CN106638052A - Method for dyeing cotton fabric with rutamine - Google Patents
Method for dyeing cotton fabric with rutamine Download PDFInfo
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- CN106638052A CN106638052A CN201611089431.5A CN201611089431A CN106638052A CN 106638052 A CN106638052 A CN 106638052A CN 201611089431 A CN201611089431 A CN 201611089431A CN 106638052 A CN106638052 A CN 106638052A
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- Prior art keywords
- ethanol
- dyeing
- cotton fabric
- phenol
- sophoraxanthin
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- 239000004744 fabric Substances 0.000 title claims abstract description 27
- 229920000742 Cotton Polymers 0.000 title claims abstract description 20
- 238000004043 dyeing Methods 0.000 title claims abstract description 20
- 238000000034 method Methods 0.000 title claims abstract description 14
- COBBNRKBTCBWQP-UHFFFAOYSA-N Graveoline Chemical compound C1=C2OCOC2=CC(C=2N(C3=CC=CC=C3C(=O)C=2)C)=C1 COBBNRKBTCBWQP-UHFFFAOYSA-N 0.000 title 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 53
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000000243 solution Substances 0.000 claims abstract description 14
- 239000011259 mixed solution Substances 0.000 claims abstract description 13
- 239000004094 surface-active agent Substances 0.000 claims abstract description 9
- 238000002604 ultrasonography Methods 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims 1
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 abstract description 14
- 229960002903 benzyl benzoate Drugs 0.000 abstract description 7
- IKGXIBQEEMLURG-UHFFFAOYSA-N Rutin Chemical compound OC1C(O)C(O)C(C)OC1OCC1C(O)C(O)C(O)C(OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 IKGXIBQEEMLURG-UHFFFAOYSA-N 0.000 abstract description 2
- 238000002525 ultrasonication Methods 0.000 abstract 1
- 239000000975 dye Substances 0.000 description 4
- QCHFTSOMWOSFHM-WPRPVWTQSA-N (+)-Pilocarpine Chemical compound C1OC(=O)[C@@H](CC)[C@H]1CC1=CN=CN1C QCHFTSOMWOSFHM-WPRPVWTQSA-N 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- QCHFTSOMWOSFHM-UHFFFAOYSA-N SJ000285536 Natural products C1OC(=O)C(CC)C1CC1=CN=CN1C QCHFTSOMWOSFHM-UHFFFAOYSA-N 0.000 description 1
- 244000046101 Sophora japonica Species 0.000 description 1
- 235000010586 Sophora japonica Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009967 direct dyeing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002214 flavonoid derivatives Chemical class 0.000 description 1
- AJDUTMFFZHIJEM-UHFFFAOYSA-N n-(9,10-dioxoanthracen-1-yl)-4-[4-[[4-[4-[(9,10-dioxoanthracen-1-yl)carbamoyl]phenyl]phenyl]diazenyl]phenyl]benzamide Chemical group O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2NC(=O)C(C=C1)=CC=C1C(C=C1)=CC=C1N=NC(C=C1)=CC=C1C(C=C1)=CC=C1C(=O)NC1=CC=CC2=C1C(=O)C1=CC=CC=C1C2=O AJDUTMFFZHIJEM-UHFFFAOYSA-N 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229960001416 pilocarpine Drugs 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000001043 yellow dye Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
本发明提供了一种槐黄素染色棉织物的方法，该方法包括如下步骤：将槐黄素溶解于乙醇/苯酚混合溶液中，再加入表面活性剂苯甲酸苄酯，超声下得到透明溶液；将棉织物投入到上述染液中，振荡加热至30~60ºC染色。本染色技术不需要对槐黄素进行改性，不采用高温染色，染色后织物色牢度高。The invention provides a method for dyeing cotton fabric with sophoraxanthin. The method comprises the following steps: dissolving sophoraxanthin in an ethanol/phenol mixed solution, adding a surfactant benzyl benzoate, and obtaining a transparent solution under ultrasonication; Put the cotton fabric into the above dyeing solution, vibrate and heat to 30~60ºC for dyeing. This dyeing technology does not need to modify sophorin, does not use high temperature dyeing, and the color fastness of the dyed fabric is high.
Description
技术领域technical field
本发明涉及一种纺织品染色技术领域，具体涉及一种槐黄素染色棉织物的方法。The invention relates to the technical field of textile dyeing, in particular to a method for dyeing cotton fabrics with sophoraxanthin.
