CN106592271A - Method of using safflower red to dye wool fabric - Google Patents

Method of using safflower red to dye wool fabric Download PDF

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Publication number
CN106592271A
CN106592271A CN201611089850.9A CN201611089850A CN106592271A CN 106592271 A CN106592271 A CN 106592271A CN 201611089850 A CN201611089850 A CN 201611089850A CN 106592271 A CN106592271 A CN 106592271A
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CN
China
Prior art keywords
ethanol
safflower red
dyeing
wool fabric
red pigment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611089850.9A
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Chinese (zh)
Inventor
卢明
樊涛
李兰倩
刘萍
刘一萍
赵振云
周菁
胡睿敏
蒲青霞
董倩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611089850.9A priority Critical patent/CN106592271A/en
Publication of CN106592271A publication Critical patent/CN106592271A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/651—Compounds without nitrogen
    • D06P1/65106—Oxygen-containing compounds
    • D06P1/65125—Compounds containing ester groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02—Material containing basic nitrogen
    • D06P3/04—Material containing basic nitrogen containing amide groups
    • D06P3/14—Wool

Abstract

The invention provides a method of using safflower red to dye wool fabric. The method includes following steps: dissolving safflower red in an alcohol/phenol mixed solution, adding a surfactant-benzyl benzoate to ultrasonically obtain a transparent solution; putting the wool fabric into above dyeing liquid, and oscillating while heating to 30-60 DEG C for dyeing. By the method, modifying of safflower red is not needed, high-temperature dyeing is not adopted, and the fabric is high in color fastness after being dyed.

Description

The method of safflower red pigment dyeing wool fabric
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of safflower red pigment dyeing wool fabric Method.
Background technology
Safflower red pigment is that, with the petal of Flos Carthami as raw material, the natural pigment for extracting, kermesinus has to russet The crystallization of gloss or crystalline powder, it is water insoluble, can be used for food industry, cosmetics industry（Such as lipstick）, dyestuff.Flos Carthami is red In ancient times the Tang Dynasty is just widely used pigment.But safflower red pigment to the protein fibres such as Pilus Caprae seu Oviss directly upper dye compared with Difference, and color fastness is poor.
The content of the invention
In order that the effective dyeing wool fabric of safflower red pigment, the present invention is adopted the following technical scheme that.
A kind of method of safflower red pigment dyeing wool fabric, comprises the steps：（1）Phenol is dissolved in ethanol；（2） Safflower red pigment is dissolved in ethanol/phenol mixed solution, surfactant benzyl benzoate is added, is obtained under ultrasound Bright solution；（3）Wool fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；（4）Will Fabric is placed in ethanol and washs after dyeing, dries under 80 C.
Further, the ethanol of described ethanol/phenol mixed solution and the mass ratio of phenol are 1:0.1~3.
Further, described surfactant benzyl benzoate is 1 with the mass ratio of ethanol/phenol mixed solution: 2000~8000。
Further, described safflower red pigment and the mass ratio of ethanol/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention is, it is not necessary to safflower red pigment is modified, high-temperature dyeing is not adopted, after dyeing Fabric color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic is not construed as isolated, and they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
The method detailed step of safflower red pigment dyeing wool fabric is as follows：
（1）20g phenol is dissolved in 180g ethanol；
（2）1g safflower red pigments are dissolved in above-mentioned ethanol/phenol mixed solution, 0.04g surfactant benzene first is added Acid benzyl ester, under ultrasound clear solution is obtained；
（3）10g wool fabrics are put in above-mentioned dye liquor, vibration is heated to 60 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 2
The method detailed step of safflower red pigment dyeing wool fabric is as follows：
（1）300g phenol is dissolved in 100g ethanol；
（2）0.2g safflower red pigments are dissolved in above-mentioned ethanol/phenol mixed solution, 0.08g surfactant benzene is added Benzyl formate, under ultrasound clear solution is obtained；
（3）10g wool fabrics are put in above-mentioned dye liquor, vibration is heated to 30 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 3
The method detailed step of safflower red pigment dyeing wool fabric is as follows：
（1）50g phenol is dissolved in 250g ethanol；
（2）0.5g safflower red pigments are dissolved in above-mentioned ethanol/phenol mixed solution, 0.06g surfactant benzene is added Benzyl formate, under ultrasound clear solution is obtained；
（3）10g wool fabrics are put in above-mentioned dye liquor, vibration is heated to 50 C, insulation dyeing 10min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 4
The method detailed step of safflower red pigment dyeing wool fabric is as follows：
（1）200g phenol is dissolved in 200g ethanol；
（2）1g safflower red pigments are dissolved in above-mentioned ethanol/phenol mixed solution, 0.01g surfactant benzene first is added Acid benzyl ester, under ultrasound clear solution is obtained；
（3）10g wool fabrics are put in above-mentioned dye liquor, vibration is heated to 40 C, insulation dyeing 15min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. a kind of method of safflower red pigment dyeing wool fabric, it is characterised in that comprise the steps：
（1）Phenol is dissolved in ethanol；
（2）Safflower red pigment is dissolved in ethanol/phenol mixed solution, surfactant benzyl benzoate is added, ultrasound Under obtain clear solution；
（3）Wool fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
2. the method for safflower red pigment dyeing wool fabric as claimed in claim 1, described ethanol/phenol mixed solution Ethanol is 1 with the mass ratio of phenol:0.1~3.
3. the method for safflower red pigment dyeing wool fabric as claimed in claim 1, described surfactant Benzyl Benzoate Ester is 1 with the mass ratio of ethanol/phenol mixed solution:2000~8000.
4. the method for safflower red pigment dyeing wool fabric as claimed in claim 1, described safflower red pigment and ethanol/benzene The mass ratio of phenol mixed solution is 1:200~4000.
CN201611089850.9A 2016-12-01 2016-12-01 Method of using safflower red to dye wool fabric Pending CN106592271A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611089850.9A CN106592271A (en) 2016-12-01 2016-12-01 Method of using safflower red to dye wool fabric

