CN106544894A - Colouring method of the alizarin to silk fabric - Google Patents
Colouring method of the alizarin to silk fabric Download PDFInfo
- Publication number
- CN106544894A CN106544894A CN201611089019.3A CN201611089019A CN106544894A CN 106544894 A CN106544894 A CN 106544894A CN 201611089019 A CN201611089019 A CN 201611089019A CN 106544894 A CN106544894 A CN 106544894A
- Authority
- CN
- China
- Prior art keywords
- alizarin
- carbon tetrachloride
- silk fabric
- dyeing
- phenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The invention provides a kind of colouring method of alizarin to silk fabric, the method comprises the steps：Alizarin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, under ultrasound, is obtained clear solution；Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C dyeing.This staining technique need not be modified to alizarin, do not adopt high-temperature dyeing, and after dyeing, fabric color fastness is high.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing side of alizarin to silk fabric
Method.
Background technology
Alizarin is a kind of typical mordant dyes.Can extract from Radix Rubiae root.Before 3500, alizarin just the Central Asia,
Egyptian, Europe and China are used as orchil.Alizarin is red acicular crystal, is practically insoluble in water, used as natural plant
Thing dyestuff is used to make the red textile of hot flame.Alizarin is used for the dyeing of cotton and stamp, obtains hunting pink during with aluminum mordant,
HONGGUANG brown is obtained during with chromium stain matchmaker, purple during with iron mordant, is obtained, gold-tinted is obtained during tin mordanting agent red.But it is alizarin
Directly upper dye is poor to protein fibres such as silks for element, and color fastness is poor.
The content of the invention
In order that alizarin effectively dyes silk fabric, the present invention is adopted the following technical scheme that.
A kind of colouring method of alizarin to silk fabric, comprises the steps：（1）Phenol is dissolved in carbon tetrachloride；（2）
Alizarin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, under ultrasound
To clear solution；（3）Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~
3。
Further, the matter of described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and carbon tetrachloride/phenol mixed solution
Amount is than being 1:2000~8000.
Further, described alizarin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention is, it is not necessary to alizarin is modified, high-temperature dyeing is not adopted, fabric color after dyeing
Fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic is not construed as isolated, and they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
Alizarin is as follows to the colouring method detailed step of silk fabric：
（1）20g phenol is dissolved in 180g carbon tetrachloride；
（2）0.8g alizarins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants 12 are added
Sodium alkyl benzene sulfonate, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 60 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 2
Alizarin is as follows to the colouring method detailed step of silk fabric：
（1）300g phenol is dissolved in 100g carbon tetrachloride；
（2）0.1g alizarins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surfactants 12 are added
Sodium alkyl benzene sulfonate, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 30 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 3
Alizarin is as follows to the colouring method detailed step of silk fabric：
（1）50g phenol is dissolved in 250g carbon tetrachloride；
（2）0.7g alizarins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants 12 are added
Sodium alkyl benzene sulfonate, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 50 C, insulation dyeing 10min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Embodiment 4
Alizarin is as follows to the colouring method detailed step of silk fabric：
（1）200g phenol is dissolved in 200g carbon tetrachloride；
（2）1g alizarins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surfactant sodium dodecyls are added
Base benzene sulfonic acid sodium salt, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 40 C, insulation dyeing 15min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. colouring method of a kind of alizarin to silk fabric, it is characterised in that comprise the steps：
（1）Phenol is dissolved in carbon tetrachloride；
（2）Alizarin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added,
Clear solution is obtained under ultrasound；
（3）Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80 C.
2. colouring method of the alizarin as claimed in claim 1 to silk fabric, described carbon tetrachloride/phenol mixed solution
Carbon tetrachloride is 1 with the mass ratio of phenol:0.1~3.
3. colouring method of the alizarin as claimed in claim 1 to silk fabric, described surfactant sodium dodecyl base benzene sulphur
Sour sodium is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. colouring method of the alizarin as claimed in claim 1 to silk fabric, described alizarin are mixed with carbon tetrachloride/phenol
The mass ratio of solution is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089019.3A CN106544894A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the alizarin to silk fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089019.3A CN106544894A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the alizarin to silk fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106544894A true CN106544894A (en) | 2017-03-29 |
Family
ID=58396409
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611089019.3A Pending CN106544894A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the alizarin to silk fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106544894A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102634995A (en) * | 2012-04-20 | 2012-08-15 | 浙江理工大学 | Method for preparing silk fabric for cultural relic protection |
| CN103410017A (en) * | 2013-07-18 | 2013-11-27 | 祝洪哲 | Ecologic self-cleaning skin care fabric processed through using purely natural Chinese herbal medicinal plant dye |
| CN106087475A (en) * | 2016-08-19 | 2016-11-09 | 宁波原真生态纺织科技有限公司 | A kind of technique using some vegetable colours to carry out contaminating on colorant match |
-
2016
- 2016-12-01 CN CN201611089019.3A patent/CN106544894A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102634995A (en) * | 2012-04-20 | 2012-08-15 | 浙江理工大学 | Method for preparing silk fabric for cultural relic protection |
| CN103410017A (en) * | 2013-07-18 | 2013-11-27 | 祝洪哲 | Ecologic self-cleaning skin care fabric processed through using purely natural Chinese herbal medicinal plant dye |
| CN106087475A (en) * | 2016-08-19 | 2016-11-09 | 宁波原真生态纺织科技有限公司 | A kind of technique using some vegetable colours to carry out contaminating on colorant match |
Non-Patent Citations (2)
| Title |
|---|
| 宋心远等: "《活性染料染色的理论和实践》", 30 September 1991, 纺织工业出版社 * |
| 徐以俊 等: "《石油化工关联行业概览——精细化学品（一）》", 30 June 1992, 上海科学普及出版社 * |
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Application publication date: 20170329 |