KR100453862B1 - 톨루일렌디이소시아네이트의제조방법,톨루일렌디아민과물의특정혼합물및톨루일렌디이소시아네이트제조를위한혼합물의용도 - Google Patents
톨루일렌디이소시아네이트의제조방법,톨루일렌디아민과물의특정혼합물및톨루일렌디이소시아네이트제조를위한혼합물의용도 Download PDFInfo
- Publication number
- KR100453862B1 KR100453862B1 KR1019960032490A KR19960032490A KR100453862B1 KR 100453862 B1 KR100453862 B1 KR 100453862B1 KR 1019960032490 A KR1019960032490 A KR 1019960032490A KR 19960032490 A KR19960032490 A KR 19960032490A KR 100453862 B1 KR100453862 B1 KR 100453862B1
- Authority
- KR
- South Korea
- Prior art keywords
- water
- tda
- toluylene
- mixture
- diamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/43—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
- C07C211/44—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
- C07C211/49—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring having at least two amino groups bound to the carbon skeleton
- C07C211/50—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring having at least two amino groups bound to the carbon skeleton with at least two amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
- C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
- C07C209/36—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/84—Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19528781A DE19528781A1 (de) | 1995-08-04 | 1995-08-04 | Verfahren zur Herstellung von Toluylendiisocyanat, spezielle Gemische aus Toluylendiamin und Wasser und deren Verwendung zur Herstellung von Toluylendiisocyanat |
| DE19528781.9 | 1995-08-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR970010735A KR970010735A (ko) | 1997-03-27 |
| KR100453862B1 true KR100453862B1 (ko) | 2005-04-08 |
Family
ID=7768754
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019960032490A Expired - Lifetime KR100453862B1 (ko) | 1995-08-04 | 1996-08-03 | 톨루일렌디이소시아네이트의제조방법,톨루일렌디아민과물의특정혼합물및톨루일렌디이소시아네이트제조를위한혼합물의용도 |
Country Status (15)
| Country | Link |
|---|---|
| US (2) | US5849947A (enExample) |
| EP (2) | EP1090906A1 (enExample) |
| JP (1) | JP4095685B2 (enExample) |
| KR (1) | KR100453862B1 (enExample) |
| CN (2) | CN1070474C (enExample) |
| BR (1) | BR9603278A (enExample) |
| CA (1) | CA2182654A1 (enExample) |
| CZ (1) | CZ292604B6 (enExample) |
| DE (2) | DE19528781A1 (enExample) |
| ES (1) | ES2176380T3 (enExample) |
| PL (1) | PL184186B1 (enExample) |
| PT (1) | PT757034E (enExample) |
| RU (1) | RU2202537C2 (enExample) |
| TW (1) | TW374080B (enExample) |
| UA (1) | UA47399C2 (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101409694B1 (ko) * | 2006-12-18 | 2014-06-19 | 바이엘 머티리얼사이언스 아게 | 방향족 아민의 제조 방법 |
| KR101531731B1 (ko) * | 2007-11-27 | 2015-06-25 | 미쓰이 가가쿠 가부시키가이샤 | 톨릴렌다이아민의 탈수 방법 및 탈수 장치 |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100311692B1 (ko) * | 1997-12-23 | 2001-11-15 | 신현준 | 활성탄소 섬유의 제조방법 |
| EP1371633A1 (en) * | 2002-06-14 | 2003-12-17 | Bayer Ag | Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column |
| DE60214195T2 (de) * | 2002-10-22 | 2007-10-04 | Bayer Materialscience Ag | Verfahren zur Reinigung von Diisocyanatotoluol unter Verwendung einer Destillationskolonne mit Trennwand in der Endreinigung |
| DE10260093A1 (de) * | 2002-12-19 | 2004-07-01 | Basf Ag | Verfahren zur Abtrennung von Isocyanaten aus einem Reaktionsgemisch |
| US7897805B2 (en) * | 2005-03-10 | 2011-03-01 | Mitsui Chemicals, Inc. | Polyisocyanate production method and polyisocyanate production system |
| JP5175033B2 (ja) * | 2005-03-10 | 2013-04-03 | 三井化学株式会社 | ポリイソシアネートの製造方法およびポリイソシアネートの製造装置 |
| DE102005032430A1 (de) * | 2005-07-12 | 2007-01-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von Toluylendiamin |
