CN1919813B - 制备高纯度锆、铪、钽和铌醇盐的方法 - Google Patents

制备高纯度锆、铪、钽和铌醇盐的方法 Download PDF

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Publication number
CN1919813B
CN1919813B CN2006101216437A CN200610121643A CN1919813B CN 1919813 B CN1919813 B CN 1919813B CN 2006101216437 A CN2006101216437 A CN 2006101216437A CN 200610121643 A CN200610121643 A CN 200610121643A CN 1919813 B CN1919813 B CN 1919813B
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CN
China
Prior art keywords
tantalum
alkoxides
crude
halogen
hal
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Expired - Fee Related
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CN2006101216437A
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English (en)
Chinese (zh)
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CN1919813A (zh
Inventor
K·罗伊特
F·策尔
M·埃布纳
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HC Starck GmbH
Heraeus Deutschland GmbH and Co KG
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HC Starck GmbH
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/94—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F17/00—Metallocenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/003—Compounds containing elements of Groups 4 or 14 of the Periodic Table without C-Metal linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/005—Compounds of elements of Group 5 of the Periodic Table without metal-carbon linkages

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
CN2006101216437A 2005-08-27 2006-08-25 制备高纯度锆、铪、钽和铌醇盐的方法 Expired - Fee Related CN1919813B (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE102005040618.1 2005-08-27
DE102005040618 2005-08-27
DE102005052444A DE102005052444A1 (de) 2005-08-27 2005-11-03 Verfahren zur Herstellung hochreiner Zirkonium-, Hafnium-, Tantal- und Niobalkoxide
DE102005052444.3 2005-11-03

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN2013100543766A Division CN103254035A (zh) 2005-08-27 2006-08-25 制备高纯度锆、铪、钽和铌醇盐的方法

Publications (2)

Publication Number Publication Date
CN1919813A CN1919813A (zh) 2007-02-28
CN1919813B true CN1919813B (zh) 2013-03-27

Family

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Family Applications (2)

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CN2006101216437A Expired - Fee Related CN1919813B (zh) 2005-08-27 2006-08-25 制备高纯度锆、铪、钽和铌醇盐的方法
CN2013100543766A Pending CN103254035A (zh) 2005-08-27 2006-08-25 制备高纯度锆、铪、钽和铌醇盐的方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN2013100543766A Pending CN103254035A (zh) 2005-08-27 2006-08-25 制备高纯度锆、铪、钽和铌醇盐的方法

Country Status (10)

Country Link
US (1) US7273943B2 (https=)
EP (1) EP1764354B1 (https=)
JP (2) JP5591437B2 (https=)
KR (1) KR101359163B1 (https=)
CN (2) CN1919813B (https=)
AT (1) ATE531682T1 (https=)
DE (1) DE102005052444A1 (https=)
IL (1) IL177687A (https=)
MY (1) MY140577A (https=)
TW (1) TWI399340B (https=)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006043042A1 (de) * 2006-09-14 2008-03-27 H.C. Starck Gmbh Verfahren zur Herstellung von hochreinen Niobalkoxiden
US20090134369A1 (en) * 2007-11-26 2009-05-28 Applied Nanoworks, Inc. Metal alkoxides, apparatus for manufacturing metal alkoxides, related methods and uses thereof
CN102040478B (zh) * 2010-12-22 2013-03-13 南京大学 四乙氧基铪的合成方法
JP2012201630A (ja) * 2011-03-25 2012-10-22 Ube Industries Ltd 金属テトラ（１−アルキルイソブチルアルコキシド）の製造方法
JP2012201629A (ja) * 2011-03-25 2012-10-22 Ube Industries Ltd 高純度ジルコニウムアルコキシド原料及びその製造方法、並びに当該原料の分析方法
CN102766154B (zh) * 2012-07-28 2015-04-22 山东大学 一步溶剂法制备氧化锆纤维生产用有机聚锆前驱体或其甩丝液的方法
WO2017058160A1 (en) 2015-09-29 2017-04-06 Pryog, Llc Metal compositions and methods of making same

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1091433A (zh) * 1993-01-13 1994-08-31 希蒙特公司 乙烯聚合用催化剂组分及催化剂
CN1537089A (zh) * 2001-03-19 2004-10-13 Hc 制备钽和铌的烷氧化物的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4741894A (en) * 1986-06-03 1988-05-03 Morton Thiokol, Inc. Method of producing halide-free metal and hydroxides
JP2831431B2 (ja) * 1990-04-10 1998-12-02 株式会社ジャパンエナジー 高純度金属アルコキサイドの製造方法
JP2599855B2 (ja) 1991-11-25 1997-04-16 株式会社ジャパンエナジー タンタルアルコキシドの精製方法
JP2575562B2 (ja) 1991-11-25 1997-01-29 株式会社ジャパンエナジー タンタルアルコキシドの精製方法
JPH1036299A (ja) 1996-07-25 1998-02-10 Wako Pure Chem Ind Ltd 金属アルコキシドの精製方法
JP3911740B2 (ja) * 1996-11-18 2007-05-09 昭和電工株式会社 タンタルアルコキシドの製造方法
JP2001114791A (ja) 1999-10-14 2001-04-24 Showa Denko Kk 高純度ペンタアルコキシタンタルおよびその製造方法
JP2002161059A (ja) 2000-11-27 2002-06-04 Kojundo Chem Lab Co Ltd タンタルアルコキシドの精製方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1091433A (zh) * 1993-01-13 1994-08-31 希蒙特公司 乙烯聚合用催化剂组分及催化剂
CN1537089A (zh) * 2001-03-19 2004-10-13 Hc 制备钽和铌的烷氧化物的方法

Also Published As

Publication number Publication date
EP1764354B1 (de) 2011-11-02
JP5591437B2 (ja) 2014-09-17
CN1919813A (zh) 2007-02-28
KR20070026039A (ko) 2007-03-08
EP1764354A1 (de) 2007-03-21
TWI399340B (zh) 2013-06-21
JP2007070357A (ja) 2007-03-22
KR101359163B1 (ko) 2014-02-05
ATE531682T1 (de) 2011-11-15
IL177687A0 (en) 2006-12-31
JP2013144688A (ja) 2013-07-25
MY140577A (en) 2009-12-31
US20070056468A1 (en) 2007-03-15
US7273943B2 (en) 2007-09-25
DE102005052444A1 (de) 2007-03-01
CN103254035A (zh) 2013-08-21
IL177687A (en) 2010-11-30
TW200720191A (en) 2007-06-01

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