DE112004000001B4 - Passivierung eines Sulfidkatalysators zur Hydrierumwandlung - Google Patents

Passivierung eines Sulfidkatalysators zur Hydrierumwandlung Download PDF

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Publication number
DE112004000001B4
DE112004000001B4 DE112004000001.7T DE112004000001T DE112004000001B4 DE 112004000001 B4 DE112004000001 B4 DE 112004000001B4 DE 112004000001 T DE112004000001 T DE 112004000001T DE 112004000001 B4 DE112004000001 B4 DE 112004000001B4
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Prior art keywords
catalyst
procedure according
passivation
oxygen
kpa
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Expired - Lifetime
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DE112004000001.7T
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German (de)
English (en)
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DE112004000001T5 (de
Inventor
Pierre Dufresne
Franck Labruyere
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Europeene de Retraitement de Catalysateurs EURECAT
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Europeene de Retraitement de Catalysateurs EURECAT
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/20—Sulfiding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/883—Molybdenum and nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/888—Tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/12—Oxidising
    • B01J37/14—Oxidising with gases containing free oxygen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
    • C10G49/02—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00 characterised by the catalyst used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J33/00—Protection of catalysts, e.g. by coating
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1014—Biomass of vegetal origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1018—Biomass of animal origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1048—Middle distillates
    • C10G2300/1051—Kerosene having a boiling range of about 180 - 230 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1048—Middle distillates
    • C10G2300/1059—Gasoil having a boiling range of about 330 - 427 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1074—Vacuum distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/30—Physical properties of feedstocks or products
    • C10G2300/301—Boiling range
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/70—Catalyst aspects
    • C10G2300/705—Passivation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
DE112004000001.7T 2003-02-11 2004-02-06 Passivierung eines Sulfidkatalysators zur Hydrierumwandlung Expired - Lifetime DE112004000001B4 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0301634A FR2850882B1 (fr) 2003-02-11 2003-02-11 Passivation de catalyseur d'hydroconversion sulfure
FR03/01634 2003-02-11
PCT/FR2004/000272 WO2004071655A1 (fr) 2003-02-11 2004-02-06 Passivation de catalyseur d'hydroconversion sulfure

Publications (2)

Publication Number Publication Date
DE112004000001T5 DE112004000001T5 (de) 2005-05-25
DE112004000001B4 true DE112004000001B4 (de) 2021-12-02

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DE112004000001.7T Expired - Lifetime DE112004000001B4 (de) 2003-02-11 2004-02-06 Passivierung eines Sulfidkatalysators zur Hydrierumwandlung

Country Status (7)

Country Link
US (1) US7582587B2 (https=)
JP (1) JP5016918B2 (https=)
CA (1) CA2485665C (https=)
DE (1) DE112004000001B4 (https=)
FR (1) FR2850882B1 (https=)
LU (1) LU91102B1 (https=)
WO (1) WO2004071655A1 (https=)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7407909B2 (en) * 2004-10-01 2008-08-05 Exxonmobil Research And Engineering Company Ex-situ reduction and dry passivation of noble metal catalysts
FR2880823B1 (fr) * 2005-01-20 2008-02-22 Total France Sa Catalyseur d'hydrotraitement, son procede de preparation et et son utilisation
FR2915908B1 (fr) * 2007-05-10 2010-09-03 Eurecat Sa Procede de sulfuration ou presulfuration de particules solides d'un catalyseur ou d'un adsorbant
US8835831B2 (en) 2010-06-22 2014-09-16 Zena Technologies, Inc. Polarized light detecting device and fabrication methods of the same
US8519379B2 (en) 2009-12-08 2013-08-27 Zena Technologies, Inc. Nanowire structured photodiode with a surrounding epitaxially grown P or N layer
US8890271B2 (en) 2010-06-30 2014-11-18 Zena Technologies, Inc. Silicon nitride light pipes for image sensors
US8269985B2 (en) 2009-05-26 2012-09-18 Zena Technologies, Inc. Determination of optimal diameters for nanowires
US9515218B2 (en) 2008-09-04 2016-12-06 Zena Technologies, Inc. Vertical pillar structured photovoltaic devices with mirrors and optical claddings
US8748799B2 (en) 2010-12-14 2014-06-10 Zena Technologies, Inc. Full color single pixel including doublet or quadruplet si nanowires for image sensors
US9299866B2 (en) 2010-12-30 2016-03-29 Zena Technologies, Inc. Nanowire array based solar energy harvesting device
US8299472B2 (en) 2009-12-08 2012-10-30 Young-June Yu Active pixel sensor with nanowire structured photodetectors
US8735797B2 (en) 2009-12-08 2014-05-27 Zena Technologies, Inc. Nanowire photo-detector grown on a back-side illuminated image sensor
US8889455B2 (en) 2009-12-08 2014-11-18 Zena Technologies, Inc. Manufacturing nanowire photo-detector grown on a back-side illuminated image sensor
US8580704B2 (en) * 2008-11-10 2013-11-12 Institut National De La Recherche Scientifique Catalyst precursors, catalysts and methods of producing same
CA2859313C (en) * 2011-12-16 2020-10-27 Basf Corporation A protected reduced metal catalyst
FR2994394B1 (fr) * 2012-08-09 2015-08-21 Eurecat Sa Procede de passivation par un compose azote d'un catalyseur zeolitique, en particulier d'un catalyseur d'hydrocraquage
CN113083376A (zh) * 2019-12-23 2021-07-09 内蒙古伊泰煤基新材料研究院有限公司 一种加氢裂化催化剂的钝化方法
GB202100248D0 (en) * 2021-01-08 2021-02-24 Johnson Matthey Plc Catalyst passivation method

