DE102005052444A1 - Verfahren zur Herstellung hochreiner Zirkonium-, Hafnium-, Tantal- und Niobalkoxide - Google Patents

Verfahren zur Herstellung hochreiner Zirkonium-, Hafnium-, Tantal- und Niobalkoxide Download PDF

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Publication number
DE102005052444A1
DE102005052444A1 DE102005052444A DE102005052444A DE102005052444A1 DE 102005052444 A1 DE102005052444 A1 DE 102005052444A1 DE 102005052444 A DE102005052444 A DE 102005052444A DE 102005052444 A DE102005052444 A DE 102005052444A DE 102005052444 A1 DE102005052444 A1 DE 102005052444A1
Authority
DE
Germany
Prior art keywords
alkoxides
hal
alkoxide
metal
raw
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE102005052444A
Other languages
German (de)
English (en)
Inventor
Knud Dr. Reuter
Friedrich Zell
Martina Ebner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Heraeus Deutschland GmbH and Co KG
Original Assignee
HC Starck GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HC Starck GmbH filed Critical HC Starck GmbH
Priority to DE102005052444A priority Critical patent/DE102005052444A1/de
Priority to EP06017017A priority patent/EP1764354B1/de
Priority to AT06017017T priority patent/ATE531682T1/de
Priority to MYPI20064019A priority patent/MY140577A/en
Priority to IL177687A priority patent/IL177687A/en
Priority to US11/509,157 priority patent/US7273943B2/en
Priority to CN2013100543766A priority patent/CN103254035A/zh
Priority to CN2006101216437A priority patent/CN1919813B/zh
Priority to KR1020060080846A priority patent/KR101359163B1/ko
Priority to TW095131223A priority patent/TWI399340B/zh
Priority to JP2006228987A priority patent/JP5591437B2/ja
Publication of DE102005052444A1 publication Critical patent/DE102005052444A1/de
Priority to JP2013037739A priority patent/JP2013144688A/ja
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/94—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F17/00—Metallocenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/003—Compounds containing elements of Groups 4 or 14 of the Periodic Table without C-Metal linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/005—Compounds of elements of Group 5 of the Periodic Table without metal-carbon linkages

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
DE102005052444A 2005-08-27 2005-11-03 Verfahren zur Herstellung hochreiner Zirkonium-, Hafnium-, Tantal- und Niobalkoxide Withdrawn DE102005052444A1 (de)

Priority Applications (12)

Application Number Priority Date Filing Date Title
DE102005052444A DE102005052444A1 (de) 2005-08-27 2005-11-03 Verfahren zur Herstellung hochreiner Zirkonium-, Hafnium-, Tantal- und Niobalkoxide
EP06017017A EP1764354B1 (de) 2005-08-27 2006-08-16 Verfahren zur Herstellung hochreiner Zirkonium-, Hafnium-, Tantal- und Niobalkoxide
AT06017017T ATE531682T1 (de) 2005-08-27 2006-08-16 Verfahren zur herstellung hochreiner zirkonium-, hafnium-, tantal- und niobalkoxide
MYPI20064019A MY140577A (en) 2005-08-27 2006-08-23 Process for the preparation of high-purity zirconium, hafnium, tantalum and niobium alkoxides
US11/509,157 US7273943B2 (en) 2005-08-27 2006-08-24 Process for the preparation of high-purity zirconium, hafnium, tantalum and niobium alkoxides
IL177687A IL177687A (en) 2005-08-27 2006-08-24 Process for the preparation of high-purity zirconium, hafnium, tantalum and niobium alkoxides
CN2013100543766A CN103254035A (zh) 2005-08-27 2006-08-25 制备高纯度锆、铪、钽和铌醇盐的方法
CN2006101216437A CN1919813B (zh) 2005-08-27 2006-08-25 制备高纯度锆、铪、钽和铌醇盐的方法
KR1020060080846A KR101359163B1 (ko) 2005-08-27 2006-08-25 고순도 지르코늄, 하프늄, 탄탈 및 니오브 알콕사이드의제조 방법
TW095131223A TWI399340B (zh) 2005-08-27 2006-08-25 高純度鋯、鉿、鉭及鈮烷氧化物之製法
JP2006228987A JP5591437B2 (ja) 2005-08-27 2006-08-25 高純度ジルコニウム、ハフニウム、タンタル及びニオブアルコキサイドの製造方法
JP2013037739A JP2013144688A (ja) 2005-08-27 2013-02-27 高純度ジルコニウム、ハフニウム、タンタル及びニオブアルコキサイドの製造方法

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102005040618.1 2005-08-27
DE102005040618 2005-08-27
DE102005052444A DE102005052444A1 (de) 2005-08-27 2005-11-03 Verfahren zur Herstellung hochreiner Zirkonium-, Hafnium-, Tantal- und Niobalkoxide

Publications (1)

Publication Number Publication Date
DE102005052444A1 true DE102005052444A1 (de) 2007-03-01

Family

ID=37692570

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102005052444A Withdrawn DE102005052444A1 (de) 2005-08-27 2005-11-03 Verfahren zur Herstellung hochreiner Zirkonium-, Hafnium-, Tantal- und Niobalkoxide

