22
JP3893180B2 (ja) 2007-03-14
ATE229025T1 (de) 2002-12-15
ZA971232B (en) 1997-08-25
AU707621B2 (en) 1999-07-15
HK1004812A1 (en) 1998-12-11
NO970698L (no) 1997-08-18
CN1166491A (zh) 1997-12-03
PT790251E (pt) 2003-04-30
HUP9700441A3 (en) 2000-03-28
PL185309B1 (pl) 2003-04-30
BR9700208A (pt) 1998-10-27

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Legal Events

Date Code Title Description
8100 Publication of patent without earlier publication of application
D1 Grant (no unexamined application published) patent law 81
8364 No opposition during term of opposition
R119 Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee

Effective date: 20130903