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611089850.9A CN106592271A (en) 2016-12-01 2016-12-01 Method of using safflower red to dye wool fabric

Publications (1)

Publication Number Publication Date
CN106592271A true CN106592271A (en) 2017-04-26

Family

ID=58594626

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611089850.9A Pending CN106592271A (en) 2016-12-01 2016-12-01 Method of using safflower red to dye wool fabric

Country Status (1)

Country Link
CN (1) CN106592271A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112521769A (en) * 2020-11-25 2021-03-19 清华大学 Safflower red pigment and preparation method and dyeing method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102295839A (en) * 2011-06-29 2011-12-28 新疆奥斯曼生物资源有限公司 Preparation method of carhamus tincwrius L. haematochrome
CN106087476A (en) * 2016-08-19 2016-11-09 宁波原真生态纺织科技有限公司 Dyeing technique on a kind of colorant match based on vegetable colour
CN106149416A (en) * 2016-08-24 2016-11-23 常熟市新华源有色毛条厂 The colouring method of wool top

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102295839A (en) * 2011-06-29 2011-12-28 新疆奥斯曼生物资源有限公司 Preparation method of carhamus tincwrius L. haematochrome
CN106087476A (en) * 2016-08-19 2016-11-09 宁波原真生态纺织科技有限公司 Dyeing technique on a kind of colorant match based on vegetable colour
CN106149416A (en) * 2016-08-24 2016-11-23 常熟市新华源有色毛条厂 The colouring method of wool top

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
唐人成等: "《双组分纤维纺织品的染色》", 31 October 2003, 中国纺织出版社 *
赵学恒等: ""羊毛织物的藏红花、苏木红、红花素和咖啡色素的染色初探"", 《北京服装学院学报》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112521769A (en) * 2020-11-25 2021-03-19 清华大学 Safflower red pigment and preparation method and dyeing method thereof
CN112521769B (en) * 2020-11-25 2021-11-30 清华大学 Safflower red pigment and preparation method and dyeing method thereof

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Application publication date: 20170426