DE1006621B - Verfahren zur Auslaugung von durch Reduktion von Titantetrachlorid und einem Reduktionsmetall hergestelltem Titanmetall - Google Patents
Verfahren zur Auslaugung von durch Reduktion von Titantetrachlorid und einem Reduktionsmetall hergestelltem TitanmetallInfo
- Publication number
- DE1006621B DE1006621B DEN7327A DEN0007327A DE1006621B DE 1006621 B DE1006621 B DE 1006621B DE N7327 A DEN7327 A DE N7327A DE N0007327 A DEN0007327 A DE N0007327A DE 1006621 B DE1006621 B DE 1006621B
- Authority
- DE
- Germany
- Prior art keywords
- metal
- leaching
- titanium
- titanium metal
- reducing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229910052751 metal Inorganic materials 0.000 title claims description 56
- 239000002184 metal Substances 0.000 title claims description 56
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims description 46
- 239000010936 titanium Substances 0.000 title claims description 46
- 229910052719 titanium Inorganic materials 0.000 title claims description 46
- 238000002386 leaching Methods 0.000 title claims description 36
- 238000000034 method Methods 0.000 title claims description 22
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 title claims description 6
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 22
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 20
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 19
- 239000000243 solution Substances 0.000 claims description 15
- 239000003929 acidic solution Substances 0.000 claims description 14
- 239000002253 acid Substances 0.000 claims description 13
- 150000003839 salts Chemical class 0.000 claims description 13
- 230000002378 acidificating effect Effects 0.000 claims description 11
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 11
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 9
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 9
- 229910017604 nitric acid Inorganic materials 0.000 claims description 9
- 229910002651 NO3 Inorganic materials 0.000 claims description 8
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 8
- 239000011707 mineral Substances 0.000 claims description 8
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 7
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical group [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 claims description 4
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 claims description 4
- ZLXPLDLEBORRPT-UHFFFAOYSA-M [NH4+].[Fe+].[O-]S([O-])(=O)=O Chemical compound [NH4+].[Fe+].[O-]S([O-])(=O)=O ZLXPLDLEBORRPT-UHFFFAOYSA-M 0.000 claims description 3
- 229910000398 iron phosphate Inorganic materials 0.000 claims description 3
- 229910000358 iron sulfate Inorganic materials 0.000 claims description 3
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 3
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical compound [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims 1
- 239000012535 impurity Substances 0.000 description 16
- 238000002844 melting Methods 0.000 description 16
- 230000008018 melting Effects 0.000 description 16
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 12
- 239000003795 chemical substances by application Substances 0.000 description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 238000010891 electric arc Methods 0.000 description 6
- 229910052742 iron Inorganic materials 0.000 description 6
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 150000007513 acids Chemical class 0.000 description 4
- 239000003513 alkali Substances 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000000356 contaminant Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 229910052749 magnesium Inorganic materials 0.000 description 3
- -1 magnesium chloride Chemical class 0.000 description 3
- 239000004317 sodium nitrate Substances 0.000 description 3
- 235000010344 sodium nitrate Nutrition 0.000 description 3
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 239000003518 caustics Substances 0.000 description 2
- 150000003841 chloride salts Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 150000002823 nitrates Chemical class 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 235000005985 organic acids Nutrition 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000012264 purified product Substances 0.000 description 1
- 238000011946 reduction process Methods 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/022—Titanium tetrachloride
- C01G23/024—Purification of tetrachloride
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1295—Refining, melting, remelting, working up of titanium
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacture And Refinement Of Metals (AREA)
