CN106544896A - The method of gardenin dyed cotton fabric - Google Patents

The method of gardenin dyed cotton fabric Download PDF

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Publication number
CN106544896A
CN106544896A CN201611089316.8A CN201611089316A CN106544896A CN 106544896 A CN106544896 A CN 106544896A CN 201611089316 A CN201611089316 A CN 201611089316A CN 106544896 A CN106544896 A CN 106544896A
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CN
China
Prior art keywords
gardenin
ethanol
dyeing
cotton fabric
dyed cotton
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611089316.8A
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Chinese (zh)
Inventor
卢明
赵振云
周菁
刘欣
刘萍
刘一萍
李兰倩
樊涛
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Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611089316.8A priority Critical patent/CN106544896A/en
Publication of CN106544896A publication Critical patent/CN106544896A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/651—Compounds without nitrogen
    • D06P1/65106—Oxygen-containing compounds
    • D06P1/65125—Compounds containing ester groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58—Material containing hydroxyl groups
    • D06P3/60—Natural or regenerated cellulose

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

The invention provides a kind of method of gardenin dyed cotton fabric, the method comprises the steps：Gardenin is dissolved in ethanol/phenol mixed solution, surfactant benzyl benzoate is added, under ultrasound, is obtained clear solution；Bafta is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C dyeing.This staining technique need not be modified to gardenin, do not adopt high-temperature dyeing, and after dyeing, fabric color fastness is high.

Description

The method of gardenin dyed cotton fabric
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of method of gardenin dyed cotton fabric.
Background technology
Gardenin is a kind of natural pigment extracted from Maguireothamnus speciosus Fructus Gardeniae, is flavone compound.Gardenin can The depth yellow of different tones is obtained with different mordant dyeing agent dyeing.Gardenin yellow plant dye most widely used since being Qin Han Material.But gardenin is to cellulose fibres such as cottons, and directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that the effective dyed cotton fabric of gardenin, the present invention is adopted the following technical scheme that.
A kind of method of gardenin dyed cotton fabric, comprises the steps：（1）Phenol is dissolved in ethanol；（2）By Fructus Gardeniae Element is dissolved in ethanol/phenol mixed solution, is added surfactant benzyl benzoate, is obtained clear solution under ultrasound；（3） Bafta is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；（4）Arrangement after dyeing Wash in ethanol, dry under 80 C.
Further, the ethanol of described ethanol/phenol mixed solution and the mass ratio of phenol are 1:0.1~3.
Further, described surfactant benzyl benzoate is 1 with the mass ratio of ethanol/phenol mixed solution: 2000~8000。
Further, described gardenin and the mass ratio of ethanol/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention is, it is not necessary to gardenin is modified, high-temperature dyeing is not adopted, fabric after dyeing Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic is not construed as isolated, and they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
The method detailed step of gardenin dyed cotton fabric is as follows：
（1）20g phenol is dissolved in 180g ethanol；
（2）0.1g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.04g surfactant benzoic acid is added Benzyl ester, obtains clear solution under ultrasound；
（3）10g baftas are put in above-mentioned dye liquor, vibration is heated to 60 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 2
The method detailed step of gardenin dyed cotton fabric is as follows：
（1）300g phenol is dissolved in 100g ethanol；
（2）1g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.08g surfactant Benzyl Benzoates are added Ester, obtains clear solution under ultrasound；
（3）10g baftas are put in above-mentioned dye liquor, vibration is heated to 30 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 3
The method detailed step of gardenin dyed cotton fabric is as follows：
（1）50g phenol is dissolved in 250g ethanol；
（2）0.2g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.06g surfactant benzoic acid is added Benzyl ester, obtains clear solution under ultrasound；
（3）10g baftas are put in above-mentioned dye liquor, vibration is heated to 50 C, insulation dyeing 10min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 4
The method detailed step of gardenin dyed cotton fabric is as follows：
（1）200g phenol is dissolved in 200g ethanol；
（2）0.6g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.01g surfactant benzoic acid is added Benzyl ester, obtains clear solution under ultrasound；
（3）10g baftas are put in above-mentioned dye liquor, vibration is heated to 40 C, insulation dyeing 15min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. a kind of method of gardenin dyed cotton fabric, it is characterised in that comprise the steps：
（1）Phenol is dissolved in ethanol；
（2）Gardenin is dissolved in ethanol/phenol mixed solution, surfactant benzyl benzoate is added, under ultrasound To clear solution；
（3）Bafta is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
2. the method for gardenin dyed cotton fabric as claimed in claim 1, the ethanol of described ethanol/phenol mixed solution with The mass ratio of phenol is 1:0.1~3.
3. the method for gardenin dyed cotton fabric as claimed in claim 1, described surfactant benzyl benzoate and second The mass ratio of alcohol/phenol mixed solution is 1:2000~8000.
4. the method for gardenin dyed cotton fabric as claimed in claim 1, described gardenin and ethanol/phenol mixed solution Mass ratio be 1:200~4000.
CN201611089316.8A 2016-12-01 2016-12-01 The method of gardenin dyed cotton fabric Pending CN106544896A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611089316.8A CN106544896A (en) 2016-12-01 2016-12-01 The method of gardenin dyed cotton fabric

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611089316.8A CN106544896A (en) 2016-12-01 2016-12-01 The method of gardenin dyed cotton fabric

Publications (1)

Publication Number Publication Date
CN106544896A true CN106544896A (en) 2017-03-29

Family

ID=58396012

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611089316.8A Pending CN106544896A (en) 2016-12-01 2016-12-01 The method of gardenin dyed cotton fabric

Country Status (1)

Country Link
CN (1) CN106544896A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101736605A (en) * 2009-12-24 2010-06-16 江南大学 Single bath finishing technology for antibacterium and dyeing of textile by natural products
CN102943395A (en) * 2012-11-15 2013-02-27 沈阳洪达信息科技有限公司 Natural yellow series cotton fabric
CN103603213A (en) * 2013-11-28 2014-02-26 李振新 Method for dyeing cotton fabrics through vegetable dyes
CN103603212A (en) * 2013-11-28 2014-02-26 李振新 Method for dyeing cotton fabrics through color matching of natural vegetable dyes
CN105040473A (en) * 2015-06-29 2015-11-11 西南大学 Microextraction staining method for vegetable dyes
CN105821686A (en) * 2016-05-26 2016-08-03 杨江源 Method for dyeing cotton fiber fabric through natural plant dye

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101736605A (en) * 2009-12-24 2010-06-16 江南大学 Single bath finishing technology for antibacterium and dyeing of textile by natural products
CN102943395A (en) * 2012-11-15 2013-02-27 沈阳洪达信息科技有限公司 Natural yellow series cotton fabric
CN103603213A (en) * 2013-11-28 2014-02-26 李振新 Method for dyeing cotton fabrics through vegetable dyes
CN103603212A (en) * 2013-11-28 2014-02-26 李振新 Method for dyeing cotton fabrics through color matching of natural vegetable dyes
CN105040473A (en) * 2015-06-29 2015-11-11 西南大学 Microextraction staining method for vegetable dyes
CN105821686A (en) * 2016-05-26 2016-08-03 杨江源 Method for dyeing cotton fiber fabric through natural plant dye

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
唐人成等: "《双组分纤维纺织品的染色》", 31 October 2003, 中国纺织出版社 *
赵翰生: "《大众纺织技术史》", 30 June 2015, 济南：山东科学技术出版社 *

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Application publication date: 20170329