Country Status (10)

Country Link
US (1) US7273943B2 (https=)
EP (1) EP1764354B1 (https=)
JP (2) JP5591437B2 (https=)
KR (1) KR101359163B1 (https=)
CN (2) CN1919813B (https=)
AT (1) ATE531682T1 (https=)
DE (1) DE102005052444A1 (https=)
IL (1) IL177687A (https=)
MY (1) MY140577A (https=)
TW (1) TWI399340B (https=)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006043042A1 (de) * 2006-09-14 2008-03-27 H.C. Starck Gmbh Verfahren zur Herstellung von hochreinen Niobalkoxiden
US20090134369A1 (en) * 2007-11-26 2009-05-28 Applied Nanoworks, Inc. Metal alkoxides, apparatus for manufacturing metal alkoxides, related methods and uses thereof
CN102040478B (zh) * 2010-12-22 2013-03-13 南京大学 四乙氧基铪的合成方法
JP2012201630A (ja) * 2011-03-25 2012-10-22 Ube Industries Ltd 金属テトラ（１−アルキルイソブチルアルコキシド）の製造方法
JP2012201629A (ja) * 2011-03-25 2012-10-22 Ube Industries Ltd 高純度ジルコニウムアルコキシド原料及びその製造方法、並びに当該原料の分析方法
CN102766154B (zh) * 2012-07-28 2015-04-22 山东大学 一步溶剂法制备氧化锆纤维生产用有机聚锆前驱体或其甩丝液的方法
WO2017058160A1 (en) 2015-09-29 2017-04-06 Pryog, Llc Metal compositions and methods of making same

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4741894A (en) * 1986-06-03 1988-05-03 Morton Thiokol, Inc. Method of producing halide-free metal and hydroxides
JP2831431B2 (ja) * 1990-04-10 1998-12-02 株式会社ジャパンエナジー 高純度金属アルコキサイドの製造方法
JP2599855B2 (ja) 1991-11-25 1997-04-16 株式会社ジャパンエナジー タンタルアルコキシドの精製方法
JP2575562B2 (ja) 1991-11-25 1997-01-29 株式会社ジャパンエナジー タンタルアルコキシドの精製方法
IT1271425B (it) * 1993-01-13 1997-05-28 Himont Inc Componenti e catalizzatori per la polimerizzazione di etilene
JPH1036299A (ja) 1996-07-25 1998-02-10 Wako Pure Chem Ind Ltd 金属アルコキシドの精製方法
JP3911740B2 (ja) * 1996-11-18 2007-05-09 昭和電工株式会社 タンタルアルコキシドの製造方法
JP2001114791A (ja) 1999-10-14 2001-04-24 Showa Denko Kk 高純度ペンタアルコキシタンタルおよびその製造方法
JP2002161059A (ja) 2000-11-27 2002-06-04 Kojundo Chem Lab Co Ltd タンタルアルコキシドの精製方法
DE10113169A1 (de) * 2001-03-19 2002-09-26 Starck H C Gmbh Verfahren zur Herstellung von Tantal- und Niobalkoholaten

Also Published As

Publication number Publication date
EP1764354B1 (de) 2011-11-02
JP5591437B2 (ja) 2014-09-17
CN1919813A (zh) 2007-02-28
KR20070026039A (ko) 2007-03-08
EP1764354A1 (de) 2007-03-21
TWI399340B (zh) 2013-06-21
JP2007070357A (ja) 2007-03-22
KR101359163B1 (ko) 2014-02-05
ATE531682T1 (de) 2011-11-15
IL177687A0 (en) 2006-12-31
JP2013144688A (ja) 2013-07-25
MY140577A (en) 2009-12-31
US20070056468A1 (en) 2007-03-15
US7273943B2 (en) 2007-09-25
CN103254035A (zh) 2013-08-21
IL177687A (en) 2010-11-30
CN1919813B (zh) 2013-03-27
TW200720191A (en) 2007-06-01

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Legal Events

Date Code Title Description
8127 New person/name/address of the applicant

Owner name: H. C. STARCK GMBH & CO. KG, 38642 GOSLAR, DE

8127 New person/name/address of the applicant

Owner name: H.C. STARCK GMBH, 38642 GOSLAR, DE

8127 New person/name/address of the applicant

Owner name: H.C. STARCK CLEVIOS GMBH, 38642 GOSLAR, DE

R082 Change of representative

Representative=s name: HERZOG FIESSER & PARTNER, DE

Representative=s name: HERZOG FIESSER & PARTNER, 40210 DUESSELDORF, DE

R081 Change of applicant/patentee

Owner name: HERAEUS CLEVIOS GMBH, DE

Free format text: FORMER OWNER: H.C. STARCK CLEVIOS GMBH, 38642 GOSLAR, DE

Effective date: 20111011

R082 Change of representative

Representative=s name: HERZOG FIESSER & PARTNER PATENTANWAELTE PARTG , DE

Effective date: 20111011

Representative=s name: HERZOG FIESSER & PARTNER, DE

Effective date: 20111011

R005 Application deemed withdrawn due to failure to request examination

Effective date: 20121106