CN1239570C - 用于制备金属氰化物催化剂多元醇引发剂淤浆的方法 - Google Patents

用于制备金属氰化物催化剂多元醇引发剂淤浆的方法 Download PDF

Info

Publication number
CN1239570C
CN1239570C CNB008195560A CN00819556A CN1239570C CN 1239570 C CN1239570 C CN 1239570C CN B008195560 A CNB008195560 A CN B008195560A CN 00819556 A CN00819556 A CN 00819556A CN 1239570 C CN1239570 C CN 1239570C
Authority
CN
China
Prior art keywords
compound
mixture
initiator
metal
inert organic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB008195560A
Other languages
English (en)
Chinese (zh)
Other versions
CN1452644A (zh
Inventor
R·M·韦迈耶
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Global Technologies LLC
Original Assignee
Dow Global Technologies LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies LLC filed Critical Dow Global Technologies LLC
Publication of CN1452644A publication Critical patent/CN1452644A/zh
Application granted granted Critical
Publication of CN1239570C publication Critical patent/CN1239570C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C08G65/10—Saturated oxiranes characterised by the catalysts used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyethers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Sludge (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB008195560A 2000-05-19 2000-07-07 用于制备金属氰化物催化剂多元醇引发剂淤浆的方法 Expired - Fee Related CN1239570C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/574,847 2000-05-19
US09/574,847 US6429166B1 (en) 2000-05-19 2000-05-19 Method for preparing metal cyanide catalyst/polyol initiator slurries

Publications (2)

Publication Number Publication Date
CN1452644A CN1452644A (zh) 2003-10-29
CN1239570C true CN1239570C (zh) 2006-02-01

Family

ID=24297899

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB008195560A Expired - Fee Related CN1239570C (zh) 2000-05-19 2000-07-07 用于制备金属氰化物催化剂多元醇引发剂淤浆的方法

Country Status (15)

Country Link
US (1) US6429166B1 (enExample)
EP (1) EP1290060B1 (enExample)
JP (1) JP4975935B2 (enExample)
KR (1) KR100707286B1 (enExample)
CN (1) CN1239570C (enExample)
AT (1) ATE400601T1 (enExample)
AU (1) AU2000260775A1 (enExample)
BR (1) BR0015890A (enExample)
CA (1) CA2408147C (enExample)
DE (1) DE60039463D1 (enExample)
ES (1) ES2304968T3 (enExample)
MX (1) MXPA02011432A (enExample)
TW (1) TW555594B (enExample)
WO (1) WO2001090216A1 (enExample)
ZA (1) ZA200209059B (enExample)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003080239A2 (en) 2002-03-19 2003-10-02 Dow Global Technologies, Inc. Method for preparing metal cyanide catalysts using insoluble metal salts
EP1490170A2 (en) * 2002-03-21 2004-12-29 Dow Global Technologies Inc. Method for preparing metal cyanide catalysts using zero valent metals
JP4921172B2 (ja) * 2003-05-22 2012-04-25 ダウ グローバル テクノロジーズ エルエルシー ナノスケールのｄｍｃ触媒粒子
KR20050041543A (ko) * 2003-10-31 2005-05-04 엘지전자 주식회사 광기록재생기의 디스플레이 제어방법 및 제어장치
US6869905B1 (en) * 2004-03-02 2005-03-22 Basf Corporation Synthesis of double metal cyanides with non-aqueous solutions
MX221601B (en) * 2004-05-14 2004-07-22 Basf Ag Functional fluids containing alkylene oxide copolymers having low pulmonary toxicity
JP2008518088A (ja) * 2004-10-26 2008-05-29 ダウ グローバル テクノロジーズ インコーポレイティド 活性水素含有化合物をアルコキシル化する改良方法及びそれから調製したアルコキシル化化合物
MX2009008311A (es) * 2007-02-05 2009-08-12 Basf Se Catalizadores de dmc, metodo para la produccion de los mismos y uso de los mismos.
HUE044164T2 (hu) 2009-10-19 2019-10-28 Basf Se Kettõs fém-cianid katalizátorok kondicionálása
WO2011160296A1 (en) 2010-06-23 2011-12-29 Basf Se Modified double metal cyanide catalyst
PL2748226T3 (pl) 2011-08-25 2016-02-29 Dow Global Technologies Llc Sposób wytwarzania polieteroalkoholi zawierających jednostki oksyetylenowe przez polimeryzację węglanu etylenu w obecności katalizatorów dimetalocyjankowych
KR102606479B1 (ko) * 2021-01-20 2023-11-24 아주대학교산학협력단 고순도의 하이드로젠 헥사시아노코발테이트 화합물 및 이의 제조 방법