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4719195A (en) 1984-10-30 1988-01-12 Europeenne De Retraitement De Catalyseurs (Eurecat) Process for presulfurizing a hydrogen treatment catalyst
US5397756A (en) 1992-04-01 1995-03-14 Europeenne De Retraitement De Catalyseurs (Eurecat) Process for the presulphurization of hydrocarbon treatment catalysts
EP0785022A1 (fr) 1996-01-17 1997-07-23 Eurecat Europeenne De Retraitement De Catalyseurs Procédé d'incorporation de soufre dans la porosité d'un catalyseur de traitement d'hydrocarbures
DE69403906T2 (de) 1993-05-04 1997-11-27 Cri Int Inc Methode zur behandlung von spontan brennbaren katalysatoren
DE69514609T2 (de) 1994-10-07 2000-06-29 Eurecat Europeene De Retraitement De Catalyseurs, La Voulte-Sur-Rhone Verfahren zur Vorbehandlung vor Verwendung eines Katalysators für die Behandlung von Kohlenwasserstoffen
US20020037806A1 (en) 1998-10-12 2002-03-28 Pierre Dufresne Ex-situ presulfuration in the presence of a hydrocarbon molecule

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US2905636A (en) * 1957-06-27 1959-09-22 Universal Oil Prod Co Manufacture and use of supported molybdenum-containing catalysts
US3838066A (en) * 1971-10-01 1974-09-24 Standard Oil Co Method for stabilizing pyrophoric materials in a catalyst bed
US5094991A (en) * 1983-08-29 1992-03-10 Chevron Research Company Slurry catalyst for hydroprocessing heavy and refractory oils
US6093309A (en) * 1993-05-04 2000-07-25 Cri International, Inc. Method of treating spontaneously combustible catalysts
FR2749779B1 (fr) * 1996-06-12 1998-09-11 Eurecat Europ Retrait Catalys Procede de presulfuration de catalyseurs d'hydrotraitement
US5922638A (en) * 1996-06-12 1999-07-13 Europeene De Retraitement De Catalyseurs Eurecat Process for presulfurizing hydrotreatment catalysts
US5958816A (en) * 1997-02-28 1999-09-28 Tricat, Inc. Method of presulfiding and passivating a hydrocarbon conversion catalyst
FR2767072B1 (fr) * 1997-08-11 1999-09-10 Eurecat Europ Retrait Catalys Protection de catalyseurs par depot de couche protectrice
FR2784312B1 (fr) * 1998-10-12 2000-11-10 Eurecat Europ Retrait Catalys Presulfuration hors site en presence de molecule hydrocarbonee
US6509291B2 (en) * 2000-04-11 2003-01-21 Akzo Nobel N.V. Process for sulfiding a catalyst containing an S-containing additive
FR2874838B1 (fr) * 2004-09-08 2006-11-24 Inst Francais Du Petrole Procede de sulfuration de catalyseurs d'hydrotraitement
US7407909B2 (en) * 2004-10-01 2008-08-05 Exxonmobil Research And Engineering Company Ex-situ reduction and dry passivation of noble metal catalysts

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4719195A (en) 1984-10-30 1988-01-12 Europeenne De Retraitement De Catalyseurs (Eurecat) Process for presulfurizing a hydrogen treatment catalyst
US5397756A (en) 1992-04-01 1995-03-14 Europeenne De Retraitement De Catalyseurs (Eurecat) Process for the presulphurization of hydrocarbon treatment catalysts
DE69403906T2 (de) 1993-05-04 1997-11-27 Cri Int Inc Methode zur behandlung von spontan brennbaren katalysatoren
DE69514609T2 (de) 1994-10-07 2000-06-29 Eurecat Europeene De Retraitement De Catalyseurs, La Voulte-Sur-Rhone Verfahren zur Vorbehandlung vor Verwendung eines Katalysators für die Behandlung von Kohlenwasserstoffen
EP0785022A1 (fr) 1996-01-17 1997-07-23 Eurecat Europeenne De Retraitement De Catalyseurs Procédé d'incorporation de soufre dans la porosité d'un catalyseur de traitement d'hydrocarbures
US20020037806A1 (en) 1998-10-12 2002-03-28 Pierre Dufresne Ex-situ presulfuration in the presence of a hydrocarbon molecule

Also Published As

Publication number Publication date
FR2850882A1 (fr) 2004-08-13
DE112004000001T5 (de) 2005-05-25
LU91102B1 (fr) 2006-02-28
US20060154812A1 (en) 2006-07-13
US7582587B2 (en) 2009-09-01
JP2006517467A (ja) 2006-07-27
WO2004071655A1 (fr) 2004-08-26
CA2485665A1 (fr) 2004-08-26
FR2850882B1 (fr) 2005-03-18
JP5016918B2 (ja) 2012-09-05
CA2485665C (fr) 2011-09-27

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