CN106758344A - Colouring method of the shikonin to wool fabric - Google Patents
Colouring method of the shikonin to wool fabric Download PDFInfo
- Publication number
- CN106758344A CN106758344A CN201611089031.4A CN201611089031A CN106758344A CN 106758344 A CN106758344 A CN 106758344A CN 201611089031 A CN201611089031 A CN 201611089031A CN 106758344 A CN106758344 A CN 106758344A
- Authority
- CN
- China
- Prior art keywords
- shikonin
- carbon tetrachloride
- wool fabric
- dyeing
- phenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The invention provides a kind of shikonin to the colouring method of wool fabric, the method comprises the following steps：Shikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound；During wool fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to shikonin, not use high-temperature dyeing, and fabric color fastness is high after dyeing.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing side of shikonin to wool fabric
Method.
Background technology
Shikonin, is primarily present in Asian puccoon root, is naphthoquinone derivatives, shiny red acicular crystal.The hydrophobicity of shikonin
Side switch is long, therefore water-soluble poor, cellulose base fiber fabric can typically be dyeed using the method for first mordant dyeing.Asian puccoon
Being compatible with the environment property of quinone is good, is harmful to human health.But shikonin is to protein fibres such as wools, and directly upper dye is poor, and color
Fastness is poor.
The content of the invention
In order that the effective dyeing wool fabric of shikonin, the present invention is adopted the following technical scheme that.
A kind of shikonin comprises the following steps to the colouring method of wool fabric：（1）Phenol is dissolved in carbon tetrachloride；
（2）Shikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, surpassed
Clear solution is obtained under sound；（3）During wool fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, and insulation dyeing 5 ~
30min；（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~
3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and the matter of carbon tetrachloride/phenol mixed solution
Amount is than being 1:2000~8000.
Further, described shikonin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to shikonin is modified, high-temperature dyeing is not used, fabric after dyeing
Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
Shikonin is as follows to the colouring method detailed step of wool fabric：
（1）20g phenol is dissolved in 180g carbon tetrachloride；
（2）1g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants 12 are added
Sodium alkyl benzene sulfonate, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 2
Shikonin is as follows to the colouring method detailed step of wool fabric：
（1）300g phenol is dissolved in 100g carbon tetrachloride；
（2）0.1g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 3
Shikonin is as follows to the colouring method detailed step of wool fabric：
（1）50g phenol is dissolved in 250g carbon tetrachloride；
（2）0.6g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 4
Shikonin is as follows to the colouring method detailed step of wool fabric：
（1）200g phenol is dissolved in 200g carbon tetrachloride；
（2）0.8g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. colouring method of a kind of shikonin to wool fabric, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in carbon tetrachloride；
（2）Shikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid is added
Sodium, clear solution is obtained under ultrasound；
（3）During wool fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
2. shikonin as claimed in claim 1 is to the colouring method of wool fabric, described carbon tetrachloride/phenol mixed solution
The mass ratio of carbon tetrachloride and phenol be 1:0.1~3.
3. shikonin as claimed in claim 1 is to the colouring method of wool fabric, described surfactant sodium dodecyl base benzene
Sodium sulfonate is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. shikonin as claimed in claim 1 is to the colouring method of wool fabric, described shikonin and carbon tetrachloride/phenol
The mass ratio of mixed solution is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089031.4A CN106758344A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the shikonin to wool fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089031.4A CN106758344A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the shikonin to wool fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106758344A true CN106758344A (en) | 2017-05-31 |
Family
ID=58915350
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611089031.4A Pending CN106758344A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the shikonin to wool fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106758344A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104088167A (en) * | 2014-07-04 | 2014-10-08 | 常州大学 | Method for improving color depth and light fastness of natural dye-dyed fabric |
| CN105040472A (en) * | 2015-06-17 | 2015-11-11 | 大连工业大学 | Clothing dyed by medicinal plants with health efficacy and fabrication method |
| CN105768256A (en) * | 2014-12-19 | 2016-07-20 | 常熟市润发服饰有限公司 | Anti-microbial wear-proof woolen sweater |
| CN105908530A (en) * | 2016-05-18 | 2016-08-31 | 江苏阳光股份有限公司 | One-bath dyeing process for wool Sorna fabric |
| CN105970672A (en) * | 2016-05-18 | 2016-09-28 | 江苏阳光股份有限公司 | Process for dyeing wool-cotton worsted fabric with vegetable dye |
-
2016
- 2016-12-01 CN CN201611089031.4A patent/CN106758344A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104088167A (en) * | 2014-07-04 | 2014-10-08 | 常州大学 | Method for improving color depth and light fastness of natural dye-dyed fabric |
| CN105768256A (en) * | 2014-12-19 | 2016-07-20 | 常熟市润发服饰有限公司 | Anti-microbial wear-proof woolen sweater |
| CN105040472A (en) * | 2015-06-17 | 2015-11-11 | 大连工业大学 | Clothing dyed by medicinal plants with health efficacy and fabrication method |
| CN105908530A (en) * | 2016-05-18 | 2016-08-31 | 江苏阳光股份有限公司 | One-bath dyeing process for wool Sorna fabric |
| CN105970672A (en) * | 2016-05-18 | 2016-09-28 | 江苏阳光股份有限公司 | Process for dyeing wool-cotton worsted fabric with vegetable dye |
Non-Patent Citations (2)
| Title |
|---|
| 何瑾馨: "《染料化学第2版》", 31 October 2016, 中国纺织出版社 * |
| 余志成等: "《紫草色素的稳定性及在羊毛上的染色性能》", 《毛纺科技》 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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Application publication date: 20170531 |