- ing And Chemical Polishing (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US321591XA | 1952-07-09 | 1952-07-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1006621B true DE1006621B (de) | 1957-04-18 |
Family
ID=21863421
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEN7327A Pending DE1006621B (de) | 1952-07-09 | 1953-06-15 | Verfahren zur Auslaugung von durch Reduktion von Titantetrachlorid und einem Reduktionsmetall hergestelltem Titanmetall |
| DEN8199A Pending DE1014330B (de) | 1952-07-09 | 1953-12-16 | Verfahren zur Herstellung eines gereinigten, fuer Lichtbogenschmelzung geeigneten Titanmetalls |
| DE1954N0009897 Pending DE1068022B (en, 2012) | 1952-07-09 | 1954-12-14 |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEN8199A Pending DE1014330B (de) | 1952-07-09 | 1953-12-16 | Verfahren zur Herstellung eines gereinigten, fuer Lichtbogenschmelzung geeigneten Titanmetalls |
| DE1954N0009897 Pending DE1068022B (en, 2012) | 1952-07-09 | 1954-12-14 |
Country Status (6)
| Country | Link |
|---|---|
| BE (2) | BE520666A (en, 2012) |
| CH (3) | CH321591A (en, 2012) |
| DE (3) | DE1006621B (en, 2012) |
| FR (3) | FR1085933A (en, 2012) |
| GB (3) | GB726367A (en, 2012) |
| NL (1) | NL83328C (en, 2012) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1111403B (de) | 1958-01-11 | 1961-07-20 | Sueddeutsche Kalkstickstoff | Verfahren zum Abtrennen der Erdalkalimetalle und Erdalkalioxyde aus dem Reaktionsprodukt der metallo-thermischen Herstellung von Titan oder Zirkonium |
| US7108539B2 (en) | 2002-06-04 | 2006-09-19 | Fci | Plug connector having a secondary locking system that engages during plug insertion |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2965521A (en) * | 1954-06-10 | 1960-12-20 | Crucible Steel Co America | Metal pickling solutions and methods |
| GB788308A (en) * | 1955-07-04 | 1957-12-23 | Ici Ltd | Improvements in or relating to the manufacture of titanium |
| GB788309A (en) * | 1955-08-11 | 1957-12-23 | Ici Ltd | Improvements in or relating to the manufacture of titanium |
| LU34971A1 (en, 2012) * | 1956-02-27 | |||
| US3102785A (en) * | 1956-09-21 | 1963-09-03 | Laporte Titanium Ltd | Process for the purification of titanium tetrachloride |
| BE563745A (en, 2012) * | 1957-01-08 | |||
| US2927855A (en) * | 1957-12-31 | 1960-03-08 | Nat Res Corp | Separation of tantalum |
| US3085874A (en) * | 1958-08-05 | 1963-04-16 | Union Carbide Corp | Metal purification process |
| TW278101B (en, 2012) * | 1994-03-08 | 1996-06-11 | Rgc Minerals Sands Ltd | |
| CN110270580A (zh) * | 2019-06-28 | 2019-09-24 | 攀钢集团钛业有限责任公司 | 粉状含钒干渣的处理方法 |
| CN110270579A (zh) * | 2019-06-28 | 2019-09-24 | 攀钢集团钛业有限责任公司 | 粉状含钒干渣的处理方法 |
-
1953
- 1953-06-09 GB GB1590653A patent/GB726367A/en not_active Expired
- 1953-06-10 GB GB1602253A patent/GB743735A/en not_active Expired
- 1953-06-11 CH CH321591D patent/CH321591A/de unknown
- 1953-06-11 NL NL179023A patent/NL83328C/xx active
- 1953-06-11 CH CH321960D patent/CH321960A/de unknown
- 1953-06-12 BE BE520666D patent/BE520666A/xx unknown
- 1953-06-13 FR FR1085933D patent/FR1085933A/fr not_active Expired
- 1953-06-15 DE DEN7327A patent/DE1006621B/de active Pending
- 1953-12-16 FR FR65485D patent/FR65485E/fr not_active Expired
- 1953-12-16 DE DEN8199A patent/DE1014330B/de active Pending
-
1954
- 1954-12-08 CH CH338969D patent/CH338969A/de unknown
- 1954-12-13 GB GB3603654A patent/GB752550A/en not_active Expired
- 1954-12-14 DE DE1954N0009897 patent/DE1068022B/de active Pending
- 1954-12-22 FR FR66249D patent/FR66249E/fr not_active Expired
-
1955
- 1955-01-18 BE BE534960D patent/BE534960A/xx unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1111403B (de) | 1958-01-11 | 1961-07-20 | Sueddeutsche Kalkstickstoff | Verfahren zum Abtrennen der Erdalkalimetalle und Erdalkalioxyde aus dem Reaktionsprodukt der metallo-thermischen Herstellung von Titan oder Zirkonium |
| US7108539B2 (en) | 2002-06-04 | 2006-09-19 | Fci | Plug connector having a secondary locking system that engages during plug insertion |
Also Published As
| Publication number | Publication date |
|---|---|
| GB752550A (en) | 1956-07-11 |
| FR1085933A (en, 2012) | 1955-02-08 |
| BE534960A (en, 2012) | 1958-11-07 |
| GB726367A (en) | 1955-03-16 |
| CH321960A (de) | 1957-05-31 |
| DE1014330B (de) | 1957-08-22 |
| FR66249E (fr) | 1956-06-05 |
| DE1068022B (en, 2012) | 1959-10-29 |
| CH338969A (de) | 1959-06-15 |
| GB743735A (en) | 1956-01-25 |
| NL83328C (en, 2012) | 1956-11-15 |
| CH321591A (de) | 1957-05-15 |
| BE520666A (en, 2012) | 1955-07-08 |
| FR65485E (fr) | 1956-02-21 |
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