CN1070474C - 甲苯二异氰酸酯的制法和甲苯二胺和水的特定混合物及其在制备甲苯二异氰酸酯中的用途 - Google Patents

甲苯二异氰酸酯的制法和甲苯二胺和水的特定混合物及其在制备甲苯二异氰酸酯中的用途 Download PDF

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Publication number
CN1070474C
CN1070474C CN96111631A CN96111631A CN1070474C CN 1070474 C CN1070474 C CN 1070474C CN 96111631 A CN96111631 A CN 96111631A CN 96111631 A CN96111631 A CN 96111631A CN 1070474 C CN1070474 C CN 1070474C
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CN
China
Prior art keywords
water
tda
tolylene diamine
mixture
toluene
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Expired - Lifetime
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CN96111631A
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English (en)
Chinese (zh)
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CN1149579A (zh
Inventor
K·比斯库
B·凯根霍夫
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Covestro Deutschland AG
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Bayer AG
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/44—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
    • C07C211/49—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring having at least two amino groups bound to the carbon skeleton
    • C07C211/50—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring having at least two amino groups bound to the carbon skeleton with at least two amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/36—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/84—Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
CN96111631A 1995-08-04 1996-08-02 甲苯二异氰酸酯的制法和甲苯二胺和水的特定混合物及其在制备甲苯二异氰酸酯中的用途 Expired - Lifetime CN1070474C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19528781A DE19528781A1 (de) 1995-08-04 1995-08-04 Verfahren zur Herstellung von Toluylendiisocyanat, spezielle Gemische aus Toluylendiamin und Wasser und deren Verwendung zur Herstellung von Toluylendiisocyanat
DE19528781.9 1995-08-04

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CNB001317962A Division CN1163470C (zh) 1995-08-04 1996-08-02 甲苯二胺和水的混合物及其在制甲苯二异氰酸酯中的用途

Publications (2)

Publication Number Publication Date
CN1149579A CN1149579A (zh) 1997-05-14
CN1070474C true CN1070474C (zh) 2001-09-05

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ID=7768754

Family Applications (2)

Application Number Title Priority Date Filing Date
CN96111631A Expired - Lifetime CN1070474C (zh) 1995-08-04 1996-08-02 甲苯二异氰酸酯的制法和甲苯二胺和水的特定混合物及其在制备甲苯二异氰酸酯中的用途
CNB001317962A Expired - Lifetime CN1163470C (zh) 1995-08-04 1996-08-02 甲苯二胺和水的混合物及其在制甲苯二异氰酸酯中的用途

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Application Number Title Priority Date Filing Date
CNB001317962A Expired - Lifetime CN1163470C (zh) 1995-08-04 1996-08-02 甲苯二胺和水的混合物及其在制甲苯二异氰酸酯中的用途

Country Status (15)

Country Link
US (2) US5849947A (enExample)
EP (2) EP1090906A1 (enExample)
JP (1) JP4095685B2 (enExample)
KR (1) KR100453862B1 (enExample)
CN (2) CN1070474C (enExample)
BR (1) BR9603278A (enExample)
CA (1) CA2182654A1 (enExample)
CZ (1) CZ292604B6 (enExample)
DE (2) DE19528781A1 (enExample)
ES (1) ES2176380T3 (enExample)
PL (1) PL184186B1 (enExample)
PT (1) PT757034E (enExample)
RU (1) RU2202537C2 (enExample)
TW (1) TW374080B (enExample)
UA (1) UA47399C2 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1896047B (zh) * 2005-07-12 2011-05-11 拜尔材料科学股份公司 甲苯二胺的制备方法