| HUE033435T2 (en) * | 2005-07-12 | 2017-11-28 | Covestro Deutschland Ag | Process for preparing toluenediamine |
| DE102005036870A1 (de) * | 2005-08-02 | 2007-02-08 | Bayer Materialscience Ag | Verfahren zur Gasphasenphosgenierung |
| JP4791783B2 (ja) * | 2005-08-31 | 2011-10-12 | 三井化学株式会社 | ポリイソシアネートの製造方法 |
| DE102006022447A1 (de) * | 2006-05-13 | 2007-11-15 | Bayer Materialscience Ag | Verfahren zur gekoppelten Herstellung von Chlor und Isocyanaten |
| US8030522B2 (en) * | 2006-06-07 | 2011-10-04 | Bayer Materialscience Llc | Process for the production of toluene diisocyanate |
| CN100455559C (zh) * | 2006-11-08 | 2009-01-28 | 大连理工大学 | 芳香族硝基化合物还原制备芳胺的方法 |
| DE102006060572A1 (de) † | 2006-12-19 | 2008-06-26 | Bayer Materialscience Ag | Verfahren zur Herstellung von Toluylendiaminen durch katalytische Hydrierung von Dinitrotoluolen |
| PL2367783T3 (pl) | 2008-11-19 | 2013-06-28 | Basf Se | Sposób wytwarzania izocyjanianu |
| CN101712621B (zh) * | 2009-09-02 | 2012-10-31 | 甘肃银达化工有限公司 | 连续制备甲苯二胺的方法 |
| CN101671277B (zh) * | 2009-09-18 | 2011-12-28 | 天津大学 | 一种甲苯二异氰酸酯连续生产中热集成的溶剂回收方法 |
| RU2518110C1 (ru) * | 2010-03-18 | 2014-06-10 | ХАНТСМЭН ИНТЕРНЭШНЛ ЭлЭлСи | Способ преобразования ароматического нитросоединения в амины |
| JP5883661B2 (ja) * | 2012-01-25 | 2016-03-15 | 旭化成ケミカルズ株式会社 | N−置換カルバミン酸エステルの製造方法 |
| IL236155B (en) * | 2014-12-09 | 2021-10-31 | List Holding Ag | Chemical production methods and devices for their execution |
| CN110234624B (zh) * | 2017-01-27 | 2023-03-21 | 科思创有限公司 | 稳定甲苯二胺残留物/水共混物的工艺、相关组合物及这类共混物作为燃料的用途 |
| CN110105248B (zh) * | 2019-05-31 | 2021-07-20 | 上海应用技术大学 | 一种甲苯二异氰酸酯的制备方法 |
| US20230159433A1 (en) * | 2020-05-19 | 2023-05-25 | Covestro Deutschland Ag | Method for preparing toluylene diamine mixtures |
| KR20240012559A (ko) * | 2021-05-25 | 2024-01-29 | 바스프 에스이 | 적어도 1종의 폴리이소시아네이트의 제조 방법 |
| EP4151619A1 (en) | 2021-09-20 | 2023-03-22 | Covestro Deutschland AG | Method for the removal of water from and transport of aliphatic diamines |
| EP4653418A1 (de) | 2024-05-22 | 2025-11-26 | Covestro Deutschland AG | Verfahren zur herstellung von organischem isocyanat mit verbesserter nachhaltigkeit |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB786407A (en) * | 1956-04-30 | 1957-11-20 | Du Pont | Process for the catalytic hydrogenation of organic nitro compounds |
| US2976320A (en) * | 1957-07-30 | 1961-03-21 | Allied Chem | Catalytic hydrogenation of the dinitro derivatives of toluene |
| GB895197A (en) * | 1960-11-25 | 1962-05-02 | Gen Aniline & Film Corp | Catalytic reduction of aromatic dinitro compounds |
| GB1164519A (en) * | 1966-07-19 | 1969-09-17 | Inst Chemii Ogolnej | Method for preparing Toluylenediisocyanates from Dinitrotoluenes |
| GB1303562A (enExample) * | 1971-03-12 | 1973-01-17 | ||
| DE2456308A1 (de) * | 1974-11-28 | 1976-08-12 | Bayer Ag | Verfahren zur herstellung von aminoverbindungen |
| US4224249A (en) * | 1979-05-14 | 1980-09-23 | Air Products And Chemicals, Inc. | Toluene diamine from non-washed dinitrotoluene |
| US4717774A (en) * | 1985-12-20 | 1988-01-05 | Basf Corporation | Process for the preparation of toluene diamines |
| DE4230098C1 (enExample) * | 1992-09-09 | 1993-06-03 | Bayer Ag, 5090 Leverkusen, De | |
| US5449832A (en) * | 1994-10-05 | 1995-09-12 | Air Products And Chemicals, Inc. | Process for storage and transport of toluenediamine |
| US5714634A (en) * | 1996-06-25 | 1998-02-03 | Air Products And Chemicals, Inc. | Process for storage and transport of toluenediamine |
| US5693862A (en) * | 1996-12-18 | 1997-12-02 | Arco Chemical Technology, L.P. | Process for transport of toluenediamine |
-
1995
