CN101736605A - Single bath finishing technology for antibacterium and dyeing of textile by natural products - Google Patents
Single bath finishing technology for antibacterium and dyeing of textile by natural products Download PDFInfo
- Publication number
- CN101736605A CN101736605A CN200910264875A CN200910264875A CN101736605A CN 101736605 A CN101736605 A CN 101736605A CN 200910264875 A CN200910264875 A CN 200910264875A CN 200910264875 A CN200910264875 A CN 200910264875A CN 101736605 A CN101736605 A CN 101736605A
- Authority
- CN
- China
- Prior art keywords
- natural products
- dyeing
- technology
- cotton fabric
- single bath
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Coloring (AREA)
Abstract
The invention provides a single bath finishing technology for antibacterium and dyeing of textile by natural products and relates to textile chemical technology. In the invention, natural products are used as raw materials to produce finishing agent. The raw material is preliminarily crushed by mini plant pulverizer into powder which is then arranged in the waterbath and stirred for some time before going through suction filtration and being produced into natural product finishing agent. The cation-modified cotton fabric is soaked in the finishing agent and treated with dyeing antibacterial finish by the single bath technology. The technology is simple and convenient to operate and energy-saving and environment-friendly. After the finishing, the fabric features good lustre, excellent antibacterial effect, and is nonhazardous to human body.
Description
Technical field
A kind of natural products single bath finishing technology antibiotic to textile dyeing that utilize belongs to the textile chemistry technical field.
Background technology
Synthetic dyestuffs have obtained being extensive use of with its colourful color and luster, good dyefastness and cheap price.Yet; advocate today of health, back to nature and promotion environmental protection in the whole world; synthetic dyestuffs more and more are subjected to people's attention to the nocuity of human body with to the shortcomings such as pollution of environment; and from natural products effective component extracting; because of it has good Environmental compatibility and biological degradability, just becoming the research focus of the ecological processing of textiles.
Utilize in the natural products finish fabric process, its drug activity composition, fragranced composition and natural colouring matter are absorbed by fabric together, and the drug effect active component promptly is the natural colouring matter composition under some situation, make the fabric after the dyeing have special medicinal health-care function.Patent CN200510028688.5 has invented a kind of preparation method of gamene vegetable dye, and the dyestuff of preparation is to people's nonhazardous, and certain medicinal health-care function is arranged.
Inorganic and organic antibacterial agent is widely used at present, but inorganic antiseptic contains metal ion more, and long-term contact easily causes skin problem, and the chemical substance that organic antibacterial agent adopts is artificial synthetic and non-biodegradation, can cause environment and health problem.Natural antibacterial agent comes from the plant, has advantage at aspects such as safety, environmental protection, more and more is subjected to people's attention.Patent CN200610042869.8 discloses the preparation method of a kind of botanical antiseptic, and this invention antibacterial effect is obvious, and free from environmental pollution, but its complex process, the operating time is long.Therefore, utilize the higher and natural products that have an antibacterial activity of pigment content to develop and integrate the antibiotic finishing technique of dyeing, shorten operation, energy savings has vast potential for future development.
Summary of the invention
The object of the present invention is to provide excellent lasting the dye finishing technique of antibiotic single bath process of natural products that utilizes of a kind of ecological, environmental protective, antibacterial effect.
Concrete experimental technique is as follows:
(1) natural products is pulverized 30～60min through FZ102 type microphyte pulverizer under rotating speed 1400rpm, get the natural products powder, described natural products powder is joined in the deionized water of 20～40 times of quality, under the magnetic stirring apparatus effect, stir 20～40min, mixing speed is 600～1000rpm, obtains natural products stoste;
(2) described natural products stoste is heated 60min under 60～80 ℃ water-bath, obtain the natural products dressing liquid through suction filtration;
(3) will put into initial temperature with 1: 30 bath raio through destarch, pure cotton fabric concise, bleaching is 40 ℃, 2,3-epoxypropyl trimethylammonium chloride ammonium concentration is that 2.5g/L, naoh concentration are in the modification liquid of 3g/L, speed with 2 ℃/min is warming up to 95 ℃, keep taking out fabric behind the 30min in 95 ℃, be washed to neutrality.
(4) will add in the described natural products dressing liquid according to bath raio 1: 40～80 through cation-modified COTTON FABRIC, in 80～100 ℃ of water-baths, handle 40～60min, wash 1～5min from the beginning, in 60～80 ℃ of convection oven, dry at 20～30 ℃.
