DE1215678B - Verfahren zur kontinuierlichen Herstellung von Zuckersaeure - Google Patents
Verfahren zur kontinuierlichen Herstellung von ZuckersaeureInfo
- Publication number
- DE1215678B DE1215678B DEC26475A DEC0026475A DE1215678B DE 1215678 B DE1215678 B DE 1215678B DE C26475 A DEC26475 A DE C26475A DE C0026475 A DEC0026475 A DE C0026475A DE 1215678 B DE1215678 B DE 1215678B
- Authority
- DE
- Germany
- Prior art keywords
- nitric acid
- reaction
- reaction mixture
- glucose
- aqueous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002253 acid Substances 0.000 title claims description 21
- 238000000034 method Methods 0.000 title claims description 15
- 238000010924 continuous production Methods 0.000 title claims description 5
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 30
- 229910017604 nitric acid Inorganic materials 0.000 claims description 30
- 238000006243 chemical reaction Methods 0.000 claims description 28
- 239000011541 reaction mixture Substances 0.000 claims description 26
- 239000000243 solution Substances 0.000 claims description 17
- GZCGUPFRVQAUEE-SLPGGIOYSA-N aldehydo-D-glucose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O GZCGUPFRVQAUEE-SLPGGIOYSA-N 0.000 claims description 14
- 238000007254 oxidation reaction Methods 0.000 claims description 14
- 230000003647 oxidation Effects 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 12
- 239000008103 glucose Substances 0.000 description 8
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 8
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 229910052700 potassium Inorganic materials 0.000 description 4
- 239000011591 potassium Substances 0.000 description 4
- 235000010288 sodium nitrite Nutrition 0.000 description 4
- 238000003756 stirring Methods 0.000 description 3
- 239000007858 starting material Substances 0.000 description 2
- 238000013459 approach Methods 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- -1 furan compounds Chemical class 0.000 description 1
- 150000002240 furans Chemical class 0.000 description 1
- 150000002391 heterocyclic compounds Chemical class 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000000825 pharmaceutical preparation Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/27—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with oxides of nitrogen or nitrogen-containing mineral acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Saccharide Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH308061A CH387611A (de) | 1961-03-14 | 1961-03-14 | Verfahren zur Herstellung von Tetraoxybutandicarbonsäuren |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1215678B true DE1215678B (de) | 1966-05-05 |
Family
ID=4248173
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEC26475A Pending DE1215678B (de) | 1961-03-14 | 1962-03-13 | Verfahren zur kontinuierlichen Herstellung von Zuckersaeure |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3242207A (https=) |
| CH (1) | CH387611A (https=) |
| DE (1) | DE1215678B (https=) |
| GB (1) | GB976725A (https=) |
| NL (1) | NL275883A (https=) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7692041B2 (en) | 2006-08-07 | 2010-04-06 | The University Of Montana | Method of oxidation using nitric acid |
| US20090250653A1 (en) | 2006-08-07 | 2009-10-08 | Kiely Donald E | Hydroxycarboxylic Acids and Salts |
| CN101918474B (zh) | 2007-11-15 | 2013-11-13 | 蒙大拿大学 | 羟基聚酰胺胶凝剂 |
| EP2638184A1 (en) | 2010-11-11 | 2013-09-18 | Rivertop Renewables | Corrosion inhibiting composition |
| CA2833374A1 (en) | 2011-04-21 | 2012-10-26 | Rivertop Renewables, Inc. | Calcium sequestering composition |
| US9346736B2 (en) | 2013-03-13 | 2016-05-24 | Rivertop Renewables, Inc. | Oxidation process |
| US9670124B2 (en) | 2013-03-13 | 2017-06-06 | Rivertop Renewables, Inc. | Nitric acid oxidation process |
| HK1215429A1 (zh) | 2013-03-13 | 2016-08-26 | Rivertop Renewables, Inc. | 改進的硝酸氧化方法 |
-
0
- NL NL275883D patent/NL275883A/xx unknown
-
1961
- 1961-03-14 CH CH308061A patent/CH387611A/de unknown
-
1962
- 1962-03-07 US US177996A patent/US3242207A/en not_active Expired - Lifetime
- 1962-03-09 GB GB9261/62A patent/GB976725A/en not_active Expired
- 1962-03-13 DE DEC26475A patent/DE1215678B/de active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US3242207A (en) | 1966-03-22 |
| GB976725A (en) | 1964-12-02 |
| NL275883A (https=) | |
| CH387611A (de) | 1965-02-15 |
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