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KR100311692B1 (ko) * 1997-12-23 2001-11-15 신현준 활성탄소 섬유의 제조방법
EP1371633A1 (en) * 2002-06-14 2003-12-17 Bayer Ag Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column
DE60214195T2 (de) * 2002-10-22 2007-10-04 Bayer Materialscience Ag Verfahren zur Reinigung von Diisocyanatotoluol unter Verwendung einer Destillationskolonne mit Trennwand in der Endreinigung
DE10260093A1 (de) * 2002-12-19 2004-07-01 Basf Ag Verfahren zur Abtrennung von Isocyanaten aus einem Reaktionsgemisch
US7897805B2 (en) * 2005-03-10 2011-03-01 Mitsui Chemicals, Inc. Polyisocyanate production method and polyisocyanate production system
JP5175033B2 (ja) * 2005-03-10 2013-04-03 三井化学株式会社 ポリイソシアネートの製造方法およびポリイソシアネートの製造装置
HUE033435T2 (en) * 2005-07-12 2017-11-28 Covestro Deutschland Ag Process for preparing toluenediamine
DE102005036870A1 (de) * 2005-08-02 2007-02-08 Bayer Materialscience Ag Verfahren zur Gasphasenphosgenierung
JP4791783B2 (ja) * 2005-08-31 2011-10-12 三井化学株式会社 ポリイソシアネートの製造方法
DE102006022447A1 (de) * 2006-05-13 2007-11-15 Bayer Materialscience Ag Verfahren zur gekoppelten Herstellung von Chlor und Isocyanaten
US8030522B2 (en) * 2006-06-07 2011-10-04 Bayer Materialscience Llc Process for the production of toluene diisocyanate
CN100455559C (zh) * 2006-11-08 2009-01-28 大连理工大学 芳香族硝基化合物还原制备芳胺的方法
DE102006059678A1 (de) * 2006-12-18 2008-06-19 Bayer Materialscience Ag Verfahren zur Herstellung von aromatischen Aminen
DE102006060572A1 (de) † 2006-12-19 2008-06-26 Bayer Materialscience Ag Verfahren zur Herstellung von Toluylendiaminen durch katalytische Hydrierung von Dinitrotoluolen
WO2009069584A1 (ja) * 2007-11-27 2009-06-04 Mitsui Chemicals Polyurethanes, Inc. トリレンジアミンの脱水方法および脱水装置
PL2367783T3 (pl) 2008-11-19 2013-06-28 Basf Se Sposób wytwarzania izocyjanianu
CN101712621B (zh) * 2009-09-02 2012-10-31 甘肃银达化工有限公司 连续制备甲苯二胺的方法
CN101671277B (zh) * 2009-09-18 2011-12-28 天津大学 一种甲苯二异氰酸酯连续生产中热集成的溶剂回收方法
RU2518110C1 (ru) * 2010-03-18 2014-06-10 ХАНТСМЭН ИНТЕРНЭШНЛ ЭлЭлСи Способ преобразования ароматического нитросоединения в амины
JP5883661B2 (ja) * 2012-01-25 2016-03-15 旭化成ケミカルズ株式会社 Ｎ−置換カルバミン酸エステルの製造方法
IL236155B (en) * 2014-12-09 2021-10-31 List Holding Ag Chemical production methods and devices for their execution
CN110234624B (zh) * 2017-01-27 2023-03-21 科思创有限公司 稳定甲苯二胺残留物/水共混物的工艺、相关组合物及这类共混物作为燃料的用途
CN110105248B (zh) * 2019-05-31 2021-07-20 上海应用技术大学 一种甲苯二异氰酸酯的制备方法
US20230159433A1 (en) * 2020-05-19 2023-05-25 Covestro Deutschland Ag Method for preparing toluylene diamine mixtures
KR20240012559A (ko) * 2021-05-25 2024-01-29 바스프 에스이 적어도 1종의 폴리이소시아네이트의 제조 방법
EP4151619A1 (en) 2021-09-20 2023-03-22 Covestro Deutschland AG Method for the removal of water from and transport of aliphatic diamines
EP4653418A1 (de) 2024-05-22 2025-11-26 Covestro Deutschland AG Verfahren zur herstellung von organischem isocyanat mit verbesserter nachhaltigkeit

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1164519A (en) * 1966-07-19 1969-09-17 Inst Chemii Ogolnej Method for preparing Toluylenediisocyanates from Dinitrotoluenes

