CN106702770A - Dyeing method of shikonin on polyester fabric - Google Patents
Dyeing method of shikonin on polyester fabric Download PDFInfo
- Publication number
- CN106702770A CN106702770A CN201611089399.0A CN201611089399A CN106702770A CN 106702770 A CN106702770 A CN 106702770A CN 201611089399 A CN201611089399 A CN 201611089399A CN 106702770 A CN106702770 A CN 106702770A
- Authority
- CN
- China
- Prior art keywords
- shikonin
- carbon tetrachloride
- dyeing
- phenol
- dacron
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The invention provides a dyeing method of shikonin on a polyester fabric. The method includes the steps of: dissolving shikonin in a carbon tetrachloride/phenol mixed solution, then adding a surfactant sodium dodecyl benzene sulfonate, and performing ultrasonic treatment to obtain a transparent solution; putting the polyester fabric into the dye solution, and performing oscillation heating to 30-60DEG C to conduct dyeing. The dyeing technology provided by the invention has no need for modification on shikonin, does not adopt high temperature dyeing, and the dyed fabric has high color fastness.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing side of shikonin to dacron
Method.
Background technology
Shikonin, is primarily present in Asian puccoon root, is naphthoquinone derivatives, shiny red acicular crystal.The hydrophobicity of shikonin
Side switch is long, therefore water-soluble poor, cellulose base fiber fabric can typically be dyeed using the method for first mordant dyeing.Asian puccoon
Being compatible with the environment property of quinone is good, is harmful to human health.But shikonin is difficult the directly synthetic fibers such as upper dye terylene.
The content of the invention
In order that the effective dyed polyester textiles of shikonin, the present invention is adopted the following technical scheme that.
A kind of shikonin comprises the following steps to the colouring method of dacron：（1）Phenol is dissolved in carbon tetrachloride；
（2）Shikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, surpassed
Clear solution is obtained under sound；（3）During dacron put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, and insulation dyeing 5 ~
30min；（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~
3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and the matter of carbon tetrachloride/phenol mixed solution
Amount is than being 1:2000~8000.
Further, described shikonin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to shikonin is modified, high-temperature dyeing is not used, fabric after dyeing
Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
Shikonin is as follows to the colouring method detailed step of dacron：
（1）20g phenol is dissolved in 180g carbon tetrachloride；
（2）0.6g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 2
Shikonin is as follows to the colouring method detailed step of dacron：
（1）300g phenol is dissolved in 100g carbon tetrachloride；
（2）0.3g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 3
Shikonin is as follows to the colouring method detailed step of dacron：
（1）50g phenol is dissolved in 250g carbon tetrachloride；
（2）1g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants 12 are added
Sodium alkyl benzene sulfonate, clear solution is obtained under ultrasound；
（3）During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 4
Shikonin is as follows to the colouring method detailed step of dacron：
（1）200g phenol is dissolved in 200g carbon tetrachloride；
（2）0.1g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. colouring method of a kind of shikonin to dacron, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in carbon tetrachloride；
（2）Shikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid is added
Sodium, clear solution is obtained under ultrasound；
（3）During dacron put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
2. shikonin as claimed in claim 1 is to the colouring method of dacron, described carbon tetrachloride/phenol mixed solution
The mass ratio of carbon tetrachloride and phenol be 1:0.1~3.
3. shikonin as claimed in claim 1 is to the colouring method of dacron, described surfactant sodium dodecyl base benzene
Sodium sulfonate is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. shikonin as claimed in claim 1 is to the colouring method of dacron, described shikonin and carbon tetrachloride/phenol
The mass ratio of mixed solution is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089399.0A CN106702770A (en) | 2016-12-01 | 2016-12-01 | Dyeing method of shikonin on polyester fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089399.0A CN106702770A (en) | 2016-12-01 | 2016-12-01 | Dyeing method of shikonin on polyester fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106702770A true CN106702770A (en) | 2017-05-24 |
Family
ID=58934400
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611089399.0A Pending CN106702770A (en) | 2016-12-01 | 2016-12-01 | Dyeing method of shikonin on polyester fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106702770A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06248581A (en) * | 1993-02-22 | 1994-09-06 | Mitsui Petrochem Ind Ltd | Method for dyeing fiber substance with shikonin-based dye |
| CN103373913A (en) * | 2012-04-15 | 2013-10-30 | 四川省中医药科学院 | Extraction method of alkannin |
| CN104088167A (en) * | 2014-07-04 | 2014-10-08 | 常州大学 | Method for improving color depth and light fastness of natural dye-dyed fabric |
| CN105780527A (en) * | 2014-12-22 | 2016-07-20 | 常熟市虹桥印染有限公司 | Dye liquor for printing and dyeing of flocked cloth |
-
2016
- 2016-12-01 CN CN201611089399.0A patent/CN106702770A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06248581A (en) * | 1993-02-22 | 1994-09-06 | Mitsui Petrochem Ind Ltd | Method for dyeing fiber substance with shikonin-based dye |
| CN103373913A (en) * | 2012-04-15 | 2013-10-30 | 四川省中医药科学院 | Extraction method of alkannin |
| CN104088167A (en) * | 2014-07-04 | 2014-10-08 | 常州大学 | Method for improving color depth and light fastness of natural dye-dyed fabric |
| CN105780527A (en) * | 2014-12-22 | 2016-07-20 | 常熟市虹桥印染有限公司 | Dye liquor for printing and dyeing of flocked cloth |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170524 |
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| WD01 | Invention patent application deemed withdrawn after publication |