CN1239570C - 用于制备金属氰化物催化剂多元醇引发剂淤浆的方法 - Google Patents

用于制备金属氰化物催化剂多元醇引发剂淤浆的方法 Download PDF

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Publication number
CN1239570C
CN1239570C CNB008195560A CN00819556A CN1239570C CN 1239570 C CN1239570 C CN 1239570C CN B008195560 A CNB008195560 A CN B008195560A CN 00819556 A CN00819556 A CN 00819556A CN 1239570 C CN1239570 C CN 1239570C
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CN
China
Prior art keywords
compound
mixture
initiator
metal
inert organic
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Expired - Fee Related
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CNB008195560A
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English (en)
Chinese (zh)
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CN1452644A (zh
Inventor
R·M·韦迈耶
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Dow Global Technologies LLC
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Dow Global Technologies LLC
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Publication of CN1452644A publication Critical patent/CN1452644A/zh
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Publication of CN1239570C publication Critical patent/CN1239570C/zh
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C08G65/10—Saturated oxiranes characterised by the catalysts used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyethers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Treatment Of Sludge (AREA)
CNB008195560A 2000-05-19 2000-07-07 用于制备金属氰化物催化剂多元醇引发剂淤浆的方法 Expired - Fee Related CN1239570C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/574,847 US6429166B1 (en) 2000-05-19 2000-05-19 Method for preparing metal cyanide catalyst/polyol initiator slurries
US09/574,847 2000-05-19

Publications (2)

Publication Number Publication Date
CN1452644A CN1452644A (zh) 2003-10-29
CN1239570C true CN1239570C (zh) 2006-02-01

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CNB008195560A Expired - Fee Related CN1239570C (zh) 2000-05-19 2000-07-07 用于制备金属氰化物催化剂多元醇引发剂淤浆的方法

Country Status (15)

Country Link
US (1) US6429166B1 (enExample)
EP (1) EP1290060B1 (enExample)
JP (1) JP4975935B2 (enExample)
KR (1) KR100707286B1 (enExample)
CN (1) CN1239570C (enExample)
AT (1) ATE400601T1 (enExample)
AU (1) AU2000260775A1 (enExample)
BR (1) BR0015890A (enExample)
CA (1) CA2408147C (enExample)
DE (1) DE60039463D1 (enExample)
ES (1) ES2304968T3 (enExample)
MX (1) MXPA02011432A (enExample)
TW (1) TW555594B (enExample)
WO (1) WO2001090216A1 (enExample)
ZA (1) ZA200209059B (enExample)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR0308674A (pt) 2002-03-19 2005-02-01 Dow Global Technologies Inc Métodos para preparar catalisador de cianeto metálico usando sais metálicos insolúveis
MXPA04009144A (es) * 2002-03-21 2004-11-26 Dow Global Technologies Inc Metodo para preparar catalizadores de cianuro de metal usando metales de valencia cero.
DE602004004531T2 (de) * 2003-05-22 2007-06-06 Dow Global Technologies, Inc., Midland Nanoskalige dmc-katalysatorpartikel
KR20050041543A (ko) * 2003-10-31 2005-05-04 엘지전자 주식회사 광기록재생기의 디스플레이 제어방법 및 제어장치
US6869905B1 (en) * 2004-03-02 2005-03-22 Basf Corporation Synthesis of double metal cyanides with non-aqueous solutions
MX221601B (en) * 2004-05-14 2004-07-22 Basf Ag Functional fluids containing alkylene oxide copolymers having low pulmonary toxicity
KR101315527B1 (ko) * 2004-10-26 2013-10-08 다우 글로벌 테크놀로지스 엘엘씨 활성 수소 함유 화합물의 알콕시화를 위한 개량된 방법 및그로부터 제조된 알콕시화 화합물
MX2009008311A (es) * 2007-02-05 2009-08-12 Basf Se Catalizadores de dmc, metodo para la produccion de los mismos y uso de los mismos.
MX2012004169A (es) 2009-10-19 2012-05-08 Basf Se Acondicionado de catalizadores de cianuro de doble metal.
WO2011160296A1 (en) 2010-06-23 2011-12-29 Basf Se Modified double metal cyanide catalyst
CN103764715B (zh) 2011-08-25 2017-02-15 陶氏环球技术有限责任公司 通过碳酸乙二醇酯在双金属氰化物催化剂的存在下的聚合制备具有氧亚乙基单元的聚醚醇的方法
KR102606479B1 (ko) * 2021-01-20 2023-11-24 아주대학교산학협력단 고순도의 하이드로젠 헥사시아노코발테이트 화합물 및 이의 제조 방법

