CN106702774A - Method for dyeing silk fabric by utilizing acetylshikonin - Google Patents
Method for dyeing silk fabric by utilizing acetylshikonin Download PDFInfo
- Publication number
- CN106702774A CN106702774A CN201611089896.0A CN201611089896A CN106702774A CN 106702774 A CN106702774 A CN 106702774A CN 201611089896 A CN201611089896 A CN 201611089896A CN 106702774 A CN106702774 A CN 106702774A
- Authority
- CN
- China
- Prior art keywords
- acetylshikonin
- ethanol
- dyeing
- silk fabric
- phenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
Abstract
The invention provides a method for dyeing a silk fabric by utilizing acetylshikonin. The method comprises the steps of dissolving acetylshikonin in an alcohol/phenol mixed solution, adding surfactant benzyl benzoate, and obtaining a transparent solution through ultrasonic treatment; placing the silk fabric in the dye liquid, and performing vibration heating to 30-60 DEG C to perform dyeing. According to the dyeing technology, acetylshikonin does not need to be modified, high temperature dyeing is not adopted, and the fabric is high in color fastness after being dyed.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of Acetylshikonin dyeing silk fabric
Method.
Background technology
Acetylshikonin is primarily present in Asian puccoon root also known as Acetyl-shikonin, is naphthalene Quinone Pigments, aubergine needle-like knot
It is brilliant.The hydrophobicity side switch of Acetylshikonin is long, therefore water-soluble poor, typically can be using the method for first mordant dyeing to cellulose
Fabric is dyeed.Being compatible with the environment property of Acetylshikonin is good, is harmful to human health.But Acetylshikonin is to silk
Deng protein fibre, directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that Acetylshikonin effectively dyes silk fabric, the present invention is adopted the following technical scheme that.
A kind of method that Acetylshikonin dyes silk fabric, comprises the following steps：（1）Phenol is dissolved in ethanol；（2）
Acetylshikonin is dissolved in ethanol/phenol mixed solution, surfactant Ergol is added, obtained under ultrasound
Bright solution；（3）During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；（4）Will
Fabric is placed in ethanol and washs after dyeing, is dried under 80oC.
Further, the ethanol of described ethanol/phenol mixed solution and the mass ratio of phenol are 1:0.1~3.
Further, described surfactant Ergol is 1 with the mass ratio of ethanol/phenol mixed solution:
2000~8000。
Further, described Acetylshikonin and the mass ratio of ethanol/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to Acetylshikonin is modified, high-temperature dyeing is not used, after dyeing
Fabric color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
The method detailed step of Acetylshikonin dyeing silk fabric is as follows：
（1）20g phenol is dissolved in 180g ethanol；
（2）1g Acetylshikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.04g surfactant benzene first is added
Acid benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 2
The method detailed step of Acetylshikonin dyeing silk fabric is as follows：
（1）300g phenol is dissolved in 100g ethanol；
（2）0.1g Acetylshikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.08g surfactant benzene is added
Benzyl formate, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 3
The method detailed step of Acetylshikonin dyeing silk fabric is as follows：
（1）50g phenol is dissolved in 250g ethanol；
（2）1g Acetylshikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.06g surfactant benzene first is added
Acid benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 4
The method detailed step of Acetylshikonin dyeing silk fabric is as follows：
（1）200g phenol is dissolved in 200g ethanol；
（2）0.7g Acetylshikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.01g surfactant benzene is added
Benzyl formate, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. a kind of method that Acetylshikonin dyes silk fabric, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in ethanol；
（2）Acetylshikonin is dissolved in ethanol/phenol mixed solution, surfactant Ergol is added, ultrasound
Under obtain clear solution；
（3）During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
2. the method that Acetylshikonin as claimed in claim 1 dyes silk fabric, described ethanol/phenol mixed solution
Ethanol is 1 with the mass ratio of phenol:0.1~3.
3. the method that Acetylshikonin as claimed in claim 1 dyes silk fabric, described surfactant Benzyl Benzoate
Ester is 1 with the mass ratio of ethanol/phenol mixed solution:2000~8000.
