CN106544899A - The method that shikonin dyes silk fabric - Google Patents

The method that shikonin dyes silk fabric Download PDF

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Publication number
CN106544899A
CN106544899A CN201611089775.6A CN201611089775A CN106544899A CN 106544899 A CN106544899 A CN 106544899A CN 201611089775 A CN201611089775 A CN 201611089775A CN 106544899 A CN106544899 A CN 106544899A
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CN
China
Prior art keywords
shikonin
ethanol
dyeing
silk fabric
phenol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611089775.6A
Other languages
Chinese (zh)
Inventor
卢明
周菁
胡睿敏
刘萍
刘一萍
李兰倩
樊涛
赵振云
蒲青霞
董倩
刘欣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611089775.6A priority Critical patent/CN106544899A/en
Publication of CN106544899A publication Critical patent/CN106544899A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/651—Compounds without nitrogen
    • D06P1/65106—Oxygen-containing compounds
    • D06P1/65125—Compounds containing ester groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02—Material containing basic nitrogen
    • D06P3/04—Material containing basic nitrogen containing amide groups

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention provides a kind of method that shikonin dyes silk fabric, the method comprises the steps：Shikonin is dissolved in ethanol/phenol mixed solution, surfactant benzyl benzoate is added, under ultrasound, is obtained clear solution；Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C dyeing.This staining technique need not be modified to shikonin, do not adopt high-temperature dyeing, and after dyeing, fabric color fastness is high.

Description

The method that shikonin dyes silk fabric
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of shikonin dyes the side of silk fabric Method.
Background technology
Shikonin, is primarily present in Radix Arnebiae (Radix Lithospermi) root, is naphthoquinone derivatives, shiny red acicular crystal.The hydrophobicity of shikonin Side switch is long, therefore water solublity is poor, can typically adopt the method for first mordant dyeing to dye cellulose base fiber fabric.Radix Arnebiae (Radix Lithospermi) Being compatible with the environment property of quinone is good, is harmful to human health.But shikonin is to protein fibres such as silks, and directly upper dye is poor, and color Fastness is poor.
The content of the invention
In order that shikonin effectively dyes silk fabric, the present invention is adopted the following technical scheme that.
A kind of method that shikonin dyes silk fabric, comprises the steps：（1）Phenol is dissolved in ethanol；（2）By purple Careless quinone is dissolved in ethanol/phenol mixed solution, is added surfactant benzyl benzoate, is obtained clear solution under ultrasound； （3）Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；（4）To knit after dyeing Thing is placed in ethanol and washs, and dries under 80 C.
Further, the ethanol of described ethanol/phenol mixed solution and the mass ratio of phenol are 1:0.1~3.
Further, described surfactant benzyl benzoate is 1 with the mass ratio of ethanol/phenol mixed solution: 2000~8000。
Further, described shikonin and the mass ratio of ethanol/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention is, it is not necessary to shikonin is modified, high-temperature dyeing is not adopted, fabric after dyeing Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic is not construed as isolated, and they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
The method detailed step of shikonin dyeing silk fabric is as follows：
（1）20g phenol is dissolved in 180g ethanol；
（2）1g shikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.04g surfactant Benzyl Benzoates are added Ester, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 60 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 2
The method detailed step of shikonin dyeing silk fabric is as follows：
（1）300g phenol is dissolved in 100g ethanol；
（2）0.1g shikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.08g surfactant benzoic acid is added Benzyl ester, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 30 C, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 3
The method detailed step of shikonin dyeing silk fabric is as follows：
（1）50g phenol is dissolved in 250g ethanol；
（2）0.6g shikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.06g surfactant benzoic acid is added Benzyl ester, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 50 C, insulation dyeing 10min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Embodiment 4
The method detailed step of shikonin dyeing silk fabric is as follows：
（1）200g phenol is dissolved in 200g ethanol；
（2）0.8g shikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.01g surfactant benzoic acid is added Benzyl ester, obtains clear solution under ultrasound；
（3）10g silk fabrics are put in above-mentioned dye liquor, vibration is heated to 40 C, insulation dyeing 15min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. a kind of method that shikonin dyes silk fabric, it is characterised in that comprise the steps：
（1）Phenol is dissolved in ethanol；
（2）Shikonin is dissolved in ethanol/phenol mixed solution, surfactant benzyl benzoate is added, under ultrasound To clear solution；
（3）Silk fabric is put in above-mentioned dye liquor, vibration is heated to 30 ~ 60 C, insulation 5 ~ 30min of dyeing；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80 C.
2. the method that shikonin as claimed in claim 1 dyes silk fabric, the ethanol of described ethanol/phenol mixed solution Mass ratio with phenol is 1:0.1~3.
3. the method that shikonin as claimed in claim 1 dyes silk fabric, described surfactant benzyl benzoate with The mass ratio of ethanol/phenol mixed solution is 1:2000~8000.
4. the method that shikonin as claimed in claim 1 dyes silk fabric, described shikonin mix molten with ethanol/phenol The mass ratio of liquid is 1:200~4000.
CN201611089775.6A 2016-12-01 2016-12-01 The method that shikonin dyes silk fabric Pending CN106544899A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611089775.6A CN106544899A (en) 2016-12-01 2016-12-01 The method that shikonin dyes silk fabric

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611089775.6A CN106544899A (en) 2016-12-01 2016-12-01 The method that shikonin dyes silk fabric

Publications (1)

Publication Number Publication Date
CN106544899A true CN106544899A (en) 2017-03-29

Family

ID=58396035

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611089775.6A Pending CN106544899A (en) 2016-12-01 2016-12-01 The method that shikonin dyes silk fabric

Country Status (1)

Country Link
CN (1) CN106544899A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002138024A (en) * 2000-10-27 2002-05-14 Riaru Kagaku Kk Hair dyeing agent, hair dyeing set and hair dyeing method using the same
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN103410017A (en) * 2013-07-18 2013-11-27 祝洪哲 Ecologic self-cleaning skin care fabric processed through using purely natural Chinese herbal medicinal plant dye
CN105256604A (en) * 2015-08-20 2016-01-20 杨白华 Method for dyeing textile by using traditional Chinese medicine
CN105780527A (en) * 2014-12-22 2016-07-20 常熟市虹桥印染有限公司 Dye liquor for printing and dyeing of flocked cloth

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002138024A (en) * 2000-10-27 2002-05-14 Riaru Kagaku Kk Hair dyeing agent, hair dyeing set and hair dyeing method using the same
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN103410017A (en) * 2013-07-18 2013-11-27 祝洪哲 Ecologic self-cleaning skin care fabric processed through using purely natural Chinese herbal medicinal plant dye
CN105780527A (en) * 2014-12-22 2016-07-20 常熟市虹桥印染有限公司 Dye liquor for printing and dyeing of flocked cloth
CN105256604A (en) * 2015-08-20 2016-01-20 杨白华 Method for dyeing textile by using traditional Chinese medicine

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
唐人成等: "《双组分纤维纺织品的染色》", 31 October 2003, 中国纺织出版社 *

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Application publication date: 20170329