- 1995-08-04 DE DE19528781A patent/DE19528781A1/de not_active Withdrawn
-
1996
- 1996-07-23 PT PT96111809T patent/PT757034E/pt unknown
- 1996-07-23 DE DE59609285T patent/DE59609285D1/de not_active Expired - Lifetime
- 1996-07-23 EP EP01100055A patent/EP1090906A1/de not_active Ceased
- 1996-07-23 EP EP96111809A patent/EP0757034B1/de not_active Expired - Lifetime
- 1996-07-23 ES ES96111809T patent/ES2176380T3/es not_active Expired - Lifetime
- 1996-07-31 JP JP21690096A patent/JP4095685B2/ja not_active Expired - Lifetime
- 1996-08-01 US US08/691,222 patent/US5849947A/en not_active Expired - Lifetime
- 1996-08-02 CZ CZ19962299A patent/CZ292604B6/cs not_active IP Right Cessation
- 1996-08-02 RU RU96115368/04A patent/RU2202537C2/ru active
- 1996-08-02 CN CN96111631A patent/CN1070474C/zh not_active Expired - Lifetime
- 1996-08-02 CA CA002182654A patent/CA2182654A1/en not_active Abandoned
- 1996-08-02 TW TW85109303A patent/TW374080B/zh not_active IP Right Cessation
- 1996-08-02 PL PL96315490A patent/PL184186B1/pl not_active IP Right Cessation
- 1996-08-02 UA UA96083118A patent/UA47399C2/uk unknown
- 1996-08-02 CN CNB001317962A patent/CN1163470C/zh not_active Expired - Lifetime
- 1996-08-03 KR KR1019960032490A patent/KR100453862B1/ko not_active Expired - Lifetime
- 1996-08-05 BR BR9603278A patent/BR9603278A/pt not_active Application Discontinuation
-
1998
- 1998-09-08 US US09/149,379 patent/US6472564B1/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101409694B1 (ko) * | 2006-12-18 | 2014-06-19 | 바이엘 머티리얼사이언스 아게 | 방향족 아민의 제조 방법 |
| KR101531731B1 (ko) * | 2007-11-27 | 2015-06-25 | 미쓰이 가가쿠 가부시키가이샤 | 톨릴렌다이아민의 탈수 방법 및 탈수 장치 |
Also Published As
| Publication number | Publication date |
|---|---|
| BR9603278A (pt) | 1998-05-12 |
| EP0757034A1 (de) | 1997-02-05 |
| CZ292604B6 (cs) | 2003-11-12 |
| JPH0952873A (ja) | 1997-02-25 |
| CZ229996A3 (en) | 1997-02-12 |
| CA2182654A1 (en) | 1997-02-05 |
| EP1090906A1 (de) | 2001-04-11 |
| RU2202537C2 (ru) | 2003-04-20 |
| PL315490A1 (en) | 1997-02-17 |
| US6472564B1 (en) | 2002-10-29 |
| EP0757034B1 (de) | 2002-06-05 |
| DE19528781A1 (de) | 1997-02-06 |
| PL184186B1 (pl) | 2002-09-30 |
| US5849947A (en) | 1998-12-15 |
| MX9603167A (es) | 1997-07-31 |
| JP4095685B2 (ja) | 2008-06-04 |
| TW374080B (enExample) | 1999-11-11 |
| CN1332149A (zh) | 2002-01-23 |
| CN1149579A (zh) | 1997-05-14 |
| UA47399C2 (uk) | 2002-07-15 |
| ES2176380T3 (es) | 2002-12-01 |
| DE59609285D1 (de) | 2002-07-11 |
| CN1070474C (zh) | 2001-09-05 |
| CN1163470C (zh) | 2004-08-25 |
| KR970010735A (ko) | 1997-03-27 |
| PT757034E (pt) | 2002-09-30 |
| MX195147B (enExample) | 2000-01-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19960803 |
|
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| PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 20010803 Comment text: Request for Examination of Application Patent event code: PA02011R01I Patent event date: 19960803 Comment text: Patent Application |
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| E902 | Notification of reason for refusal | ||
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Comment text: Notification of reason for refusal Patent event date: 20040128 Patent event code: PE09021S01D |
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| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 20040831 |
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| GRNT | Written decision to grant | ||
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Comment text: Registration of Establishment Patent event date: 20041012 Patent event code: PR07011E01D |
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