背景技术Background technique
槐花中的色素成分为芸香碱，又名槐黄素。槐黄素属黄酮类衍生物。槐黄素难不溶于水，是色彩鲜亮、牢度优良的黄色染料，与环境相容性好，对人体健康无害。但是槐黄素对棉等纤维素纤维直接上染较差，且色牢度较差。The pigment component in Sophora japonica is pilocarpine, also known as sophoraxanthin. Sophoraxanthin is a flavonoid derivative. Sophoraxanthin is hardly insoluble in water. It is a yellow dye with bright color and excellent fastness. It has good compatibility with the environment and is harmless to human health. However, sophoraxanthin is poor in direct dyeing of cellulose fibers such as cotton, and its color fastness is poor.
发明内容Contents of the invention
为了使槐黄素有效染色棉织物，本发明采取如下技术方案。In order to make sophorin effectively dye cotton fabrics, the present invention takes the following technical solutions.
一种槐黄素染色棉织物的方法，包括如下步骤：（1）将苯酚溶于乙醇中；（2）将槐黄素溶解于乙醇/苯酚混合溶液中，再加入表面活性剂苯甲酸苄酯，超声下得到透明溶液；（3）将棉织物投入到上述染液中，振荡加热至30~60ºC，保温染色5~30min；（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。A method for dyeing cotton fabric with sophoraxanthin, comprising the steps of: (1) dissolving phenol in ethanol; (2) dissolving sophoraxanthin in a mixed solution of ethanol/phenol, and then adding surfactant benzyl benzoate , to obtain a transparent solution under ultrasonic; (3) Put the cotton fabric into the above dyeing solution, oscillate and heat to 30~60ºC, and keep it warm for 5~30min; (4) Wash the dyed fabric in ethanol and dry it at 80ºC .
进一步的，所述的乙醇/苯酚混合溶液的乙醇与苯酚的质量比为1:0.1~3。Further, the mass ratio of ethanol to phenol in the ethanol/phenol mixed solution is 1:0.1~3.
进一步的，所述的表面活性剂苯甲酸苄酯与乙醇/苯酚混合溶液的质量比为1:2000~8000。Further, the mass ratio of the surfactant benzyl benzoate to the ethanol/phenol mixed solution is 1:2000-8000.
进一步的，所述的槐黄素与乙醇/苯酚混合溶液的质量比为1:200~4000。Further, the mass ratio of sophoraxanthin to ethanol/phenol mixed solution is 1:200~4000.
本发明的有益效果在于，不需要对槐黄素进行改性，不采用高温染色，染色后织物色牢度高。The beneficial effect of the invention is that it does not need to modify the sophoraxanthin, does not use high temperature dyeing, and the color fastness of the dyed fabric is high.
具体实施方式detailed description
下文将结合具体实施例详细描述本发明。应当注意的是，下述实施例中描述的技术特征或者技术特征的组合不应当被认为是孤立的，它们可以被相互组合从而达到更好的技术效果。The present invention will be described in detail below in conjunction with specific embodiments. It should be noted that the technical features or combinations of technical features described in the following embodiments should not be regarded as isolated, and they can be combined with each other to achieve better technical effects.
实施例1Example 1
槐黄素染色棉织物的方法详细步骤如下：The detailed steps of the method for dyeing cotton fabric with sophoraxanthin are as follows:
（1）将20g苯酚溶于180g乙醇中；(1) Dissolve 20g of phenol in 180g of ethanol;
（2）将1g槐黄素溶解于上述乙醇/苯酚混合溶液中，再加入0.04g表面活性剂苯甲酸苄酯，超声下得到透明溶液；(2) Dissolve 1g of sophoraxanthin in the above ethanol/phenol mixed solution, then add 0.04g of surfactant benzyl benzoate, and obtain a transparent solution under ultrasound;
（3）将10g棉织物投入到上述染液中，振荡加热至60ºC，保温染色30min；(3) Put 10g of cotton fabric into the above dyeing solution, vibrate and heat to 60ºC, keep warm and dye for 30min;
（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。(4) Wash the dyed fabric in ethanol and dry at 80ºC.