4. the method that Acetylshikonin as claimed in claim 1 dyes silk fabric, described Acetylshikonin and ethanol/benzene
The mass ratio of phenol mixed solution is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089896.0A CN106702774A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing silk fabric by utilizing acetylshikonin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089896.0A CN106702774A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing silk fabric by utilizing acetylshikonin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106702774A true CN106702774A (en) | 2017-05-24 |
Family
ID=58934448
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611089896.0A Pending CN106702774A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing silk fabric by utilizing acetylshikonin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106702774A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101666044A (en) * | 2008-09-03 | 2010-03-10 | 上海市长宁区少年科技指导站 | Application of alkannin serving as dye |
| CN103174041A (en) * | 2013-04-12 | 2013-06-26 | 祝洪哲 | Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye |
| CN103215831A (en) * | 2013-04-19 | 2013-07-24 | 江阴职业技术学院 | Polyester/sorona mixed fabric disperse dye one-bath process dyeing method |
| CN105648799A (en) * | 2016-01-25 | 2016-06-08 | 苏州印丝特纺织数码科技有限公司 | Neutral leveling agent for dyeing wool fiber with acid dye |
-
2016
- 2016-12-01 CN CN201611089896.0A patent/CN106702774A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101666044A (en) * | 2008-09-03 | 2010-03-10 | 上海市长宁区少年科技指导站 | Application of alkannin serving as dye |
| CN103174041A (en) * | 2013-04-12 | 2013-06-26 | 祝洪哲 | Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye |
| CN103215831A (en) * | 2013-04-19 | 2013-07-24 | 江阴职业技术学院 | Polyester/sorona mixed fabric disperse dye one-bath process dyeing method |
| CN105648799A (en) * | 2016-01-25 | 2016-06-08 | 苏州印丝特纺织数码科技有限公司 | Neutral leveling agent for dyeing wool fiber with acid dye |
Non-Patent Citations (2)
| Title |
|---|
| 姜颖: "《山东丝绸》", 31 December 2013, 齐鲁书社 * |
| 范洪琼等: "《基础化学》", 31 August 2015, 重庆大学出版社 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106702774A (en) | Method for dyeing silk fabric by utilizing acetylshikonin | |
| CN106592271A (en) | Method of using safflower red to dye wool fabric | |
| CN106758335A (en) | Colouring method of the Acetylshikonin to wool fabric | |
| CN106758363A (en) | The method of Acetylshikonin dyeing wool fabric | |
| CN106758334A (en) | The method of Acetylshikonin dyed cotton fabric | |
| CN106758354A (en) | The method of shikonin dyed cotton fabric | |
| CN106702775A (en) | Method for dyeing polyester fabric through alizarin | |
| CN106758355A (en) | The method of Acetylshikonin dyed polyester textiles | |
| CN106544899A (en) | The method that shikonin dyes silk fabric | |
| CN106702772A (en) | Method for dyeing silk fabric with rutin | |
| CN106638052A (en) | Method for dyeing cotton fabric with rutamine | |
| CN106702770A (en) | Dyeing method of shikonin on polyester fabric | |
| CN106758347A (en) | Colouring method of the Acetylshikonin to silk fabric | |
| CN106544897A (en) | The method of shikonin dyeing wool fabric | |
| CN106702773A (en) | Method for dyeing wool fabric with gardenin | |
| CN106702769A (en) | Method for dyeing silk fabrics with gardenin | |
| CN106758339A (en) | The method of shikonin dyed polyester textiles | |
| CN106638029A (en) | Method for dyeing cotton fabric through acetyl shikonin | |
| CN106544898A (en) | The method that alizarin dyes silk fabric | |
| CN106758353A (en) | Colouring method of the gardenin to wool fabric | |
| CN106702771A (en) | Method for dyeing polyester textile by rutamine | |
| CN106638050A (en) | Method for dyeing silk fabric with shikonin | |
| CN106758342A (en) | The method of alizarin dyeing wool fabric | |
| CN106702768A (en) | Method for dyeing silk fabric by using curcumin | |
| CN106758343A (en) | The method that safflower red pigment dyes silk fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170524 |