Described natural products is cape jasmine, safflower, Asian puccoon, purple perilla, turmeric, dark plum.
The invention has the advantages that technical process is simple, energy savings and non-environmental-pollution, the fabric dye-uptake height after the arrangement, antibacterial effect are excellent lasting, and to human body nonhazardous effect.
The specific embodiment
The used test method:
1. dye-uptake test
With the absorbance of 722 type grating spectrophotometers dye liquor before and after the maximum absorption wave strong point is surveyed dyeing, calculate with following formula: dye-uptake (%)=(A
0-A)/A
0
In the formula: A
0Absorbance for dye liquor before dyeing; A is the absorbance of dyeing back raffinate.
2. the fabric face color depth is measured
The surface color degree of depth is represented with storehouse Bel's card-Munch equation usually:
In the formula: K is an absorption coefficient; S is a scattering coefficient; R is a spectral reflectance.
The mensuration of 3 antibacterial fabric performances
Test with reference to GB/T 20944.3-2008 antibacterial fabric method for testing performance.The anti-microbial property of sample is estimated by bacteriostasis rate, and computing formula is:
X
S＝(B-A)/B
In the formula: X
SBe bacteriostasis rate, %; A is the clump count on the sample of regularly cultivating; B is the clump count on " 0 " sample contact time.
Embodiment 1
(1) cape jasmine is pulverized 60min through FZ102 type microphyte pulverizer under rotating speed 1400rpm, get the cape jasmine powder, described cape jasmine powder is joined in the deionized water of 20 times of quality, under the magnetic stirring apparatus effect, stir 30min, mixing speed is 1000rpm, obtains cape jasmine stoste;
(2) described cape jasmine stoste is put into 70 ℃ of water-baths and heat 60min, obtain the cape jasmine dressing liquid through suction filtration;
(3) will put into initial temperature with 1: 30 bath raio through destarch, pure cotton fabric concise, bleaching is 40 ℃, 2,3-epoxypropyl trimethylammonium chloride ammonium concentration is that 2.5g/L, naoh concentration are in the modification liquid of 3g/L, speed with 2 ℃/min is warming up to 95 ℃, keep taking out fabric behind the 30min in 95 ℃, be washed to neutrality.
(4) described COTTON FABRIC after cation-modified is added in described cape jasmine dressing liquid according to bath raio at 1: 60, in 100 ℃ of water-baths, handle 50min, wash 3min from the beginning, in 80 ℃ of convection oven, dry at 20 ℃.
Fabric dye-uptake after above-mentioned arrangement is 45.3%, and the K/S value is 1.23, and bacteriostasis rate is 85%.
Embodiment 2
(1) Asian puccoon is pulverized 45min through FZ102 type microphyte pulverizer under rotating speed 1400rpm, get the Asian puccoon powder, described Asian puccoon powder is joined in the deionized water of 30 times of quality, under the magnetic stirring apparatus effect, stir 20min, mixing speed is 800rpm, obtains Asian puccoon stoste;
(2) described Asian puccoon stoste is put into 60 ℃ of water-baths and heat 60min, obtain the Asian puccoon dressing liquid through suction filtration;
(3) will put into temperature with 1: 30 bath raio through destarch, pure cotton fabric concise, bleaching is 40 ℃, 2,3-epoxypropyl trimethylammonium chloride ammonium concentration is that 2.5g/L, naoh concentration are in the modification liquid of 3g/L, speed with 2 ℃/min is warming up to 95 ℃, keep taking out fabric behind the 30min in 95 ℃, be washed to neutrality.
(4) described COTTON FABRIC after cation-modified is added in described Asian puccoon dressing liquid according to bath raio at 1: 80, in 80 ℃ of water-baths, handle 40min, wash 5min from the beginning, in 70 ℃ of convection oven, dry at 25 ℃.
Fabric dye-uptake after above-mentioned arrangement is 62.1%, and the K/S value is 4.21, and bacteriostasis rate is 87%.