实施例2Example 2
槐黄素染色棉织物的方法详细步骤如下：The detailed steps of the method for dyeing cotton fabric with sophoraxanthin are as follows:
（1）将300g苯酚溶于100g乙醇中；(1) Dissolve 300g phenol in 100g ethanol;
（2）将0.8g槐黄素溶解于上述乙醇/苯酚混合溶液中，再加入0.08g表面活性剂苯甲酸苄酯，超声下得到透明溶液；(2) Dissolve 0.8g sophoraxanthin in the above ethanol/phenol mixed solution, then add 0.08g surfactant benzyl benzoate, and obtain a transparent solution under ultrasound;
（3）将10g棉织物投入到上述染液中，振荡加热至30ºC，保温染色30min；(3) Put 10g of cotton fabric into the above dyeing solution, vibrate and heat to 30ºC, keep warm and dye for 30min;
（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。(4) Wash the dyed fabric in ethanol and dry at 80ºC.
实施例3Example 3
槐黄素染色棉织物的方法详细步骤如下：The detailed steps of the method for dyeing cotton fabric with sophoraxanthin are as follows:
（1）将50g苯酚溶于250g乙醇中；(1) Dissolve 50g of phenol in 250g of ethanol;
（2）将0.1g槐黄素溶解于上述乙醇/苯酚混合溶液中，再加入0.06g表面活性剂苯甲酸苄酯，超声下得到透明溶液；(2) Dissolve 0.1g sophoraxanthin in the above ethanol/phenol mixed solution, then add 0.06g surfactant benzyl benzoate, and obtain a transparent solution under ultrasound;
（3）将10g棉织物投入到上述染液中，振荡加热至50ºC，保温染色10min；(3) Put 10g of cotton fabric into the above dye solution, vibrate and heat to 50ºC, and keep warm for 10min;
（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。(4) Wash the dyed fabric in ethanol and dry at 80ºC.
实施例4Example 4
槐黄素染色棉织物的方法详细步骤如下：The detailed steps of the method for dyeing cotton fabric with sophoraxanthin are as follows:
（1）将200g苯酚溶于200g乙醇中；(1) Dissolve 200g phenol in 200g ethanol;
（2）将0.4g槐黄素溶解于上述乙醇/苯酚混合溶液中，再加入0.01g表面活性剂苯甲酸苄酯，超声下得到透明溶液；(2) Dissolve 0.4g sophoraxanthin in the above ethanol/phenol mixed solution, then add 0.01g surfactant benzyl benzoate, and obtain a transparent solution under ultrasound;
（3）将10g棉织物投入到上述染液中，振荡加热至40ºC，保温染色15min；(3) Put 10g of cotton fabric into the above dyeing solution, vibrate and heat to 40ºC, and keep it warm for 15 minutes;
（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。(4) Wash the dyed fabric in ethanol and dry at 80ºC.
本文虽然已经给出了本发明的一些实施例，但是本领域的技术人员应当理解，在不脱离本发明精神的情况下，可以对本文的实施例进行改变。上述实施例只是示例性的，不应以本文的实施例作为本发明权利范围的限定。Although some embodiments of the present invention have been given herein, those skilled in the art should understand that the embodiments herein can be changed without departing from the spirit of the present invention. The above-mentioned embodiments are only exemplary, and the embodiments herein should not be used as limitations on the scope of rights of the present invention.
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Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089431.5A CN106638052A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing cotton fabric with rutamine |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089431.5A CN106638052A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing cotton fabric with rutamine |
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| Publication Number | Publication Date |
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| CN106638052A true CN106638052A (en) | 2017-05-10 |
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| CN201611089431.5A Pending CN106638052A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing cotton fabric with rutamine |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1966585A (en) * | 2006-11-27 | 2007-05-23 | 江南大学 | Method of extracting and preparing yellow pigment of pagodatree flower |
| CN101148826A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing purified cotton yarn by vegetable dye |
| CN105086508A (en) * | 2015-10-08 | 2015-11-25 | 嘉兴市欣纺纺织品有限公司 | Sophora japonica plant dye extraction method and dyeing method through dye |
-
2016
- 2016-12-01 CN CN201611089431.5A patent/CN106638052A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1966585A (en) * | 2006-11-27 | 2007-05-23 | 江南大学 | Method of extracting and preparing yellow pigment of pagodatree flower |
| CN101148826A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing purified cotton yarn by vegetable dye |
| CN105086508A (en) * | 2015-10-08 | 2015-11-25 | 嘉兴市欣纺纺织品有限公司 | Sophora japonica plant dye extraction method and dyeing method through dye |
Non-Patent Citations (3)
| Title |
|---|
| 巩梦婷: "古文献修复中染色配纸的研究", 《中国优秀硕士学位论文全文数据库信息科技辑》 * |
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