CN106702769A - Method for dyeing silk fabrics with gardenin - Google Patents
Method for dyeing silk fabrics with gardenin Download PDFInfo
- Publication number
- CN106702769A CN106702769A CN201611088960.3A CN201611088960A CN106702769A CN 106702769 A CN106702769 A CN 106702769A CN 201611088960 A CN201611088960 A CN 201611088960A CN 106702769 A CN106702769 A CN 106702769A
- Authority
- CN
- China
- Prior art keywords
- gardenin
- ethanol
- dyeing
- phenol
- silk fabric
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
Abstract
The invention provides a method for dyeing silk fabrics with gardenin. The method includes the following steps: gardenin is dissolved in an ethanol/phenol mixed solution, a surfactant benzyl benzoate is then added, and a transparent solution is ultrasonically obtained; and a silk fabric is put into the dye solution, and is oscillated and heated to 30 DEG C to 60 DEG C for dyeing. The dyeing technique does not require the modification of gardenin, and does not adopt high-temperature dyeing, and the color fastness of the dyed fabric is high.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of gardenin dyes the side of silk fabric
Method.
Background technology
Gardenin is a kind of natural pigment extracted from madder wort cape jasmine, is flavone compound.Gardenin can
The depth yellow for obtaining different tones is dyeed with different mordant dyeing agent.Gardenin yellow plant dye most widely used since being Qin Han
Material.But gardenin is to protein fibres such as silks, and directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that gardenin effectively dyes silk fabric, the present invention is adopted the following technical scheme that.
A kind of method that gardenin dyes silk fabric, comprises the following steps：（1）Phenol is dissolved in ethanol；（2）By Cape jasmine
Sub- element is dissolved in ethanol/phenol mixed solution, adds surfactant Ergol, and clear solution is obtained under ultrasound；
（3）During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；（4）To be knitted after dyeing
Thing is placed in ethanol and washs, and is dried under 80oC.
Further, the ethanol of described ethanol/phenol mixed solution and the mass ratio of phenol are 1:0.1~3.
Further, described surfactant Ergol is 1 with the mass ratio of ethanol/phenol mixed solution:
2000~8000。
Further, described gardenin and the mass ratio of ethanol/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to gardenin is modified, high-temperature dyeing is not used, fabric after dyeing
Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
The method detailed step of gardenin dyeing silk fabric is as follows：
（1）20g phenol is dissolved in 180g ethanol；
（2）0.1g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.04g surfactant benzoic acid is added
Benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 2
The method detailed step of gardenin dyeing silk fabric is as follows：
（1）300g phenol is dissolved in 100g ethanol；
（2）1g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.08g surfactant Benzyl Benzoates are added
Ester, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 3
The method detailed step of gardenin dyeing silk fabric is as follows：
（1）50g phenol is dissolved in 250g ethanol；
（2）0.2g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.06g surfactant benzoic acid is added
Benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 4
The method detailed step of gardenin dyeing silk fabric is as follows：
（1）200g phenol is dissolved in 200g ethanol；
（2）0.6g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.01g surfactant benzoic acid is added
Benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. a kind of method that gardenin dyes silk fabric, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in ethanol；
（2）Gardenin is dissolved in ethanol/phenol mixed solution, surfactant Ergol is added, under ultrasound
To clear solution；
（3）During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
2. the method that gardenin as claimed in claim 1 dyes silk fabric, the ethanol of described ethanol/phenol mixed solution
It is 1 with the mass ratio of phenol:0.1~3.
3. the method that gardenin as claimed in claim 1 dyes silk fabric, described surfactant Ergol with
The mass ratio of ethanol/phenol mixed solution is 1:2000~8000.
4. the method that gardenin as claimed in claim 1 dyes silk fabric, described gardenin mixes molten with ethanol/phenol
The mass ratio of liquid is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611088960.3A CN106702769A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing silk fabrics with gardenin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611088960.3A CN106702769A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing silk fabrics with gardenin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106702769A true CN106702769A (en) | 2017-05-24 |
Family
ID=58934385
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611088960.3A Pending CN106702769A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing silk fabrics with gardenin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106702769A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101148827A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing silk face fabric by vegetable dye |
| CN103741505A (en) * | 2013-12-20 | 2014-04-23 | 大连创达技术交易市场有限公司 | Silk dyeing process adopting gardenia yellow vegetable dye |
| CN104233862A (en) * | 2013-06-17 | 2014-12-24 | 无锡市东新织造有限公司 | Process for aluminum salt pre-mordanting and after-dyeing for real silk fabric by using henna pigment |
| CN105297493A (en) * | 2015-11-30 | 2016-02-03 | 无锡新德印染制品有限公司 | Method for dyeing real silk fabric by adopting natural dyestuff |
-
2016
- 2016-12-01 CN CN201611088960.3A patent/CN106702769A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101148827A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing silk face fabric by vegetable dye |
| CN104233862A (en) * | 2013-06-17 | 2014-12-24 | 无锡市东新织造有限公司 | Process for aluminum salt pre-mordanting and after-dyeing for real silk fabric by using henna pigment |
| CN103741505A (en) * | 2013-12-20 | 2014-04-23 | 大连创达技术交易市场有限公司 | Silk dyeing process adopting gardenia yellow vegetable dye |
| CN105297493A (en) * | 2015-11-30 | 2016-02-03 | 无锡新德印染制品有限公司 | Method for dyeing real silk fabric by adopting natural dyestuff |
Non-Patent Citations (1)
| Title |
|---|
| 唐人成等: "《双组分纤维纺织品的染色》", 31 October 2003, 中国纺织出版社 * |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170524 |