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GB786407A (en) * 1956-04-30 1957-11-20 Du Pont Process for the catalytic hydrogenation of organic nitro compounds
US2976320A (en) * 1957-07-30 1961-03-21 Allied Chem Catalytic hydrogenation of the dinitro derivatives of toluene
GB895197A (en) * 1960-11-25 1962-05-02 Gen Aniline & Film Corp Catalytic reduction of aromatic dinitro compounds
GB1303562A (enExample) * 1971-03-12 1973-01-17
DE2456308A1 (de) * 1974-11-28 1976-08-12 Bayer Ag Verfahren zur herstellung von aminoverbindungen
US4224249A (en) * 1979-05-14 1980-09-23 Air Products And Chemicals, Inc. Toluene diamine from non-washed dinitrotoluene
US4717774A (en) * 1985-12-20 1988-01-05 Basf Corporation Process for the preparation of toluene diamines
DE4230098C1 (enExample) * 1992-09-09 1993-06-03 Bayer Ag, 5090 Leverkusen, De
US5449832A (en) * 1994-10-05 1995-09-12 Air Products And Chemicals, Inc. Process for storage and transport of toluenediamine
US5714634A (en) * 1996-06-25 1998-02-03 Air Products And Chemicals, Inc. Process for storage and transport of toluenediamine
US5693862A (en) * 1996-12-18 1997-12-02 Arco Chemical Technology, L.P. Process for transport of toluenediamine

Patent Citations (1)

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Publication number Priority date Publication date Assignee Title
GB1164519A (en) * 1966-07-19 1969-09-17 Inst Chemii Ogolnej Method for preparing Toluylenediisocyanates from Dinitrotoluenes

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1896047B (zh) * 2005-07-12 2011-05-11 拜尔材料科学股份公司 甲苯二胺的制备方法

Also Published As

Publication number Publication date
BR9603278A (pt) 1998-05-12
KR100453862B1 (ko) 2005-04-08
EP0757034A1 (de) 1997-02-05
CZ292604B6 (cs) 2003-11-12
JPH0952873A (ja) 1997-02-25
CZ229996A3 (en) 1997-02-12
CA2182654A1 (en) 1997-02-05
EP1090906A1 (de) 2001-04-11
RU2202537C2 (ru) 2003-04-20
PL315490A1 (en) 1997-02-17
US6472564B1 (en) 2002-10-29
EP0757034B1 (de) 2002-06-05
DE19528781A1 (de) 1997-02-06
PL184186B1 (pl) 2002-09-30
US5849947A (en) 1998-12-15
MX9603167A (es) 1997-07-31
JP4095685B2 (ja) 2008-06-04
TW374080B (enExample) 1999-11-11
CN1332149A (zh) 2002-01-23
CN1149579A (zh) 1997-05-14
UA47399C2 (uk) 2002-07-15
ES2176380T3 (es) 2002-12-01
DE59609285D1 (de) 2002-07-11
CN1163470C (zh) 2004-08-25
KR970010735A (ko) 1997-03-27
PT757034E (pt) 2002-09-30
MX195147B (enExample) 2000-01-31

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Owner name: CARCOUSTICS TECHCONSULT GMBH

Free format text: FORMER OWNER: BAYER AKTIENGESELLSCHAFT

Effective date: 20120801

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Address after: Germany Leverkusen

Patentee after: Carcoustics Techconsult GmbH

Address before: Germany Leverkusen

Patentee before: Bayer Aktiengesellschaft

EE01 Entry into force of recordation of patent licensing contract

Application publication date: 19970514

Assignee: Bayer Material Science (China) Co., Ltd.

Assignor: Carcoustics Techconsult GmbH

Contract record no.: 2012990000854

Denomination of invention: Process for toluene diisocyanate and specific mixture of tolylene diamine and water and use in preparing toluene diisocyanate

Granted publication date: 20010905

License type: Common License

Record date: 20121128

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