CN106544892A - Colouring method of the gardenin to silk fabric - Google Patents

Colouring method of the gardenin to silk fabric Download PDF

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Publication number
CN106544892A
CN106544892A CN201611088949.7A CN201611088949A CN106544892A CN 106544892 A CN106544892 A CN 106544892A CN 201611088949 A CN201611088949 A CN 201611088949A CN 106544892 A CN106544892 A CN 106544892A
Authority
CN
China
Prior art keywords
gardenin
carbon tetrachloride
silk fabric
dyeing
phenol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611088949.7A
Other languages
Chinese (zh)
Inventor
卢明
周菁
刘萍
刘一萍
李兰倩
樊涛
赵振云
刘欣
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Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611088949.7A priority Critical patent/CN106544892A/en
Publication of CN106544892A publication Critical patent/CN106544892A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621—Compounds without nitrogen
    • D06P1/622—Sulfonic acids or their salts
    • D06P1/625—Aromatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02—Material containing basic nitrogen
    • D06P3/04—Material containing basic nitrogen containing amide groups

Abstract

The invention provides a kind of colouring method of gardenin to silk fabric, the method comprises the steps：Gardenin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, under ultrasound, is obtained clear solution；Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C dyeing.This staining technique need not be modified to gardenin, do not adopt high-temperature dyeing, and after dyeing, fabric color fastness is high.

Description

Colouring method of the gardenin to silk fabric
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing side of gardenin to silk fabric Method.
Background technology
Gardenin is a kind of natural pigment extracted from Maguireothamnus speciosus Fructus Gardeniae, is flavone compound.Gardenin can The depth yellow of different tones is obtained with different mordant dyeing agent dyeing.Gardenin yellow plant dye most widely used since being Qin Han Material.But gardenin is to protein fibres such as silks, and directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that gardenin effectively dyes silk fabric, the present invention is adopted the following technical scheme that.
A kind of colouring method of gardenin to silk fabric, comprises the steps：（1）Phenol is dissolved in carbon tetrachloride； （2）Gardenin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, is surpassed Clear solution is obtained under sound；（3）Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation dyeing 5 ~ 30min；（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~ 3。
Further, the matter of described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and carbon tetrachloride/phenol mixed solution Amount is than being 1:2000~8000.
Further, described gardenin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention is, it is not necessary to gardenin is modified, high-temperature dyeing is not adopted, fabric after dyeing Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic is not construed as isolated, and they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
Gardenin is as follows to the colouring method detailed step of silk fabric：
（1）20g phenol is dissolved in 180g carbon tetrachloride；
（2）0.1g gardenins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants ten are added Dialkyl benzene sulfonic acids sodium, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 60 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 2
Gardenin is as follows to the colouring method detailed step of silk fabric：
（1）300g phenol is dissolved in 100g carbon tetrachloride；
（2）1g gardenins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surfactants 12 are added Sodium alkyl benzene sulfonate, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 30 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 3
Gardenin is as follows to the colouring method detailed step of silk fabric：
（1）50g phenol is dissolved in 250g carbon tetrachloride；
（2）0.2g gardenins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants ten are added Dialkyl benzene sulfonic acids sodium, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 50 C, insulation dyeing 10min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 4
Gardenin is as follows to the colouring method detailed step of silk fabric：
（1）200g phenol is dissolved in 200g carbon tetrachloride；
（2）0.6g gardenins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surfactants ten are added Dialkyl benzene sulfonic acids sodium, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 40 C, insulation dyeing 15min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. colouring method of a kind of gardenin to silk fabric, it is characterised in that comprise the steps：
（1）Phenol is dissolved in carbon tetrachloride；
（2）Gardenin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzenesulfonic acid is added Sodium, obtains clear solution under ultrasound；
（3）Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
2. colouring method of the gardenin as claimed in claim 1 to silk fabric, described carbon tetrachloride/phenol mixed solution The mass ratio of carbon tetrachloride and phenol be 1:0.1~3.
3. colouring method of the gardenin as claimed in claim 1 to silk fabric, described surfactant sodium dodecyl base benzene Sodium sulfonate is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. colouring method of the gardenin as claimed in claim 1 to silk fabric, described gardenin and carbon tetrachloride/phenol The mass ratio of mixed solution is 1:200~4000.
CN201611088949.7A 2016-12-01 2016-12-01 Colouring method of the gardenin to silk fabric Pending CN106544892A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611088949.7A CN106544892A (en) 2016-12-01 2016-12-01 Colouring method of the gardenin to silk fabric

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611088949.7A CN106544892A (en) 2016-12-01 2016-12-01 Colouring method of the gardenin to silk fabric

Publications (1)

Publication Number Publication Date
CN106544892A true CN106544892A (en) 2017-03-29

Family

ID=58396013

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611088949.7A Pending CN106544892A (en) 2016-12-01 2016-12-01 Colouring method of the gardenin to silk fabric

Country Status (1)

Country Link
CN (1) CN106544892A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103174041A (en) * 2013-04-12 2013-06-26 祝洪哲 Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye
CN103741505A (en) * 2013-12-20 2014-04-23 大连创达技术交易市场有限公司 Silk dyeing process adopting gardenia yellow vegetable dye
CN106087476A (en) * 2016-08-19 2016-11-09 宁波原真生态纺织科技有限公司 Dyeing technique on a kind of colorant match based on vegetable colour

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103174041A (en) * 2013-04-12 2013-06-26 祝洪哲 Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye
CN103741505A (en) * 2013-12-20 2014-04-23 大连创达技术交易市场有限公司 Silk dyeing process adopting gardenia yellow vegetable dye
CN106087476A (en) * 2016-08-19 2016-11-09 宁波原真生态纺织科技有限公司 Dyeing technique on a kind of colorant match based on vegetable colour

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
徐以俊 等: "《石油化工关联行业概览——精细化学品（一）》", 30 June 1992, 上海科学普及出版社 *

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Application publication date: 20170329