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3278457A (en) 1963-02-14 1966-10-11 Gen Tire & Rubber Co Method of making a polyether using a double metal cyanide complex compound
AU551979B2 (en) 1982-03-31 1986-05-15 Shell Internationale Research Maatschappij B.V. Epoxy polymerisation catalysts
AU552988B2 (en) 1982-03-31 1986-06-26 Shell Internationale Research Maatschappij B.V. Polymerizing epoxides and catalyst suspensions for this
US5470813A (en) 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5482908A (en) 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5767323A (en) 1995-12-22 1998-06-16 Arco Chemical Technology, L.P. Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation
US5639705A (en) 1996-01-19 1997-06-17 Arco Chemical Technology, L.P. Double metal cyanide catalysts and methods for making them
US5777177A (en) 1996-02-07 1998-07-07 Arco Chemical Technology, L.P. Preparation of double metal cyanide-catalyzed polyols by continuous addition of starter
US5627120A (en) * 1996-04-19 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5689012A (en) 1996-07-18 1997-11-18 Arco Chemical Technology, L.P. Continuous preparation of low unsaturation polyoxyalkylene polyether polyols with continuous additon of starter
DE19709031A1 (de) * 1997-03-06 1998-09-10 Basf Ag Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren
DE19730467A1 (de) 1997-07-16 1999-01-21 Bayer Ag Neue Zink/Metall-Hexacyanocobaltat-Katalysatoren für die Herstellung von Polyetherpolyolen
DE19809538A1 (de) 1998-03-05 1999-09-09 Basf Ag Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren
DE19809539A1 (de) * 1998-03-05 1999-09-09 Basf Ag Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren
US6063897A (en) * 1998-05-05 2000-05-16 Arco Chemical Technology, L.P. Acid-treated double metal cyanide complex catalysts
US6800583B2 (en) * 1999-06-02 2004-10-05 Basf Aktiengesellschaft Suspension of multimetal cyanide compounds, their preparation and their use
US6613714B2 (en) * 1999-06-02 2003-09-02 Basf Aktiengesellschaft Multimetal cyanide compounds, their preparation and their use
ES2244446T3 (es) * 1999-06-02 2005-12-16 Basf Aktiengesellschaft Procedimiento para la preparacion de polieterpolioles con empleo de catalizadores cristalinos de cianuros polimetalicos.
EP1200506B1 (en) * 1999-07-09 2006-04-12 Dow Global Technologies Inc. Polymerization of ethylene oxide using metal cyanide catalsyts
AU5788500A (en) * 1999-07-09 2001-01-30 Dow Chemical Company, The Polymerization of alkylene oxides using metal cyanide catalysts and unsaturated initiator compounds

Also Published As

Publication number Publication date
JP4975935B2 (ja) 2012-07-11
WO2001090216A1 (en) 2001-11-29
BR0015890A (pt) 2003-06-10
WO2001090216A9 (en) 2004-02-12
ATE400601T1 (de) 2008-07-15
CA2408147A1 (en) 2001-11-29
ES2304968T3 (es) 2008-11-01
TW555594B (en) 2003-10-01
JP2004516337A (ja) 2004-06-03
EP1290060B1 (en) 2008-07-09
CN1452644A (zh) 2003-10-29
DE60039463D1 (de) 2008-08-21
EP1290060A1 (en) 2003-03-12
US6429166B1 (en) 2002-08-06
MXPA02011432A (es) 2003-06-06
AU2000260775A8 (enExample) 2002-02-21
KR100707286B1 (ko) 2007-04-16
CA2408147C (en) 2009-01-06
AU2000260775A1 (en) 2001-12-03
ZA200209059B (en) 2003-11-27
KR20030017976A (ko) 2003-03-04

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Granted publication date: 20060201

Termination date: 20120707