Embodiment 3
(1) safflower is pulverized 30min through FZ102 type microphyte pulverizer under rotating speed 1400rpm, get the safflower powder, described safflower powder is joined in the deionized water of 40 times of quality, under the magnetic stirring apparatus effect, stir 40min, mixing speed is 600rpm, obtains safflower stoste;
(2) described safflower stoste is put into 80 ℃ of water-baths and heat 60min, obtain the safflower dressing liquid through suction filtration;
(3) will put into initial temperature with 1: 30 bath raio through destarch, pure cotton fabric concise, bleaching is 40 ℃, 2,3-epoxypropyl trimethylammonium chloride ammonium concentration is that 2.5g/L, naoh concentration are in the modification liquid of 3g/L, speed with 2 ℃/min is warming up to 95 ℃, keep taking out fabric behind the 30min in 95 ℃, be washed to neutrality.
(4) described COTTON FABRIC after cation-modified is added in described safflower dressing liquid according to bath raio at 1: 40, in 90 ℃ of water-baths, handle 60min, wash 1min from the beginning, in 60 ℃ of convection oven, dry at 30 ℃.
Fabric dye-uptake after above-mentioned arrangement is 52.6%, and the K/S value is 1.79, and bacteriostasis rate is 84%.
Claims (2)
1. one kind is utilized the natural products single bath finishing technology antibiotic to cotton fabric dyeing process, it is characterized in that this technology may further comprise the steps:
(1) natural products is pulverized 30～60min through FZ102 type microphyte pulverizer under rotating speed 1400rpm, get the natural products powder, described natural products powder is joined in the deionized water of 20～40 times of quality, under the magnetic stirring apparatus effect, stir 20～40min, mixing speed is 600～1000rpm, obtains natural products stoste;
(2) described natural products stoste is heated 60min under 60～80 ℃ water-bath, obtain the natural products dressing liquid through suction filtration;
(3) will add in the described natural products dressing liquid according to bath raio 1: 40～80 through cation-modified COTTON FABRIC, in 80～100 ℃ of water-baths, handle 40～60min, wash 1～5min from the beginning, in 60～80 ℃ of convection oven, dry at 20～30 ℃.
2. a kind of natural products single bath finishing technology antibiotic to cotton fabric dyeing process that utilize as claimed in claim 1, it is characterized in that: described natural products is cape jasmine, safflower, Asian puccoon, purple perilla, turmeric, dark plum.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910264875A CN101736605A (en) | 2009-12-24 | 2009-12-24 | Single bath finishing technology for antibacterium and dyeing of textile by natural products |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910264875A CN101736605A (en) | 2009-12-24 | 2009-12-24 | Single bath finishing technology for antibacterium and dyeing of textile by natural products |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101736605A true CN101736605A (en) | 2010-06-16 |
Family
ID=42460593
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910264875A Pending CN101736605A (en) | 2009-12-24 | 2009-12-24 | Single bath finishing technology for antibacterium and dyeing of textile by natural products |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101736605A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102367636A (en) * | 2011-07-28 | 2012-03-07 | 吴江兰瑞特纺织品有限公司 | Natural antibacterial textile containing turmeric extract and preparation process thereof |
| CN102433772A (en) * | 2011-09-07 | 2012-05-02 | 浙江理工大学 | Natural dye dyeing method based on non-damaging modification of real silk fabrics |
| CN102978972A (en) * | 2012-11-29 | 2013-03-20 | 常熟市新达纬编厂 | Dyeing method for yellow silk fabric |
| CN104532562A (en) * | 2014-12-23 | 2015-04-22 | 常熟市华博毛纺织有限公司 | Finishing process of garment fabric |
| CN105178069A (en) * | 2015-10-15 | 2015-12-23 | 绍兴文理学院 | Cotton fabric medium-free dyeing method |
| CN106351001A (en) * | 2016-08-26 | 2017-01-25 | 相里海霞 | Method for manufacturing ultraviolet-proof textile fabric based on moxa |
| CN106544890A (en) * | 2016-12-01 | 2017-03-29 | 西南大学 | Colouring method of the gardenin to bafta |
| CN106544896A (en) * | 2016-12-01 | 2017-03-29 | 西南大学 | The method of gardenin dyed cotton fabric |
| CN112877877A (en) * | 2021-01-05 | 2021-06-01 | 中山国泰染整有限公司 | Preparation process of cationic modified cotton fiber knitted fabric |