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3278457A (en) 1963-02-14 1966-10-11 Gen Tire & Rubber Co Method of making a polyether using a double metal cyanide complex compound
AU552988B2 (en) 1982-03-31 1986-06-26 Shell Internationale Research Maatschappij B.V. Polymerizing epoxides and catalyst suspensions for this
AU551979B2 (en) 1982-03-31 1986-05-15 Shell Internationale Research Maatschappij B.V. Epoxy polymerisation catalysts
US5470813A (en) 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5482908A (en) 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5767323A (en) 1995-12-22 1998-06-16 Arco Chemical Technology, L.P. Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation
US5639705A (en) * 1996-01-19 1997-06-17 Arco Chemical Technology, L.P. Double metal cyanide catalysts and methods for making them
US5777177A (en) 1996-02-07 1998-07-07 Arco Chemical Technology, L.P. Preparation of double metal cyanide-catalyzed polyols by continuous addition of starter
US5627120A (en) * 1996-04-19 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5689012A (en) 1996-07-18 1997-11-18 Arco Chemical Technology, L.P. Continuous preparation of low unsaturation polyoxyalkylene polyether polyols with continuous additon of starter
DE19709031A1 (de) * 1997-03-06 1998-09-10 Basf Ag Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren
DE19730467A1 (de) 1997-07-16 1999-01-21 Bayer Ag Neue Zink/Metall-Hexacyanocobaltat-Katalysatoren für die Herstellung von Polyetherpolyolen
DE19809538A1 (de) 1998-03-05 1999-09-09 Basf Ag Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren
DE19809539A1 (de) * 1998-03-05 1999-09-09 Basf Ag Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren
US6063897A (en) * 1998-05-05 2000-05-16 Arco Chemical Technology, L.P. Acid-treated double metal cyanide complex catalysts
US6613714B2 (en) * 1999-06-02 2003-09-02 Basf Aktiengesellschaft Multimetal cyanide compounds, their preparation and their use
ES2244446T3 (es) * 1999-06-02 2005-12-16 Basf Aktiengesellschaft Procedimiento para la preparacion de polieterpolioles con empleo de catalizadores cristalinos de cianuros polimetalicos.
US6800583B2 (en) * 1999-06-02 2004-10-05 Basf Aktiengesellschaft Suspension of multimetal cyanide compounds, their preparation and their use
WO2001004178A1 (en) * 1999-07-09 2001-01-18 The Dow Chemical Company Polymerization of alkylene oxides using metal cyanide catalysts and unsaturated initiator compounds
AU5923400A (en) * 1999-07-09 2001-01-30 Dow Chemical Company, The Polymerization of ethylene oxide using metal cyanide catalysts

Also Published As

Publication number Publication date
AU2000260775A8 (enExample) 2002-02-21
AU2000260775A1 (en) 2001-12-03
JP2004516337A (ja) 2004-06-03
MXPA02011432A (es) 2003-06-06
KR100707286B1 (ko) 2007-04-16
ZA200209059B (en) 2003-11-27
TW555594B (en) 2003-10-01
WO2001090216A9 (en) 2004-02-12
US6429166B1 (en) 2002-08-06
EP1290060B1 (en) 2008-07-09
WO2001090216A1 (en) 2001-11-29
CA2408147C (en) 2009-01-06
BR0015890A (pt) 2003-06-10
CA2408147A1 (en) 2001-11-29
EP1290060A1 (en) 2003-03-12
DE60039463D1 (de) 2008-08-21
ATE400601T1 (de) 2008-07-15
JP4975935B2 (ja) 2012-07-11
CN1452644A (zh) 2003-10-29
KR20030017976A (ko) 2003-03-04
ES2304968T3 (es) 2008-11-01

Similar Documents

Publication Publication Date Title
CN1104954C (zh) 锌/金属六氰钴酸盐配位化合物,它们的制备方法,以及在聚醚多元醇生产过程中的应用
CN1239570C (zh) 用于制备金属氰化物催化剂多元醇引发剂淤浆的方法
CN1072225C (zh) 制备具有官能端基聚合物的保护了官能基的引发剂
CN1252129C (zh) 多金属氰化物化合物的制备
CN1138811C (zh) 用于制备聚醚多元醇的双金属氰化物催化剂
CN1205250C (zh) 使用金属氰化物催化剂聚合环氧乙烷
CN1142825C (zh) 制备聚醚多元醇的双金属氰化物催化剂
US11174333B2 (en) Macromonomers containing polyisobutene groups, and homopolymers or copolymers thereof
CN101077480A (zh) 可用于制备多元醇的双金属氰化物催化剂及其相关方法
CN1297967A (zh) 调理有机颜料的方法
CN1009934B (zh) 烯烃聚合催化剂
CN112142969A (zh) 一种苯酚聚氧乙烯醚的制备方法、高分子量苯酚聚氧乙烯聚氧丙烯醚的制备方法
US20110218321A1 (en) Processes for producing polyalkylene carbonates
TWI849041B (zh) 脂肪族聚碳酸酯、脂肪族聚碳酸酯組成物及其等之用途
CN1129477C (zh) 制备聚醚多元醇用的双金属氰化物催化剂
CN1642642A (zh) 用不溶解金属盐制备金属氰化物催化剂的方法
TW201916938A (zh) 高活性雙金屬氰化物觸媒及其製備方法與應用
CN1735647A (zh) 应用可聚合络合试剂制备金属氰化物催化剂的方法
CN1057847A (zh) 光刻胶和光学应用用的低光密度聚合物和共聚物的制备方法
CN112135858B (zh) 作为用于通过co2与环氧化物共聚来合成聚碳酸酯的引发剂的负载型鎓盐
HK1046417A1 (en) Double metal cyanide catalysts for the production of polyether polyols
EP3778022A1 (en) Method for preparing organic zinc catalyst, and method for preparing polyalkylene carbonate resin using organic zinc catalyst prepared therefby
CN110724039A (zh) 一种乙二醇单叔丁醚的制备方法
CN1204155C (zh) 用于烯烃聚合催化剂的配体及其过渡金属配合物
CN1289569C (zh) 用于制备聚醚型多元醇的双金属氰化物催化剂

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20060201

Termination date: 20120707