CN106544890A - Colouring method of the gardenin to bafta - Google Patents

Colouring method of the gardenin to bafta Download PDF

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Publication number
CN106544890A
CN106544890A CN201611088942.5A CN201611088942A CN106544890A CN 106544890 A CN106544890 A CN 106544890A CN 201611088942 A CN201611088942 A CN 201611088942A CN 106544890 A CN106544890 A CN 106544890A
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CN
China
Prior art keywords
gardenin
carbon tetrachloride
bafta
dyeing
phenol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611088942.5A
Other languages
Chinese (zh)
Inventor
卢明
胡睿敏
刘萍
刘一萍
李兰倩
樊涛
赵振云
周菁
刘欣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611088942.5A priority Critical patent/CN106544890A/en
Publication of CN106544890A publication Critical patent/CN106544890A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621Compounds without nitrogen
    • D06P1/622Sulfonic acids or their salts
    • D06P1/625Aromatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58Material containing hydroxyl groups
    • D06P3/60Natural or regenerated cellulose

Abstract

The invention provides a kind of colouring method of gardenin to bafta, the method comprises the steps:Gardenin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, under ultrasound, is obtained clear solution;Bafta is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C dyeing.This staining technique need not be modified to gardenin, do not adopt high-temperature dyeing, and after dyeing, fabric color fastness is high.

Description

Colouring method of the gardenin to bafta
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing side of gardenin to bafta Method.
Background technology
Gardenin is a kind of natural colouring matter extracted from madder wort cape jasmine, is flavone compound.Gardenin can The depth yellow of different tones is obtained with different mordant dyeing agent dyeing.Gardenin yellow plant dye most widely used since being Qin Han Material.But gardenin is to cellulose fibres such as cottons, and directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that the effective dyed cotton fabric of gardenin, the present invention is adopted the following technical scheme that.
A kind of colouring method of gardenin to bafta, comprises the steps:(1)Phenol is dissolved in carbon tetrachloride;(2) Gardenin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, under ultrasound Obtain clear solution;(3)Bafta is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing; (4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~ 3。
Further, the matter of described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and carbon tetrachloride/phenol mixed solution Amount is than being 1:2000~8000.
Further, described gardenin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention is, it is not necessary to gardenin is modified, high-temperature dyeing is not adopted, fabric after dyeing Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic is not construed as isolated, and they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
Gardenin is as follows to the colouring method detailed step of bafta:
(1)20g phenol is dissolved in 180g carbon tetrachloride;
(2)0.1g gardenins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants ten are added Dialkyl benzene sulfonic acids sodium, obtains clear solution under ultrasound;
(3)10g baftas are put in above-mentioned dye liquor, vibration is heated to 60 C, insulation dyeing 30min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 2
Gardenin is as follows to the colouring method detailed step of bafta:
(1)300g phenol is dissolved in 100g carbon tetrachloride;
(2)1g gardenins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surfactants 12 are added Sodium alkyl benzene sulfonate, obtains clear solution under ultrasound;
(3)10g baftas are put in above-mentioned dye liquor, vibration is heated to 30 C, insulation dyeing 30min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 3
Gardenin is as follows to the colouring method detailed step of bafta:
(1)50g phenol is dissolved in 250g carbon tetrachloride;
(2)0.2g gardenins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants ten are added Dialkyl benzene sulfonic acids sodium, obtains clear solution under ultrasound;
(3)10g baftas are put in above-mentioned dye liquor, vibration is heated to 50 C, insulation dyeing 10min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 4
Gardenin is as follows to the colouring method detailed step of bafta:
(1)200g phenol is dissolved in 200g carbon tetrachloride;
(2)0.6g gardenins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surfactants ten are added Dialkyl benzene sulfonic acids sodium, obtains clear solution under ultrasound;
(3)10g baftas are put in above-mentioned dye liquor, vibration is heated to 40 C, insulation dyeing 15min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. colouring method of a kind of gardenin to bafta, it is characterised in that comprise the steps:
(1)Phenol is dissolved in carbon tetrachloride;
(2)Gardenin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid is added Sodium, obtains clear solution under ultrasound;
(3)Bafta is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
2. colouring method of the gardenin as claimed in claim 1 to bafta, described carbon tetrachloride/phenol mixed solution Carbon tetrachloride is 1 with the mass ratio of phenol:0.1~3.
3. colouring method of the gardenin as claimed in claim 1 to bafta, described surfactant sodium dodecyl base benzene sulphur Sour sodium is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. colouring method of the gardenin as claimed in claim 1 to bafta, described gardenin are mixed with carbon tetrachloride/phenol The mass ratio for closing solution is 1:200~4000.
CN201611088942.5A 2016-12-01 2016-12-01 Colouring method of the gardenin to bafta Pending CN106544890A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611088942.5A CN106544890A (en) 2016-12-01 2016-12-01 Colouring method of the gardenin to bafta

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611088942.5A CN106544890A (en) 2016-12-01 2016-12-01 Colouring method of the gardenin to bafta

Publications (1)

Publication Number Publication Date
CN106544890A true CN106544890A (en) 2017-03-29

Family

ID=58396023

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611088942.5A Pending CN106544890A (en) 2016-12-01 2016-12-01 Colouring method of the gardenin to bafta

Country Status (1)

Country Link
CN (1) CN106544890A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN101736605A (en) * 2009-12-24 2010-06-16 江南大学 Single bath finishing technology for antibacterium and dyeing of textile by natural products
CN103437141A (en) * 2013-08-28 2013-12-11 河北宁纺集团有限责任公司 Dyeing treatment process for pure cotton fabrics based on pure natural biological preparations
CN103451965A (en) * 2013-08-28 2013-12-18 句容市后白镇迎瑞印花厂 Natural dyeing method of yellow modal fabric

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN101736605A (en) * 2009-12-24 2010-06-16 江南大学 Single bath finishing technology for antibacterium and dyeing of textile by natural products
CN103437141A (en) * 2013-08-28 2013-12-11 河北宁纺集团有限责任公司 Dyeing treatment process for pure cotton fabrics based on pure natural biological preparations
CN103451965A (en) * 2013-08-28 2013-12-18 句容市后白镇迎瑞印花厂 Natural dyeing method of yellow modal fabric

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
何瑾馨: "《染料化学》", 31 October 2016, 中国纺织出版社 *

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Application publication date: 20170329