| CN115125742A (en) * | 2022-06-21 | 2022-09-30 | 苏州市职业大学 | Method for dyeing natural fiber at normal temperature by using alkannin |
-
2009
- 2009-12-24 CN CN200910264875A patent/CN101736605A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102367636A (en) * | 2011-07-28 | 2012-03-07 | 吴江兰瑞特纺织品有限公司 | Natural antibacterial textile containing turmeric extract and preparation process thereof |
| CN102433772A (en) * | 2011-09-07 | 2012-05-02 | 浙江理工大学 | Natural dye dyeing method based on non-damaging modification of real silk fabrics |
| CN102433772B (en) * | 2011-09-07 | 2014-04-09 | 浙江理工大学 | Natural dye dyeing method based on non-damaging modification of real silk fabrics |
| CN102978972A (en) * | 2012-11-29 | 2013-03-20 | 常熟市新达纬编厂 | Dyeing method for yellow silk fabric |
| CN104532562A (en) * | 2014-12-23 | 2015-04-22 | 常熟市华博毛纺织有限公司 | Finishing process of garment fabric |
| CN105178069A (en) * | 2015-10-15 | 2015-12-23 | 绍兴文理学院 | Cotton fabric medium-free dyeing method |
| CN106351001A (en) * | 2016-08-26 | 2017-01-25 | 相里海霞 | Method for manufacturing ultraviolet-proof textile fabric based on moxa |
| CN106544890A (en) * | 2016-12-01 | 2017-03-29 | 西南大学 | Colouring method of the gardenin to bafta |
| CN106544896A (en) * | 2016-12-01 | 2017-03-29 | 西南大学 | The method of gardenin dyed cotton fabric |
| CN112877877A (en) * | 2021-01-05 | 2021-06-01 | 中山国泰染整有限公司 | Preparation process of cationic modified cotton fiber knitted fabric |
| CN115125742A (en) * | 2022-06-21 | 2022-09-30 | 苏州市职业大学 | Method for dyeing natural fiber at normal temperature by using alkannin |
| CN115125742B (en) * | 2022-06-21 | 2023-08-15 | 苏州市职业大学 | Method for dyeing natural fiber at normal temperature by shikonin |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101736605A (en) | Single bath finishing technology for antibacterium and dyeing of textile by natural products | |
| Vankar et al. | Ultrasonic dyeing of cotton fabric with aqueous extract of Eclipta alba | |
| Adeel et al. | Appraisal of marigold flower based lutein as natural colourant for textile dyeing under the influence of gamma radiations | |
| CN100540799C (en) | The dye yam extract is to the colouring method of silk broadcloth | |
| CN101851868B (en) | Ecological dyeing method for dyeing cotton fabric with mulberry red natural dye | |
| CN103265823A (en) | Pomegranate rind nature dye preparation and application of pomegranate rind nature dye in fabric | |
| CN100549102C (en) | The preparation method of spatholobus stem natural dye | |
| CN102634993A (en) | Method for dyeing cotton fibers by using natural dye | |
| Mongkholrattanasit et al. | Natural dye from eucalyptus leaves and application for wool fabric dyeing by using padding techniques | |
| CN105970675A (en) | Method for dyeing natural fiber fabric with vegetable dye | |
| CN105297493A (en) | Method for dyeing real silk fabric by adopting natural dyestuff | |
| CN103725032A (en) | Preparation method and application of natural lotus receptacle pigment | |
| CN104894890A (en) | One-bath dyeing method of wool fabric or silk fabric based on natural xanthophyll | |
| Chungkrang et al. | Natural dyes: extraction and applications | |
| CN104073022A (en) | Preparation and application of onion-skin natural dye | |
| CN104611947B (en) | Make natural plants dyed cloth or the method for silk goods | |
| CN102094341B (en) | A kind of colouring method of real silk fabrics by extracting pigment from phytolacca by ultrasonic technology | |
| CN109537314B (en) | Dyeing method of natural black dye of real silk fabric | |
| Rashdi et al. | Lyocell fabric dyed with natural dye extracted from marigold flower using metallic salts | |
| CN104059380B (en) | The preparation of Waxberry fruit natural dyestuff and application thereof | |
| CN102924965B (en) | Tea tree fruit reddish brown pigment and its preparation method and use | |
| CN104140689B (en) | The method of natural pigment is extracted from Ramulus et folium taxi cuspidatae pharmacy residue | |
| Vastrad et al. | Dyeing of cotton yarn with marigold (Tagetes erecta) petals: An emphasis on pre-treatments and mordants | |
| CN102978972A (en) | Dyeing method for yellow silk fabric | |
| CN105544238A (en) | Printing color paste containing grape pigment and printing process by using the same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Open date: 20100616 |